DLTS Study of Room-Temperature Defect Annealing in High-Purity n-Type Si

2019 ◽  
Vol 3 (4) ◽  
pp. 387-393 ◽  
Author(s):  
Jan Bleka ◽  
Eduard V. Monakhov ◽  
Berit S. Avset ◽  
Bengt G. Svensson
Keyword(s):  
High Purity ◽  
Room Temperature ◽  
Defect Annealing

Preparation of High-Purity Ultrafine α-Al2O3 by Solid-State Reaction at Room Temperature

2008 ◽  
Vol 368-372 ◽  
pp. 683-685
Author(s):  
Cheng Wei Hao ◽  
Bo Lin Wu ◽  
Ji Yan Li
Keyword(s):  
Solid State ◽  
High Purity ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Raw Materials ◽  
Phase Particle ◽  
Phase Transformation Temperature ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Α Al2o3

Ammonium aluminium carbonate hydroxide (AACH), with a small quantity of γ-AlOOH, was synthesized through solid-state reaction at room temperature using AlCl3·6H2O and NH4HCO3 as raw materials and polyethylene glycol (PEG-10000) as the dispersant. After calcined at 1100°C for 1.5h, α-Al2O3 powders with primary particle sizes of 20~30nm were obtained. The crystal phase, particle size and morphology of the high-purity ultrafine α-Al2O3 were characterized. The results showed that a small quantity of γ-AlOOH in the AACH decomposed and formed crystal seeds. The presence of crystal seeds reduced the nucleation activation energy and therefore reduced the phase transformation temperature.

Anelastic deformation of high purity aluminum at room temperature

1976 ◽  
Vol 10 (2) ◽  
pp. 189-194 ◽  
Author(s):  
Nahum Nir ◽  
Edward W. Hart ◽  
Che-Yu Li
Keyword(s):  
High Purity ◽  
Room Temperature ◽  
High Purity Aluminum ◽  
Anelastic Deformation

Preparing high purity λ-Ti3O5 and Li/λ-Ti3O5 as a high performance electromagnetic wave absorber

2021 ◽  
Author(s):  
xiankai fu ◽  
Wanqi Chen ◽  
Xiaowen Hao ◽  
Zhimin Zhang ◽  
Ruolan Tang ◽  
...  
Keyword(s):  
Electromagnetic Wave ◽  
Microwave Absorption ◽  
High Purity ◽  
High Performance ◽  
Room Temperature

This paper reports a new candidate material λ-Ti3O5 for microwave absorption. λ-Ti3O5 has been proposed to be metastable and has emerged at room temperature only in the form of nanocrystals....

Zinc carbonate recovery from brass melting slag

2021 ◽  
Vol 98 ◽  
pp. 14-18
Author(s):  
Thao Nguyen Thi ◽  
◽  
Nam Pham Ky ◽  
Ngoc Tran Vu Diem
Keyword(s):  
Sulfuric Acid ◽  
High Purity ◽  
Room Temperature ◽  
Ph Value ◽  
Zinc Carbonate ◽  
Leaching Solution ◽  
Optimized Conditions ◽  
Melting Slag

Brass melting slag (20.38 wt.% Zn) was leached in sulfuric acid with concentration of (50 + 80) g/l H2SO4, leaching temperature of (30 + 60) °C for (30 + 120) min. The optimized conditions for 94.16% Zn extraction from brass melting slag were found as 70 g/l H2SO4, room temperature and 90 min. The leaching solution was purified by removal of Fe through Fe(OH)3 precipitation when adding ZnO to adjust pH value of 5. The solution was continuously cemented by Zn metal at 60 °C for 60 min to obtain Cu metal with high purity of 99 wt.% Cu. The purified solution with 37.64 g/l Zn was modified by Na2C03 to have pH value of about 6 and precipitation of ZnC03 (94.14 %).

Fatigue Crack Growth in SA508-CL2 Steel in a High Temperature, High Purity Water Environment

1974 ◽  
Vol 96 (4) ◽  
pp. 255-260 ◽  
Author(s):  
T. L. Gerber ◽  
J. D. Heald ◽  
E. Kiss
Keyword(s):  
Fatigue Crack ◽  
Fatigue Crack Growth ◽  
Crack Growth ◽  
Growth Rates ◽  
High Purity ◽  
Room Temperature ◽  
Water Environment ◽  
Cyclic Frequency ◽  
Asme Code ◽  
Temperature Rate

Fatigue crack growth tests were conducted with 1 in. (25.4 mm) plate specimens of SA508-CL2 steel in room temperature air, 550 deg F (288 deg C) air and in a 550 deg F (288 deg C), high purity, water environment. Zero-tension load controlled tests were run at cyclic frequencies as low as 0.037 CPM. Results show that growth rates in the simulated Boiling Water Reactor (BWR) water environment are 4 to 8 times faster than growth rates observed in 550 deg F (288 deg C) air and these rates are 8 to 15 times faster than the room temperature rate. In the BWR water environment, lowering the cyclic frequency from 0.37 CPM to 0.037 CPM caused only a slight increase in the fatigue crack growth rate. All growth rates measured in these tests were below the upper bound design curve presented in Section XI of the ASME Code.

scholarly journals The significance of self-annealing at room temperature in high purity copper processed by high-pressure torsion

2016 ◽  
Vol 656 ◽  
pp. 55-66 ◽  
Author(s):  
Yi Huang ◽  
Shima Sabbaghianrad ◽  
Abdulla I. Almazrouee ◽  
Khaled J. Al-Fadhalah ◽  
Saleh N. Alhajeri ◽  
...  
Keyword(s):  
High Pressure ◽  
High Purity ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Purity Copper

Fracture Mechanics of Y2O3 Ceramics at High Temperatures

2014 ◽  
Vol 89 ◽  
pp. 88-93
Author(s):  
Marek Boniecki ◽  
Zdzislaw Librant ◽  
Władysław Wesołowski ◽  
Magdalena Gizowska ◽  
Marcin Osuchowski ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Grain Size ◽  
High Temperature ◽  
Fracture Mechanics ◽  
High Purity ◽  
Room Temperature ◽  
Bending Strength ◽  
Hot Isostatic Pressing ◽  
Temperature Changes ◽  
Four Point Bending

Fracture toughness KIc and four-point bending strength σc at high temperature (up to 1500 °C) of Y2O3 ceramics of various grain size were measured. The ceramics were prepared by pressureless air sintering and next hot isostatic pressing of high purity (99.99%) Y2O3 powder. Relative density of about 99 % was achieved. Photos of microstructures revealed small pores distributed mainly inside grains. For smallest grain size (2 - 9 μm) ceramics KIc and σc are almost constant from 20 ° to 1200 °C and next they decrease. For biggest grain size (about 44 μm) they increase up to 800 °C and next they keep constant up to 1200 °C. The micrographs analyses of fracture surfaces indicated that transgranular mode of fracture at room temperature changes to almost intergranular at higher temperatures.

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