X-ray flux concentrating optics for improving the performance of light element energy dispersive spectroscopy

1998 ◽  
Author(s):  
David B. O'Hara
1999 ◽  
Vol 5 (S2) ◽  
pp. 588-589
Author(s):  
A. Nielson ◽  
J. Thorne

Ultra-thin polymer x-ray windows have been developed for energy dispersive spectroscopy (EDS) that enable analysis of the elements lighter in mass than sodium while protecting the detector from light and gases. Windowless detectors produce the ultimate in detector sensitivity, however that sensitivity is lost when ice and other contaminants form on the detector. Polymer windows have had a problem with icing in the past, however modern ultra-thin polymer windows contain metalized layers to prevent the diffusion of water. Nevertheless, over the course of time it has been observed that some detectors with polymer windows that are kept continually cool with liquid nitrogen form a thin layer of ice that attenuates light element sensitivity. The source of this water has been hypothesized to be a gradual leak of water vapor through the polymer x-ray window. This hypothesis has been questioned on the basis that the windows were helium leak tight to 1 x 10−9 mbar L/sec and helium is a smaller molecule than water.


The Analyst ◽  
1995 ◽  
Vol 120 (3) ◽  
pp. 783 ◽  
Author(s):  
Jill A. Cargnello ◽  
Jonathan J. Powell ◽  
Richard P. H. Thompson ◽  
Peter R. Crocker ◽  
Frank Watt

2011 ◽  
Vol 383-390 ◽  
pp. 7619-7623
Author(s):  
Z Z Lu ◽  
F. Yu ◽  
L. Yu ◽  
L. H. Cheng ◽  
P. Han

In this work, Si, Ge element composition distribution in Ge /Si1-xGex:C /Si substrate structure has been characterized and modified by planar scanning energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The Ge /Si1-xGex:C /Si substrate samples are grown by chemical vapor deposition (CVD) method. The accuracy of EDS value can be improved by ~ 32%. And the modified EDS results indicate the Ge distribution in the Ge/Si1-xGex:C/Si sub structure.


1980 ◽  
Vol 112 (6) ◽  
pp. 609-614 ◽  
Author(s):  
W. J. Turnock ◽  
G. H. Gerber ◽  
D. U. Sabourin

AbstractSamples of the bodies and elytra of Entomoscelis americana Brown were analyzed separately by X-ray energy-dispersive spectroscopy. Discriminant analysis revealed that the chemoprints of the bodies of newly-emerged beetles (1 wk old) were distinct from those of post-aestivation beetles (9- to 10-wk old). However, the chemoprints of the elytra of newly-emerged and post-aestivation beetles were not as different as those of the bodies as demonstrated by the overlap in the plot of the first two canonical variables. The variances of the mean difference of individual variables between newly-emerged and post-aestivation groups generally were smaller for elytra than for bodies. This suggests that the chemoprints of the elytra of E. americana are more stable than those of the bodies and consequently the elytra should be more suitable than the bodies in insect dispersal studies utilizing the X-ray energy-dispersive spectroscopy technique.


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