scholarly journals Optimization of Ionic Liquid Based Simultaneous Ultrasonic- and Microwave-Assisted Extraction of Rutin and Quercetin from Leaves of Velvetleaf (Abutilon theophrasti) by Response Surface Methodology

2014 ◽  
Vol 2014 ◽  
pp. 1-11 ◽  
Author(s):  
Chunjian Zhao ◽  
Zhicheng Lu ◽  
Chunying Li ◽  
Xin He ◽  
Zhao Li ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Extraction Time ◽  
Conventional Heating ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Influential Parameters

An ionic liquids based simultaneous ultrasonic and microwave assisted extraction (ILs-UMAE) method has been proposed for the extraction of rutin (RU), quercetin (QU), from velvetleaf leaves. The influential parameters of the ILs-UMAE were optimized by the single factor and the central composite design (CCD) experiments. A 2.00 M 1-butyl-3-methylimidazolium bromide ([C4mim]Br) was used as the experimental ionic liquid, extraction temperature 60°C, extraction time 12 min, liquid-solid ratio 32 mL/g, microwave power of 534 W, and a fixed ultrasonic power of 50 W. Compared to conventional heating reflux extraction (HRE), the RU and QU extraction yields obtained by ILs-UMAE were, respectively, 5.49 mg/g and 0.27 mg/g, which increased, respectively, 2.01-fold and 2.34-fold with the recoveries that were in the range of 97.62–102.36% for RU and 97.33–102.21% for QU with RSDs lower than 3.2% under the optimized UMAE conditions. In addition, the shorter extraction time was used in ILs-UMAE, compared with HRE. Therefore, ILs-UMAE was a rapid and an efficient method for the extraction of RU and QU from the leaves of velvetleaf.

scholarly journals Microwave – Assisted Extraction of Chlorogenic Acid from Coffee liberica L

2015 ◽  
Vol 14 (2) ◽  
pp. 58 ◽  
Author(s):  
Josephine Q. Borja ◽  
Marylou M Uy ◽  
Jose Salvador Lim ◽  
Matthew Edson Ong ◽  
Alejandro Miguel Ros
Keyword(s):  
Chlorogenic Acid ◽  
Taguchi Design ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Solvent Concentration ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Effect On Yield

This study applied microwave-assisted extraction of chlorogenic acid (CGA) from Coffee liberica L. using ethanol as solvent. It sought to determine the effects of temperature, extraction time, solvent-to-solid ratio, and solvent concentration on the CGA yield expressed as gallic acid equivalent per litre (mg GAE L-1). The values of these factors were varied at three levels each and experiments were implemented using the L934 orthogonal array of the Taguchi design of experiment. Results showed that increasing the solvent-to-solid ratio from 2.5 to 7.5 mL g--1decreased the yield significantly. Conversely, increasing the solvent concentration from 0.6 to 0.7 (v v-1) increased the yield, but beyond this, lower yield was obtained. Likewise, yield increased when the extraction time was increased from 5 to 7 minutes but decreased subsequently when extraction was extended to 10 minutes. Temperature did not show significant effect on yield. Among the factors tested the solvent- to-solid ratio has the most significant effect on yield, followed by solvent concentration and extraction time while temperature had no significant effect. In the Taguchi design the highest yield of 304.90±0.58 mg GAE L-1 was obtained at 90°C, extraction time of 7 minutes, solvent-to-solid ratio of 2.5 mL g-1 and solvent concentration of 0.8 (v v-1). Using the same extraction temperature and time and solvent-to-solid ratio but lower solvent concentration, the confirmatory run resulted is significantly higher yield of 854.35±3.35 mg GAE L-1. Chlorogenic acid was identified in the extract at a concentration of 3152 mg L-1. By applying Soxhlet extraction using the same solvent concentration and solvent-to-solid ratio at the same temperature as that of the confirmatory run the yield was significantly lower at 570.42±5.3 mg GAE L-1.

scholarly journals Application of Ionic Liquids in the Microwave-Assisted Extraction of Pectin from Lemon Peels

2012 ◽  
Vol 2012 ◽  
pp. 1-8 ◽  
Author(s):  
Huang Guolin ◽  
Shi Jeffrey ◽  
Zhang Kai ◽  
Huang Xiaolan
Keyword(s):  
Response Surface Methodology ◽  
Ionic Liquid ◽  
Fourier Transform ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Optimal Parameters ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Scanning Electron

Microwave-assisted extraction of pectin from lemon peels by using ionic liquid as alternative solvent was investigated. The extracted pectin was detected by Fourier transform infrared spectra. The extraction conditions were optimized through the different experiments in conjunction with the response surface methodology. A pectin yield of 24.68 % was obtained under the optimal parameters: the extraction temperature of 88°C, the extraction time of 9.6 min, and a liquid-solid ratio of 22.7 ml⋅g-1. The structure of the pretreated lemon peel samples and the samples after microwave-assisted extraction were characterized by a field emission scanning electron microscope.

scholarly journals Separation of the main flavonoids and essential oil from seabuckthorn leaves by ultrasonic/microwave-assisted simultaneous distillation extraction

2018 ◽  
Vol 5 (7) ◽  
pp. 180133 ◽  
Author(s):  
Chunying Li ◽  
Jingjing Zhang ◽  
Chunjian Zhao ◽  
Lei Yang ◽  
Wenyan Zhao ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Extraction Time ◽  
Ultrasonic Power ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Simultaneous Distillation Extraction ◽  
Ultrasonic Assisted Extraction ◽  
Optimized Conditions

Volatile essential oils (EOs), non-volatile rutin (RU), quercetin (QU), kaempferol (KA) and isorhamnetin (IS) were effectively extracted and isolated from seabuckthorn ( Hippophae rhamnoides L.) leaves by ionic liquid-based ultrasound/microwave-assisted simultaneous distillation extraction (ILUMASDE). After optimization by response surface methodology, EOs, RU, QU, KA and IS were separated under the following optimum conditions: an ionic liquid of 1.0 M 1-butyl-3-methyl imidazole bromine salt ([C4mim]), liquid/solid ratio of 12 ml g −1 , extraction time of 34 min, microwave power of 540 W and a fixed ultrasonic power of 50 W. Under the optimized conditions of ILUMASDE, the extraction yields of RU, QU, KA, IS and EOs were 9.18 ± 0.35, 5.52 ± 0.23, 3.03 ± 0.11, 5.64 ± 0.24 mg g −1 and 0.095 ± 0.004%, respectively. The yield of EOs obtained using ILUMASDE was 1.07-fold higher than that obtained by conventional hydrodistillation extraction (HDE). In addition, the components of the EOs obtained using ILUMASDE and HDE were similar. The extraction yields of RU, QU, KA, IS obtained by ILUMASDE were 1.03–1.35-fold higher than that obtained by the ethanol ultrasonic-assisted extraction (EUAE), ionic liquid-based ultrasonic-assisted extraction (ILUAE) and ionic liquid-based microwave-assisted extraction (ILMAE). And the extraction time used by ILUMASDE was 34 min, which is 14.17%, 56.67%, 56.67% and 85.00% less than those used by HDE, EUAE, ILUAE and ILMAE, respectively. Therefore, ILUMASDE can be considered a rapid and efficient method for extracting flavonoids and EO from seabuckthorn ( Hippophae rhamnoids L.) leaves.

Microwave-Assisted Extraction of Chlorophyll from Filter Mud of Sugercane Mill and Component Analysis

2012 ◽  
Vol 518-523 ◽  
pp. 430-435 ◽  
Author(s):  
Hai Rong Guo ◽  
Shao Ying Ma ◽  
Xiao Fei Wang ◽  
Er Fang Ren ◽  
Yuan Yuan Li
Keyword(s):  
Irradiation Time ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Optimal Conditions ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Conventional Extraction ◽  
Filter Mud ◽  
Strong Absorption Peak

Microwave-assisted extraction (MAE) was used to extract chlorophylls from filter mud. Ethanol was used as the solvent. The optimal conditions for the MAE of chlorophylls were concluded from the study as the irradiation time, 50 s, the ratio of liquid to solid, 8:1 (mL/g), the extraction temperature, 40 °C, and the extraction time, 60 min. Compared with conventional extraction, the MAE of chlorophylls from the filter mud was more effective. The extraction time for MAE was 60 min with 0.277 mg/g chlorophyll yield, while conventional extraction needed 240 min with only about 0.259 mg/g chlorophyll yield. The Ultraviolet Absorption Spectra of the extracted chlorophylls showed that there was a strong absorption peak at about 663 nm. C=N, Mg-N and C-N was not seen existed from the infrared spectroscopy probably because that the mixed extracts were not purified and the chlorophyll content was less.

scholarly journals Microwave-assisted extraction of non-polar compounds from pistachio hull and characterization of extracts

2018 ◽  
Vol 69 (3) ◽  
pp. 260 ◽  
Author(s):  
H. N. Özbek ◽  
D. Koçak Yanık ◽  
S. Fadıloğlu ◽  
H. Keskin Çavdar ◽  
F. Göğüş
Keyword(s):  
Microwave Power ◽  
Polar Compounds ◽  
Good Alternative ◽  
Tocopherol Content ◽  
Extraction Time ◽  
Total Phenolic ◽  
Microwave Assisted Extraction ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction

Soxhlet and microwave assisted extraction (MAE) methods were used to obtain non-polar compounds from pistachio hull. MAE parameters (liquid to solid ratio, microwave power, and extraction time) were studied to obtain maximum extraction yield. The optimal conditions were found to be liquid to solid ratio of 15:1 (v/w), microwave power of 250 W and extraction time of 12.5 min. The extraction yields were 9.81 and 9.50% for MAE and Soxhlet methods, respectively. The total phenolic content, antioxidant activity and tocopherol content of the extract obtained by MAE was found to be significantly higher than those of the Soxhlet extract (p < 0.05). The results showed that the extract contained α-tocopherols (567.65 mg/kg) and oleic acid (48.46%) as the major tocopherols and fatty acids. These findings propose that hull extracts can be considered as a good source of natural bioactive compounds and MAE can be a good alternative to the traditional Soxhlet method.

scholarly journals Effects of Microwave-Assisted Extraction Conditions on Antioxidant Capacity of Sweet Tea (Lithocarpus polystachyus Rehd.)

Antioxidants ◽  
2020 ◽  
Vol 9 (8) ◽  
pp. 678
Author(s):  
Ao Shang ◽  
Min Luo ◽  
Ren-You Gan ◽  
Xiao-Yu Xu ◽  
Yu Xia ◽  
...  
Keyword(s):  
Antioxidant Capacity ◽  
Microwave Power ◽  
Ethanol Concentration ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Optimal Conditions ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Sample Ratio

In this study, the effects of microwave-assisted extraction conditions on antioxidant capacity of sweet tea (Lithocarpus polystachyus Rehd.) were studied and the antioxidants in the extract were identified. The influences of ethanol concentration, solvent-to-sample ratio, microwave power, extraction temperature and extraction time on Trolox equivalent antioxidant capacity (TEAC) value, ferric reducing antioxidant power (FRAP) value and total phenolic content (TPC) were investigated by single-factor experiments. The response surface methodology (RSM) was used to study the interaction of three parameters which had significant influences on antioxidant capacity including ethanol concentration, solvent-to-sample ratio and extraction time. The optimal conditions for the extraction of antioxidants from sweet tea were found as follows—ethanol concentration of 58.43% (v/v), solvent-to-sample ratio of 35.39:1 mL/g, extraction time of 25.26 min, extraction temperature of 50 ℃ and microwave power of 600 W. The FRAP, TEAC and TPC values of the extract under the optimal conditions were 381.29 ± 4.42 μM Fe(II)/g dry weight (DW), 613.11 ± 9.32 μM Trolox/g DW and 135.94 ± 0.52 mg gallic acid equivalent (GAE)/g DW, respectively. In addition, the major antioxidant components in the extract were detected by high-performance liquid chromatography with diode array detection (HPLC-DAD), including phlorizin, phloretin and trilobatin. The crude extract could be used as food additives or developed into functional food for the prevention and management of oxidative stress-related diseases.

Study on Microwave-Assisted Extraction of Polysaccharides from Radix astragali

2014 ◽  
Vol 675-677 ◽  
pp. 1634-1637 ◽  
Author(s):  
Cong Liang Huang
Keyword(s):  
Irradiation Time ◽  
Good Alternative ◽  
Extraction Yield ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Radix Astragali ◽  
Solid Ratio ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Orthogonal Test Design

In this study, microwave-assisted extraction (MAE) was employed for the extraction of polysaccharides from Radix Astragali (PRA). The extraction parameters that influenced the extraction yield of PRA were optimized by orthogonal test design. The results showed that the optimal MAE conditions were as followings: liquid-solid ratio of 18 ml/g, irradiation time of 8 min, irradiation power of 300 W and extraction temperature of 65°C, while extraction yield of PRA was 8.39 %. The developed MAE method provided a good alternative for the extraction of PRA.

Optimization of Ultrasound-Assisted Extraction of Polysaccharides from the Chinese Medicinal Plant Rhodiola Sachalinensis A. BOR

2013 ◽  
Vol 448-453 ◽  
pp. 1085-1088
Author(s):  
Chuan Jun Zhang ◽  
Feng Lin Li
Keyword(s):  
Medicinal Plant ◽  
Extraction Time ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Ultrasound Assisted Extraction ◽  
Rhodiola Sachalinensis ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Chinese Medicinal Plant

Ultrasound-assisted extraction (UAE) of polysaccharides from the Chinese medicinal plantRhodiola sachalinensisA. BOR (PRs) was studied. The effects of four factors (extraction time, ultrasonic power, liquid-solid ratio and extraction temperature) on the extraction yield of PRs were investigated by the single-factor test, and the optimum UAE conditions were investigated by the orthogonal test. The results demonstrated that the optimum UAE conditions for PRs were as followings: extraction time of 30 min, ultrasonic power of 85 W, liquid-solid ratio of 45 ml/g, and extraction temperature of 45°C. The present data might provide a theoretic base for full utilization ofRhodiola sachalinensisA. BOR.

scholarly journals Optimization of a Microwave Assisted Extraction of Organic Sulphur from Domestic Sewage Sludge by UV-Vis Spectrophotometry Determination

2017 ◽  
Vol 5 (4) ◽  
pp. 1
Author(s):  
Darlan Ferreira Silva ◽  
Maria Olimpia Oliveira Rezende
Keyword(s):  
Hydrochloric Acid ◽  
Sewage Sludge ◽  
Factorial Design ◽  
Spectrophotometric Determination ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Organic Sulphur ◽  
Assisted Extraction

An alternative method for microwave-assisted extraction of organic sulphur in sewage sludge samples was optimized based on response surface methodology. The extraction process was defined by a 23 factorial design. In the factorial design, the temperature, the extraction time and the volume of hydrochloric acid in the solvent mixture were evaluated. The samples were extracted with a mixture of nitric acid and hydrochloric acid. The data obtained for study were based on the concentration of sulphur in the sulfate form (S-SO42-) obtained spectrophotometrically in the sludge samples. The initial extraction parameters were adjusted so that spectrophotometric determination was feasible. According to the levels (minimum and maximum) defined for each parameter, the methodology showed that the best extraction conditions were achieved with an extraction temperature of 150 °C, using a longer extraction time (40 min). This study was carried out to evaluate the efficiency of microwave-assisted extraction in spectrophotometric determination of sulphur in sludge samples.

scholarly journals Product Quality of Quercetin Extract From Carica Papaya L Flower by Microwave-Assisted Extraction (MAE)

2019 ◽  
Vol 14 (2) ◽  
pp. 139-146
Author(s):  
Iman Mukhaimin ◽  
Enggar Ayu Saraswati ◽  
Rahma Ajizah ◽  
Meilya Suzan Triyastuti
Keyword(s):  
Product Quality ◽  
Microwave Power ◽  
Carica Papaya ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Microwave Assisted Extraction ◽  
Group Function ◽  
Microwave Assisted ◽  
Assisted Extraction

These work aims are to determine the best condition extraction and product quality of quercetin from Carica papaya L flowers extract. The extraction of quercetin from Carica papaya L flowers had done by microwave-assisted extraction (MAE) method.  Dried flowers prepared by cutting into 0,125 mm of particle size. Dried flowers were extracted using methanol 80% (w/w) to determine  influence of solid to liquid, S/L, ratio (1:10, 1:15, 1:20), microwave power (120, 200, 280, 400 W), and extraction time (1-5 minutes) on extraction process. Using the phytochemical test by Mg-HCl-amyl alcohol and UV-Vis spectrophotometer techniques, the quercetin detected by qualitative and quantitative analysis. As a result, the presence of flavonoids detected by the formation of a brownish red-colored flavylium compound.  Increasing extraction time, power, and S/L ratio increased the extraction temperature. Consequently, yield quercetin decreased when the temperature extraction exceeds its temperature degradation. The highest quercetin yield, 0.214%, was detected with solid to liquid ratio (1:15), microwave power (400 Watt), and extraction time (4 minutes). FTIR spectrophotometer technique on the highest yield quercetin proved that have product quality with 91,17% similarity on group function like –OH, C=O, C=C, and C-H with quercetin standard spectrum.

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