Hot deformation behavior and dynamic recrystallization constitutive modeling of Al–Cu–Mg powder compacts processed by extrusion at elevated temperatures

Author(s):  
Katti Bharath ◽  
Asit Kumar Khanra ◽  
MJ Davidson

The deformation behavior of Al–Cu–Mg sintered preforms has been investigated by extrusion in the temperature range of 450–550°C and strain rate range of 0.1–0.3 s−1, respectively. The aim of this study is to analyze the effect of initial preform relative density on the hot deformation behavior and to model and predict the flow stress of extruded samples using constitutive equations. The true stress–strain curves exhibit three stages of deformation, which represent work hardening, dynamic recovery, and dynamic recrystallization during deformation at different temperatures, strain rates, and initial preform relative densities of 70%, 80%, and 90%, respectively. The results show that the flow stress values are influenced by initial preform relative density, deformation temperature, and strain rate. Microstructural examination of extruded specimens has been performed by optical microscopy and scanning electron microscopy. Arrhenius-type constitutive equations are developed to predict the flow stress of hot-extruded powder metallurgy processed aluminum alloy (Al–4%Cu–0.5%Mg). Zener–Hollomon parameter is used to explain the relationship between peak flow stress, temperature, and strain rate in an exponential equation containing the deformation activation energy and material constants. Subsequently, the statistical indicators correlation coefficient ( R) and the average absolute relative error are assessed to confirm the validity of constitutive equations. The results indicate the experimental and predicted peak flow stress values are in good agreement, which indicate the accuracy and reliability of the developed model for powder metallurgy processed Al–4%Cu–0.5%Mg preforms.

Processes ◽  
2021 ◽  
Vol 9 (3) ◽  
pp. 451
Author(s):  
Yexin Jiang ◽  
Xu Wang ◽  
Zhou Li ◽  
Zhu Xiao ◽  
Xiaofei Sheng ◽  
...  

The hot deformation behavior of Cu-20.0Ni-5.0Sn-0.25Zn-0.22Mn was investigated using a Gleeble-3500 thermal simulator with a temperature range from 720 °C to 880 °C and a strain rate range from 0.001 s−1 to 1 s−1. The results show that the flow stress increased with the increase of the strain rate and the decrease of the temperature. The constitutive equation of the alloy was established based on the peak flow stress. Figures of the power dissipation efficiency and flow instability with the variable of the true strain from 0.2 to 0.8 displayed the dynamic change of power dissipation efficiency and the instability area. The domain of 730–770 °C and 0.001–0.01 s−1 possessed a power dissipation efficiency over 40% throughout the whole deformation. The flow instability always appeared at a high strain rate from 0.1 s−1 to 1 s−1 during the whole deformation process. The nucleation site of the dynamic recrystallization generally appeared along the grain boundaries, indicating the discontinuous dynamic recrystallization mechanism. The appropriate conditions for deformation with a true strain of 0.9 is in a safe domain (820–860 °C with a strain rate of 0.001–0.01 s−1). There were four kinds of variation tendencies of the power dissipation efficiency with the increase of the true strain under various conditions, suggesting a changing situation for the main softening mechanisms.


Metals ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 481 ◽  
Author(s):  
Zhang ◽  
Lian ◽  
Chen ◽  
Sun ◽  
Zhang ◽  
...  

The hot deformation behavior and microstructure evolution of a 7.5 vol% TiBw/near α-Ti composite with fine matrix microstructure were investigated under the deformation conditions in a temperature range of 800–950 °C and strain rate range of 0.001–1 s−1 using plane strain compression tests. The flow stress curves show different characteristics according to the various deformation conditions. At a higher strain rate (1 s−1), the flow stress of the composite continuously increases until a peak value is reached. The activation energy is 410.40 kJ/mol, much lower than the activation energy of as-sintered or as-forged composites. The decreased activation energy is ascribed to the breaking of the TiBw reinforcement during the multi-directional forging and the resultant fine matrix microstructure. Refined reinforcement and refined matrix microstructure significantly improve the hot deformation ability of the composite. The deformation conditions determine the morphology and fraction of α and β phases. At 800–900 °C and 0.01 s−1 the matrix α grains are much refined due to the continuous dynamic recrystallization (CDRX). The processing map is constructed based on the hot deformation behavior and microstructure evolution. The optimal hot processing window is determined to be 800–950 °C/0.001–0.01 s−1, which lead to CDRX of primary α grains or dynamic recovery (DRV) and dynamic recrystallization (DRX) of β phase.


Author(s):  
H. R. Rezaei Ashtiani ◽  
H. Bisadi ◽  
M. H. Parsa

The experimental stress–strain data from isothermal hot compression tests, in a wide range of temperatures (350–500 °C) and strain rates (0.005–0.5 s−1), were employed to develop constitutive equations in a commercially pure aluminum (AA1070). The effects of temperature and strain rate on the hot deformation behavior were represented by Zener–Hollomon parameter including Arrhenius term. The results show that the hardening rate and flow stress are evidently affected by both deformation temperature and strain rate. The power law, exponential, and hyperbolic sinusoidal types of Zener–Hollomon equations were used to determine the hot deformation behavior of AA1070. The results suggested that the highest correlation coefficient was achieved for the hyperbolic sine law for the studied material. So the proposed deformation constitutive equations can give an accurate and precise estimate of the flow stress for AA1070, which means it can be used for numerical simulation of hot forming processes and for choosing proper forming parameters in engineering practice accurately.


2013 ◽  
Vol 709 ◽  
pp. 143-147 ◽  
Author(s):  
Tao Wang ◽  
Zhao Li ◽  
Shu Hong Fu ◽  
Yong Zhang ◽  
Yu Xin Zhao ◽  
...  

The hot deformation behavior of U720Li was investigated by isothermal compression tests at temperature ranging from 1060-1180°C and strain rate from 0.001s-1 to 20s-1. The flow stress-strain curves and microstructures were investigated and a constitutive equation was established. It is found that flow stress is sensitive to stain rate and deformation temperature greatly. The higher stain rate resultes in a larger fluctuation in flow stress. The hot deformation activation energy is determined to be 552.8kJ/mol. Grain size increases with increasing temperature and decreases firstly and then increases with increasing strain rate. U720Li alloy should be deformed below the solve temperature of γ primary phase with lower strain rate in order to obtain the even and fine grain size.


2013 ◽  
Vol 17 (5) ◽  
pp. 1523-1528
Author(s):  
Bao-Hua Jia ◽  
Wei-Dong Song ◽  
Hui-Ping Tang ◽  
Jian-Guo Ning

Isothermal compression tests of TC18 titanium alloy at the deformation temperatures ranging from 25?C to 800?C and strain rate ranging from 10-4 to 10-2 s-1 were conducted by using a WDW-300 electronic universal testing machine. The hot deformation behavior of TC18 was characterized based on an analysis of the true stress-true strain curves of TC18 titanium alloy. The curves show that the flow stress increases with increasing the strain rate and decreases with increasing the temperature, and the strain rate play an important role in the flow stress when increasing the temperatures. By taking the effect of strain into account, an improved constitutive relationship was proposed based on the Arrhenius equation. By comparison with the experimental results, the model prediction agreed well with the experimental data, which demonstrated the established constitutive relationship was reliable and can be used to predict the hot deformation behavior of TC18 titanium alloy.


2016 ◽  
Vol 684 ◽  
pp. 35-41 ◽  
Author(s):  
S.V. Rushchits ◽  
E.V. Aryshensky ◽  
S.M. Sosedkov ◽  
A.M. Akhmed'yanov

The deformation behavior of 1565ch alloy under the plane-strain conditions in the temperature range of 350–490 оС and strain rates range of 0,1–10 s-1 is studied. The expression for steady flow stress as the functions of temperature of deformation and strain rate is obtained. It is established that 1565ch alloy with zirconium addition shows higher strain resistance and less tendency to dynamic and static recrystallization than AMg6.


2015 ◽  
Vol 2015 ◽  
pp. 1-8 ◽  
Author(s):  
Ming-wei Guo ◽  
Zhen-hua Wang ◽  
Ze-an Zhou ◽  
Shu-hua Sun ◽  
Wan-tang Fu

316LN stainless steel with 0.08%N (08N) and 0.17%N (17N) was compressed at 1073–1473 K and 0.001–10 s−1. The hot deformation behavior was investigated using stress-strain curve analysis, processing maps, and so forth. The microstructure was analyzed through electron backscatter diffraction analysis. Under most conditions, the deformation resistance of 17N was higher than that of 08N. This difference became more pronounced at lower temperatures. The strain rate sensitivity increased with increasing temperature for types of steel. In addition, the higher the N content, the higher the strain rate sensitivity. Hot deformation activation energy increased from 487 kJ/mol to 549 kJ/mol as N concentration was increased from 0.08% to 0.17%. The critical strain for initiation of dynamic recrystallization was lowered with increasing N content. In the processing maps, both power dissipation ratio and unstable region increased with increasing N concentration. In terms of microstructure evolution, N promoted dynamic recrystallization kinetic and decreased dynamic recrystallization grain size. The grain growth rate was lower in 17N than in 08N during heat treatment. Finally, it was found that N favored twin boundary formation.


Author(s):  
Mei-ling Li ◽  
Wen-jin Gao ◽  
Ying-hao Zhou

Abstract The 60NiTi (Ni60wt%–Ti40wt%) intermetallic is a hard-to-process material. Understanding of hot deformation behavior is crucial for the hot working of 60NiTi. This work studied hot deformation behavior and corresponding microstructure of the hot isostatic pressed 60NiTi in the temperature range of 900 °C–1050 °C and at strain rates of 0.1, 0.01, and 0.001 s-1 through a hot compression test. The flow stress and microstructure were susceptible to the hot deformation parameters. The flow stress decreased with the increase in deformation temperature and decrease in strain rate. Work hardening occurred at a small strain, then followed by softening; finally, near-dynamic equilibrium was achieved between work hardening and softening. A constitutive equation was developed to describe the effects of strain rate and temperature on flow stress. Simulation of hot deformation via the finite element method revealed the workpiece’s inhomogeneous deformation. The deformation occurred mainly in the center area of the cylindrical sample, resulting in high stress and strain concentrations in this region and causing the equiaxial grains to be compressed into prolate grains. This work can provide guidance for the hot working, such as forging and hot rolling, of 60NiTi.


2011 ◽  
Vol 695 ◽  
pp. 361-364 ◽  
Author(s):  
Ying Han ◽  
Guan Jun Qiao ◽  
Dong Na Yan ◽  
De Ning Zou

The hot deformation behavior of super 13Cr martensitic stainless steel was investigated using artificial neural network (ANN). Hot compression tests were carried out at the temperature range of 950°C to 1200°C and strain rate range of 0.1–50s–1at an interval of an order of magnitude. Based on the limited experimental data, the ANN model for the constitutive relationship existed between flow stress and strain, strain rate and deformation temperature was developed by back-propagation (BP) neural network method. A three layer structured network with one hidden layer and ten hidden neurons was trained and the normalization method was employed in training for avoiding over fitting. Modeling results show that the developed ANN model can efficiently predict the flow stress of the steel and reflect the hot deformation behavior in the whole deforming process.


Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 920 ◽  
Author(s):  
Zhihao Yao ◽  
Hongying Wang ◽  
Jianxin Dong ◽  
Jinglin Wang ◽  
He Jiang ◽  
...  

The hot deformation behavior of an advanced nickel-based Haynes282 superalloy was systematically investigated employing isothermal compression tests in the sub-solvus and super-solvus temperature with various strain rates. The influence of deformation temperature and strain rate on the microstructure was studied by transmission electron microscope. The results reveal that the interaction between work hardening and dynamic softening did not reach equilibrium under lower deformation temperature and higher strain rate. The active energy of alloy is around 537.12 kJ/mol and its hot deformation constitutive relationship equation was expressed. According to the processing map and microstructure observations, two unsafe flow instability domains should be avoided. The optimum hot processing condition for homogeneous and fine dynamic recrystallization grains are obtained. TEM micrograph observations indicated that deformation temperature and strain rate affected recrystallization by affecting the evolution of dislocation substructures within the alloy. The nucleation and growth of DRX grains can be promoted by the relatively high deformation temperature and low strain rate. The main mechanism of dynamic recrystallization nucleation preferred to discontinuous dynamic recrystallization and the typical feature of discontinuous dynamic recrystallization showed grain boundary migration nucleation. The findings improve the understanding of hot deformation behavior and dislocation substructures evolution of the superalloy, which benefits the accurate control of microstructures of nickel-based superalloys, and tailors the properties of final components used in the land-based gas turbine.


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