Position of erosion marks on the surface of single-crystal and coarse-grained cathodes after a short-pulse vacuum spark

Author(s):  
E. V. Nefedtsev ◽  
S. A. Onischenko
2012 ◽  
Vol 14 (2) ◽  
pp. 126-134 ◽  
Author(s):  
Nithyanand Kota ◽  
O. Burak Ozdoganlar

2011 ◽  
Vol 78 (4) ◽  
Author(s):  
X. Yin ◽  
K. Komvopoulos

Elastic-plastic indentation of a single-crystal half-space by a rigid cylinder was analyzed by discrete dislocation plasticity. Short-range dislocation interactions were modeled by a set of constitutive rules of dislocation emission, glide, pinning (by obstacles), and annihilation. The occurrence of the first dislocation dipole, multiplication of dislocations, and evolution of subsurface stress field were examined in terms of contact load, dislocation source density, slip-plane distance and orientation angle, and indenter radius. In the presence of defects (dislocation sources), the critical load for dislocation initiation is less than that of a defect-free medium and depends on dislocation source density, slip-plane distance, and indenter radius. The critical indenter radius resulting in deformation under the theoretical material strength is determined from numerical results, and the role of dislocation obstacles is interpreted in terms of their spatial density. Simulations provide insight into yielding and plastic deformation of indented single-crystal materials, and establish a basis for developing coarse-grained plasticity models of localized contact deformation in polycrystalline solids.


2000 ◽  
Vol 657 ◽  
Author(s):  
A. V. Sumant ◽  
O. Auciello ◽  
A. R. Krauss ◽  
D. M. Gruen ◽  
D. Ersoy ◽  
...  

ABSTRACTThe mechanical, thermal, chemical, and tribological properties of diamond make it an ideal material for the fabrication of MEMS components. However, conventional CVD diamond deposition methods result in either a coarse-grained pure diamond structure that prevents high- resolution patterning, or in a fine-grained diamond film with a significant amount of intergranular non-diamond carbon. At Argonne National Laboratory, we are able to produce phase-pure ultrananocrystalline diamond (UNCD) films for the fabrication of MEMS components. UNCD is grown by microwave plasma CVD using C60-Ar or CH4-Ar plasmas, resulting in films that have 3-5 nm grain size, are 10-20 times smoother than conventionally grown diamond films, and can have mechanical properties similar to that of single crystal diamond. We used lithographic patterning, lift-off, and etching, in conjunction with the capability for growing UNCD on SiO2 to fabricate 2-D and 3-D UNCD-MEMS structures. We have performed initial characterization of mechanical properties by using nanoindentation and in-situ TEM indentor techniques. The values of Hardness (∼88 GPa) and Young's modulus (∼ 864 GPa) measured are very close to those of single crystal diamond (100 GPa and 1000 GPa respectively). The results show that UNCD is a promising material for future high performance MEMS devices.


2018 ◽  
Author(s):  
Roberto Köferstein

Preparation of a very fine BaSnO3 powder by calcination of a barium tin 1,2-ethanediolato complex precursor and its sintering behaviour are described herein. A ratecontrolled calcination process to 820 °C leads to a nm-sized BaSnO3 powder with aspecific surface area of S = 15.1 m2/g (dav. = 55 nm). The powder has a slightly largercell parameter of a = 412.22(7) pm compared to the single crystal value, whichdecreases with increasing calcination temperature and reaches the reference value above1000 °C. The sintering behaviour is compared between fine- and coarse-grainedBaSnO3 powders. Corresponding powder compacts of the nano-sized BaSnO3 achieve arelative density of 90 % after sintering at 1600 °C for 1 h and at 1500 °C and a soakingtime of 30 h, whereas coarse-grained powder compacts reach only 80 % of the relative density at 1650 °C (10 h). Furthermore, the shrinkage mechanisms of fine and coarsegrainedpowder compacts have been investigated and are discussed.


1990 ◽  
Vol 195 ◽  
Author(s):  
Yening Wang ◽  
Linhai Sun ◽  
Jin Wu ◽  
Min Gu

ABSTRACTA large thermal hysteresis ( > 100 K) of elastic modulus was measured for coarse grained Y-Ba-Cu-O and Bi-Sr-Ca-Cu-O. Whereas, only a small thermal hysteresis (2∼3 K) near the velocity minima at 240 K, and 150 K was observed in Bi2 Sr2 CaCu2 O8 single crystal, which were found to be associated with phaselike transitions (PLT). The investigations of isothermal recovery of modulus for coarse grained YBCO and BSCCO disclose that the large thermal hysteresis may be attributed to the defects of pore size generated in the interconnecting region between grains as a result of PLT of weak first order but covering a wide temperature range. The mechanism of a large thermal hysteresis for coarse grained samples has been discussed in detail.


2013 ◽  
Vol 28 (20) ◽  
pp. 2763-2770 ◽  
Author(s):  
Weizhong Han ◽  
E.G. Fu ◽  
Michael J. Demkowicz ◽  
Yongqiang Wang ◽  
Amit Misra

Abstract


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