scholarly journals Effect of steam autoclaving on laser sintered polyamide 12

2020 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
James Robert Wingham ◽  
Maha Omran ◽  
Joanna Shepherd ◽  
Candice Majewski
Keyword(s):  
Mechanical Properties ◽  
Water Content ◽  
Elongation At Break ◽  
Content Type ◽  
Polyamide 12 ◽  
Root Cause ◽  
Medical Sector ◽  
Influence Of Water ◽  
The Difference ◽  
Direct Use

Purpose The use of laser sintering (LS) in the medical sector has increased dramatically in recent years. With the move towards direct use of these parts in clinical applications, there is a greater need to understand the effects of standard processes on the part properties. The purpose of this study is to determine the effect that steam sterilisation has on the mechanical properties of LS polyamide 12 parts. Design/methodology/approach The research presented here focusses on the effect of a single steam sterilisation cycle on the mechanical properties of polyamide 12 parts manufactured using LS. The influence of water content on the properties was investigated, with additional drying steps trialled to establish the potential to reverse any changes observed and to determine their root cause. Findings The results show that steam sterilisation has a significant effect on the mechanical properties of LS polyamide 12 parts, with a 39% reduction in elastic modulus, a 13% decrease in ultimate tensile strength and a 64% increase in the elongation at break. These properties were also all found to correlate with the water content, suggesting that this was the cause of the difference. The original properties of the parts were able to be recovered after oven drying. Practical implications These results show that with an additional drying step, LS polyamide 12 parts can be steam sterilised with no effect on the mechanical properties. Originality/value This is believed to be the first investigation into the effects of steam sterilisation in isolation on LS polyamide 12 parts, the first instance of drying parts to recover mechanical properties and the first instance of multiple water content measurements being directly linked to the mechanical properties.

scholarly journals Influence of Water Content on the β-Sheet Formation, Thermal Stability, Water Removal, and Mechanical Properties of Silk Materials

2016 ◽  
Vol 17 (3) ◽  
pp. 1057-1066 ◽  
Author(s):  
Kenjiro Yazawa ◽  
Kana Ishida ◽  
Hiroyasu Masunaga ◽  
Takaaki Hikima ◽  
Keiji Numata
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Water Content ◽  
Water Removal ◽  
Influence Of Water ◽  
Β Sheet

Influence of energy density on polyamide 12 processed by SLS: from physical and mechanical properties to microstructural and crystallization evolution

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Tiago Czelusniak ◽  
Fred Lacerda Amorim
Keyword(s):  
Mechanical Properties ◽  
Surface Roughness ◽  
Energy Density ◽  
Laser Energy ◽  
Polymer Degradation ◽  
High Energy ◽  
Content Type ◽  
Polyamide 12 ◽  
Line Spacing ◽  
Scan Line

Purpose This paper aims to provide a detailed study on influence of the laser energy density on mechanical, surface and dimensional properties of polyamide 12 (PA12) parts produced by selective laser sintering (SLS), providing the microstructural and crystallization evolution of the samples produced at different energy densities. Design/methodology/approach Making use of a space filling design of experiments, a wide range of laser sintering parameters is covered. Surface morphology is assessed by means of profile measurements and scanning electron microscopy (SEM) images. Mechanical testing, SEM, X-ray diffraction (XRD), differential scanning calorimeter (DSC) and infrared spectroscopy (FTIR) were used to assess the influence of energy density on structural and mechanical properties. Findings Results show a high dependency of the properties on the laser energy density and also a compromise existing between laser exposure parameters and desired properties of laser sintered parts. Surface roughness could be associated to overlap degree when using higher scan line spacing values and lower laser speeds improved surface roughness when high scan line spacing is used. Higher mechanical properties were found at higher energy density levels, but excessively high energy density decreased mechanical properties. A transition from brittle to ductile fracture with increasing energy density could be clearly observed by mechanical analysis and SEM. XRD and DSC measurements show a decrease on the crystal fraction with increasing energy densities, which corroborated the plastic behavior observed, and FTIR measurements revealed polymer degradation through chain scission might occur at too high energy densities. Originality/value Valuable guidelines are given regarding energy density optimization for SLS of PA12 considering not only quality criteria but also microstructure characteristics. Surface properties are studied based on the concept of degree of overlap between laser scanning lines. For the first time, crystallization behavior of SLS PA12 parts produced at different energy levels was studied by means of XRD measurements. Polymer degradation of SLS PA12 parts was evaluated with FTIR, which is a non-destructive and easy test to be conducted.

Influence of Strength Attenuation for Silt Soil on the Fatigue Life of Semi-Rigid Base

2013 ◽  
Vol 353-356 ◽  
pp. 120-124
Author(s):  
Xiao Ming Yi ◽  
Song Gen Wang ◽  
Xiu Guang Song ◽  
Zhen Qing Liu
Keyword(s):  
Fatigue Life ◽  
Water Content ◽  
Yellow River ◽  
Asphalt Pavement ◽  
Rigid Base ◽  
Influence Of Water ◽  
Design Value ◽  
The Difference ◽  
Early Damage ◽  
Resilience Modulus

Influence of water content on the resilience modulus for silt soil in Yellow River alluvial plane is studied by laboratory tests. And its found that resilience modulus decrease dramatically when the water content exceeds the optimum. So the subgrade cant support the pavement structure enough, which could make the fatigue life of semi-rigid base little than the design value. Basing on the distribution of the water content in real, the silt subgrade is divided into three parts in accordance with the difference of resilience modulus. Then, the tensile stress and fatigue life of semi-rigid base is gotten, and results show the strength decay of subgrade reduced the fatigue life of semi-rigid base up to 50%, which exposes the causes of early damage of semi-rigid base asphalt pavement on silt subgrade.

Preparation and Properties of Sponge Rubber Based on Natural Rubber and Cassava Starch

2014 ◽  
Vol 931-932 ◽  
pp. 68-72
Author(s):  
Komsun Temna ◽  
Nitinart Saetung ◽  
Anuwat Saetung
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Cassava Starch ◽  
Interfacial Interaction ◽  
Morphological Properties ◽  
Elongation At Break ◽  
Cure Time ◽  
The Difference ◽  
Cure Characteristic

In this work, the sponge rubbers based on cassava starch masterbatch in latex phase with the difference technique (non-gelatinized and gelatinized cassava starch) were preformed. The cassava starch contents from 0 to 70 phr were also studied. The cure characteristic, mechanical and morphological properties were investigated. It was found that the scorch time and cure time were increased with an increasing of cassava starch contents in both techniques. The mechanical properties i.e., tensile strength, elongation at break and tear strength were decreased with an increasing of cassava starch contents, except 500% modulus. However, the sponge based on gelatinized technique gave the better mechanical properties than that of non-gelatinized cassava starch. The SEM micrographs of sponge NR from gelatinized technique were also able to confirm a good interfacial interaction between hydrophilic cassava starch and hydrophobic NR.

scholarly journals Experimental Investigation on the Influence of Water Content on the Mechanical Properties of Coal under Conventional Triaxial Compression

2020 ◽  
Vol 2020 ◽  
pp. 1-11
Author(s):  
Meichang Zhang ◽  
Rongshan Nie
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Internal Friction ◽  
Water Content ◽  
Triaxial Compression ◽  
Friction Angle ◽  
Conventional Triaxial Compression ◽  
Influence Of Water ◽  
Confining Pressures ◽  
Water Contents

The presence of water is one of the most important factors in coal mining, and it has a dual influence on the mechanical behavior of rock. To study the influence of water content on the mechanical properties of coal under complicated stress conditions, dry coal specimens and wet coal specimens with water contents of 1.8% and 3.6% were conducted by uniaxial and conventional triaxial compression tests. The relations between the uniaxial compressive strength, deformation, and water content were observed. The reductions in the strength and elastic modulus under different confining pressures were obtained. The mechanical properties of coal specimens with different water contents under triaxial compression were studied. The influences of water content on the microstructure, clay minerals, internal friction angle, and cohesive force of coal were discussed. The results show that the strengths and elastic moduli of wet specimens are clearly lower than those of dry specimens under different confining pressures. The water content has a significant influence on the postfailure mechanical behavior of coal. The loss rates of strength and elastic modulus decrease with increasing confining pressure. The water content has almost no effect on the internal friction angle, while the cohesive force of the saturated specimens is 36.5% lower than that of the dry specimens. The results can provide a reference for inhibiting the occurrence of disasters during coal mining and exploiting coal efficiently.

Mechanical properties and water absorption behaviour of PLA and PLA/wood composites prepared by 3D printing and injection moulding

2019 ◽  
Vol 25 (4) ◽  
pp. 672-678 ◽  
Author(s):  
Josef Valentin Ecker ◽  
Andreas Haider ◽  
Ivana Burzic ◽  
Axel Huber ◽  
Gerhard Eder ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
3D Printing ◽  
Water Absorption ◽  
Tensile Properties ◽  
Injection Moulding ◽  
Water Storage ◽  
Wood Composites ◽  
Content Type ◽  
Influence Of Water ◽  
3D Printed

Purpose This papers aims to study the influence of water absorption on the mechanical properties of poly lactic acid (PLA) and PLA/Wood composites. Virgin PLA and PLA/Wood double-bone-shaped specimens were prepared by two methods: injection moulding and 3D printing. The results were compared to each other and showed the influence of the production method on the properties of the produced parts. Design/methodology/approach Morphology studies were done by scanning electron microscopy (SEM) from fracture surfaces of tensile and notched impact specimens of all samples. Tensile properties were analysed by the production and testing of dog-bone-shaped samples. Heat deflection temperature (HDT) was tested, as also was the crystallinity of the tested samples by differential scanning calorimetry. Findings The values for notched impact strength were higher upon water uptake in the case of injection-moulded specimens, which was not the case with 3D-printed specimens. Tensile properties of the specimens produced by both methods were reduced after water absorption tests. Values of the HDT were also lower after water absorption tests studied for both processing methods. Originality/value Morphology studies were done by SEM from fracture surfaces of tensile as well as notched impact specimens of injection-moulded and 3D-printed samples. The effect of water storage on various samples was tested. The two different production technologies were compared to each other owing to their influence of water storage. This study also dealt with NFC compounds and produced NFC composites and the influence of water storage on these samples.

Test and Calculation Model of Thermal Conductivity of Concrete

2022 ◽  
Vol 905 ◽  
pp. 314-319
Author(s):  
Lin Liu ◽  
Jing Chang Wang
Keyword(s):  
Thermal Conductivity ◽  
Water Content ◽  
Engineering Calculation ◽  
Calculation Model ◽  
Test Results ◽  
Hydration Degree ◽  
Plate Method ◽  
Influence Of Water ◽  
The Difference ◽  
Calculated Model

In order to study the influence of water content and hydration degree on the thermal conductivity of concrete, based on the steady-state plate method, the influence of water content, temperature, hydration degree and other factors on the thermal conductivity of early concrete was studied, and the calculation model of thermal conductivity of early concrete was established according to the test results and influence rules. The results show that there is a linear relationship between the thermal conductivity and water content at 28d, the higher the hydration degree is, the lower the thermal conductivity of concrete is; the difference between the measured value and the calculated model value is small, and the calculation formula can meet the requirements of engineering calculation.

Effects of the 3DP process parameters on mechanical properties of polylactic acid part used for medical purposes

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Sunthorn Chaitat ◽  
Nattapon Chantarapanich ◽  
Sujin Wanchat
Keyword(s):  
Mechanical Properties ◽  
Gamma Radiation ◽  
Polylactic Acid ◽  
Gamma Ray ◽  
Compressive Load ◽  
Tensile Load ◽  
Test Method ◽  
Content Type ◽  
Tension And Compression ◽  
The Difference

Purpose This paper aims to investigate effect of infill density, fabricated built orientation and dose of gamma radiation to mechanical tensile and compressive properties of polylactic acid (PLA) part fabricated by fused deposit modelling (FDM) technique for medical applications. Design/methodology/approach PLA specimens for tensile and compressive tests were fabricated using FDM machine. The specimens geometry and test method were referred to ASTM D638 and ASTM D695, respectively. Three orientations under consideration were flat, edge and upright, whereas the infill density ranged from 0 to 100%. The gamma radiation dose used to expose to specimens was 25 kGy. The collected data included stress and strain, which was used to find mechanical properties, i.e. yield strength, ultimate tensile strength (UTS), fracture strength, elongation at yield, elongation at UTS and elongation at break. The t-test was used to access the difference in mechanical properties. Findings Compressive mechanical properties is greater than tensile mechanical properties. Increasing number of layer parallel to loading direction and infill density, it enhances the material property. Upright presents the lowest mechanical property in tensile test, but greatest in compressive test. Upright orientation should not be used for part subjecting to tensile load. FDM is more proper for part subjecting to compressive load. FDM part requires undergoing gamma ray for sterilisation, the infill density no less than 70 and 60% should be selected for part subjecting to tensile and compressive load, respectively. Originality/value This study investigated all mechanical properties in both tension and compression as well as exposure to gamma radiation. The results can be applied in selection of FDM parameters for medical device manufacturing.

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