scholarly journals Degradation, Fatigue, and Failure of Resin Dental Composite Materials

2008 ◽  
Vol 87 (8) ◽  
pp. 710-719 ◽  
Author(s):  
J.L. Drummond
Keyword(s):  
Composite Materials ◽  
Cyclic Loading ◽  
Material Selection ◽  
Resin Composite ◽  
Dental Composite ◽  
Resin Matrix ◽  
Dental Resin ◽  
3D Tomography ◽  
Time Period ◽  
Cause Of Failure

The intent of this article is to review the numerous factors that affect the mechanical properties of particle- or fiber-filler-containing indirect dental resin composite materials. The focus will be on the effects of degradation due to aging in different media, mainly water and water and ethanol, cyclic loading, and mixed-mode loading on flexure strength and fracture toughness. Several selected papers will be examined in detail with respect to mixed and cyclic loading, and 3D tomography with multi-axial compression specimens. The main cause of failure, for most dental resin composites, is the breakdown of the resin matrix and/or the interface between the filler and the resin matrix. In clinical studies, it appears that failure in the first 5 years is a restoration issue (technique or material selection); after that time period, failure most often results from secondary decay.

scholarly journals Improved performance of Bis-GMA dental composites reinforced with surface-modified PAN nanofibers

2021 ◽  
Vol 32 (7) ◽  
Author(s):  
Parisa Amiri ◽  
Zahra Talebi ◽  
Dariush Semnani ◽  
Rouhollah Bagheri ◽  
Hossein Fashandi
Keyword(s):  
Network Formation ◽  
Resin Composite ◽  
Flexural Modulus ◽  
Weight Ratio ◽  
Dental Composite ◽  
Dental Composites ◽  
Resin Matrix ◽  
Dental Resin ◽  
Polymerization Shrinkage ◽  
Surface Modified

AbstractIn the present work, polyacrylonitrile (PAN) nanofibers reinforced dental composites were investigated to achieve the improved interfacial adhesion between the PAN nanofiber and resin matrix using surface modification of nanofibers. PAN nanofibers mat were prepared by electrospinning and then, surface treated with the activated bisphenol A glycidyl methacrylate (Bis-GMA)/triethyleneglycol dimethacrylate (TEGDMA) (50/50 mass ratio) dental resin followed by photo-curing. Also, the treated nanofibers mat was milled into a powder to achieve the uniform distribution of nanofibers in the matrix resin. The reinforced dental composite were prepared by mixing the various mass fraction of the powder (0.5–15 wt%) with the Bis-GMA/TEGDMA dental monomers. The effect of weight ratio of surface-modified nanofibers to blend resin on the chemical structure, morphology, compression and flexural properties, color and polymerization shrinkage of dental composites was evaluated. The results showed that using surface-treated nanofibers with content of 5 wt% enhanced the compression strength, flexural strength, flexural modulus and work of rupture of the resultant dental composite by factors of 23%, 7%, 80%, and 145%, respectively, comparing to the unreinforced neat resin. Also, the polymerization shrinkage reduces by 37%. These significant improved properties of the dental composite could be due to the semi-interpenetration network formation between surface-modified nanofibers and resin matrix and well distribution of nanofibers in the dental resin. Further increasing the nanofiber content led to poor mechanical properties of obtained dental composites. The results also, revealed that the color of resin composite could be whiter using modified PAN nanofibers as the filler.

scholarly journals THE EFFECT OF COCONUT COIR FIBER POWDER CONTENT AND HARDENER WEIGHT FRACTIONS ON MECHANICAL PROPERTIES OF AN EPR-174 EPOXY RESIN COMPOSITE

SINERGI ◽  
2021 ◽  
Vol 25 (3) ◽  
pp. 361
Author(s):  
Muhamad Fitri ◽  
Shahruddin Mahzan ◽  
Imam Hidayat ◽  
Nurato Nurato
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Composite Materials ◽  
Impact Strength ◽  
Epoxy Resin ◽  
Resin Composite ◽  
Weight Fraction ◽  
Resin Matrix ◽  
Powder Content ◽  
Made In

The development of composite materials is increasingly widespread, which require superior mechanical properties. From many studies, it is found that the mechanical properties of composite materials are influenced by various factors, including the reinforcement content, both in the form of fibers and particle powder. However, those studies have not investigated the effect of the hardener weight fraction on the mechanical properties of resin composite materials. Even though its function as a hardener is likely to affect its mechanical properties, it might obtain the optimum composition of the reinforcing content and hardener fraction to get the specific mechanical properties. This study examines the effect of hardener weight fraction combined with fiber powder content on mechanical properties of EPR-174 epoxy resin matrix composite and determines the optimum of Them. The research was conducted by testing a sample of composite matrix resin material reinforced with coconut fiber powder. The Powder content was made in 3 levels, i.e.: 6%, 8%, and 10%. While the hardener fraction of resin was made in 3 levels, i.e.: 0.4, 0.5, and 0.6. The test results showed that pure resin had the lowest impact strength of 1.37 kJ/m2. The specimen with a fiber powder content of 6% has the highest impact strength i.e.: 4.92 kJ/m2. The hardener fraction of 0.5 has the highest impact strength i.e.: 4.55 kJ/m2. The fiber powder content of 8% produced the highest shear strength i.e.: 1.00 MPa. Meanwhile, the hardener fraction of 0.6 has the highest shear strength i.e.: 2.03 MPa.

Time-dependent nanoindentation behavior of high elastic modulus dental resin composites

2010 ◽  
Vol 25 (3) ◽  
pp. 529-536 ◽  
Author(s):  
Yijun Wang ◽  
Isabel K. Lloyd
Keyword(s):  
Elastic Modulus ◽  
Volume Fraction ◽  
Resin Composite ◽  
Acrylic Resin ◽  
Resin Matrix ◽  
Resin Composites ◽  
Dental Resin ◽  
Elastic Plastic ◽  
High Elastic Modulus ◽  
Continuous Stiffness Measurement

Nanoindentation and the viscous-elastic–plastic (VEP) model developed by Oyen and Cook for lightly filled thermoplastic polymer composites were used to characterize the elastic modulus, hardness, and viscoelastic response of a new high elastic modulus dental resin composite. The VEP model was used because loading rate studies indicated a viscous component in the loading/unloading response of our highly filled, thermosetting acrylic resin composites. Increasing the volume fraction of our high modulus filler increased the elastic modulus and hardness and decreased the viscous response in our composites. Coupling the filler and resin matrix with a commercial coupling agent like Metaltite or MPTMS (3-methacryloxypropyltrimethoxysilane) that ionically bonds to the filler and covalently bonds to the matrix decreases the viscous response and increases the hardness of the composite. The coupling agents did not affect the elastic modulus. The ability of the VEP model to predict load–displacement trajectories and the correlation of the elastic modulus and hardness values determined from the VEP model with those from the direct continuous stiffness measurement mode nanoindentation measurements indicate that the VEP model can be extended to highly filled, thermosetting systems. This is valuable since the potential to predict elastic, plastic, and viscous contributions to behavior should be valuable in the design and understanding of future highly filled resin composite systems.

Fiber Reinforced Epoxy Resin Composite Materials Using Carboxylate-Alumoxanes as Cross-Linking Agents

1999 ◽  
Vol 581 ◽  
Author(s):  
Cullen T. Vogelson ◽  
Yoshihiro Koide ◽  
Andrew R. Barrona
Keyword(s):  
Composite Materials ◽  
Resin Composite ◽  
Diglycidyl Ether ◽  
Alumina Nanoparticles ◽  
Resin Matrix ◽  
Hybrid Resin ◽  
Organic Hybrid ◽  
New Class ◽  
Epoxy Resin Composite ◽  
Ceramic Fillers

ABSTRACTChemically functionalized alumina nanoparticles (carboxylate-alumoxanes) are used as the inorganic component of a new class of inorganic-organic hybrid materials. Lysine- or para- hydroxybenzoic acid-derivatized alumoxanes are readily prepared from the reaction of boehmite, [Al(O)(OH)]n, with the appropriate carboxylic acid. The peripheral organic hydroxides and amines of these carboxylate-alumoxanes either react directly with epoxide resins, such as the diglycidyl ether of bisphenol-A (DER 332), to form a hybrid material, or in the presence of an organic resin and hardener system to form a composite material. SEM and AFM show a uniform distribution of alumina nanoparticles within the resin matrix. The properties and cure times of the alumoxane hybrid and composite materials are distinct from both the pure resins and from a physical blend of the resins with traditional ceramic fillers. A significant increase in thermal stability and tensile strength is observed for both the hybrid and composite resin systems. In addition, both carbon fiber and carbon/Kevlar® matting have been successfully incorporated into the hybrid resin systems resulting in further property improvements.

Simulated Body Fluid Sorption and Solubility of Silica Reinforced Dental Resin Composites

2013 ◽  
Vol 795 ◽  
pp. 626-630 ◽  
Author(s):  
Saad Omar Alsharif ◽  
Md Akil Hazizan ◽  
Nasser Abbas Abd El-Aziz ◽  
Zainal Arifin Ahmad
Keyword(s):  
Simulated Body Fluid ◽  
Body Fluid ◽  
Resin Composite ◽  
Triethylene Glycol ◽  
Filler Loading ◽  
Resin Matrix ◽  
Resin Composites ◽  
Dental Resin ◽  
Triethylene Glycol Dimethacrylate ◽  
Dental Resin Composites

The aim of this study is to investigate the effect of filler loading on the sorption and solubility of Simulated Body Fluid (SBF) of self-prepared micro dental resin composites. The prepared resin composite was based on silica (SiO2) particles and bisphenol-a-glycidyl methacrylate (Bis-GMA) as a base monomer and triethylene glycol dimethacrylate (TEGDMA) as a co-monomer. The filler was mixed with monomers, in proportions of 40, 50 and 60 wt.%. A resin matrix containing 0 wt.% filler was used as the control composition to evaluate the effect of filler loading on the sorption and solubility of SBF. The experimental methods were based on the procedure mentioned in the ISO 4049 (2009) standard for dentistry-Polymer-based restorative Materials. The sorption and solubility of resin matrix/SiO2composite decreased gradually as the filler loading increased. The increase of filler loading showed significant differences in the sorption and solubility as tested by ANOVA (P= 0.000).

Effect of cyclic loading and environmental aging on the fracture toughness of dental resin composite

2006 ◽  
Vol 80B (1) ◽  
pp. 226-235 ◽  
Author(s):  
Viswanath Ravindranath ◽  
Michael Gosz ◽  
Eduardo De Santiago ◽  
James L. Drummond ◽  
Sheldon Mostovoy
Keyword(s):  
Fracture Toughness ◽  
Cyclic Loading ◽  
Resin Composite ◽  
Dental Resin ◽  
Environmental Aging

Effect of Cyclic Loading on the Bond Strength of Class II Restorations with Different Composite Materials

10.2341/07-65 ◽  
2008 ◽  
Vol 33 (2) ◽  
pp. 163-168 ◽  
Author(s):  
A. N. Cavalcanti ◽  
F. H. O. Mitsui ◽  
F. Silva ◽  
A. R. Peris ◽  
A. Bedran-Russo ◽  
...  
Keyword(s):  
Composite Materials ◽  
Cyclic Loading ◽  
Bond Strength ◽  
Clinical Relevance ◽  
Resin Composite ◽  
Clinical Situation ◽  
Class Ii ◽  
Selection Of

Clinical Relevance New resin composite technologies, such as nano-filled-based systems, have been developed. The assessment of such materials in a simulated laboratory chewing condition may assist with the selection of composites in a clinical situation.

scholarly journals Elution of Monomers from Provisional Composite Materials

2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Simon Daniel Schulz ◽  
Tobias Laquai ◽  
Klaus Kümmerer ◽  
Richard Bolek ◽  
Volker Mersch-Sundermann ◽  
...  
Keyword(s):  
Composite Materials ◽  
Storage Time ◽  
Resin Composite ◽  
Storage Media ◽  
High Release ◽  
Time Period ◽  
Materials Used ◽  
By Products

The aim of this study was to evaluate the elution of substances from different materials used for the manufacturing of temporary indirect restorations, after storage in saliva and ethanol 75%. 10 samples of three chemically cured materials (Protemp 3 Garant, Systemp.c&b, and Trim) and one light-cured material (Clip F) were stored in saliva and ethanol 75% for 24 h, 7, and days 28 days. From the storage media at each time period, samples were prepared and analysed by LC-MS/MS, in order to access the elution of monomers. The results differed among the materials (P≤ 0.05). No monomers were detected in the samples of Protemp 3 Garant and Clip F. Substances were detected only in ethanol samples of Systemp.c&b and Trim. The amount of BisGMA, TEGDMA, and UDMA 2 released from Systemp.c&b was higher compared to Trim. Storage time affected the release of substances (P≤ 0.05). The highest release was observed within the first 24 h. It can be concluded that provisional resin composite materials do not show high release of monomers and this release is material dependent. However, the detection of additional peaks during the analysis, suggesting the formation of by-products of the eluted substances, may not be in favour of these materials with respect to their toxicity.

SEM/EDX and FTIR Characterization of a Dental Resin Cement with Antibacterial Agents Incorporated

2005 ◽  
Vol 284-286 ◽  
pp. 391-394
Author(s):  
Emílio Akaki ◽  
Herman S. Mansur ◽  
Lúcia H. Angelis ◽  
Barbara A. Castro ◽  
Henrique F. Valadão ◽  
...  
Keyword(s):  
Antibacterial Agents ◽  
Resin Composite ◽  
Resin Cement ◽  
Dental Composite ◽  
Inorganic Filler ◽  
Dental Resin ◽  
Posterior Teeth ◽  
Ftir Characterization ◽  
The Aesthetic ◽  
Ceramic Restorations

The demand from patients for aesthetic in posterior teeth restoration has been increasing in recent years. As an alternative to metal alloy restorations used in posterior tooth, aesthetical materials such as ceramics have been more often utilized. Resin cement, a derivative from dental composite, based on the combination of bis-GMA and inorganic filler is used to fixate these ceramic restorations to posterior teeth. Similar to resin composite, incorporated antibacterial agents to resin cement can be an effective way to increase the aesthetic restoration durability. Resin cements C&B® (Bisco) and Fill Magic Dual Cement® (Vigodent) were used in the present study. For experimental resin cement, Triclosan was incorporated to the base cement paste. Samples were investigated by Scanning Electron Microscopy coupled to EDX microprobe (SEM/EDX) and FTIR spectroscopy. The results have demonstrated that the incorporation of antibacterial agents to resin cement is possible through the developed procedure.

scholarly journals Prevention of Periodontitis by the Addition of a Bactericidal Particulate Glass/Glass-Ceramic to a Dental Resin: A Pilot Study in Dogs

Coatings ◽  
2018 ◽  
Vol 8 (8) ◽  
pp. 259 ◽  
Author(s):  
Roberto López-Píriz ◽  
Luis Díaz ◽  
Belén Cabal ◽  
Adolfo Fernández ◽  
Marta Suárez ◽  
...  
Keyword(s):  
Bone Loss ◽  
Glass Ceramic ◽  
Resin Composite ◽  
Antimicrobial Properties ◽  
Negative Control ◽  
Resin Matrix ◽  
Dental Resin ◽  
Prevention Of Bone Loss

The aim of the study is to evaluate, in a ligature-induced periodontitis model, the efficacy of a commercially available dental resin containing different antimicrobial glass/glass-ceramic additions (0–26 wt.%). It has been proved that a 26 wt.% glass addition to a conventional dental resin matrix does not alter neither its workability nor its adhesion to the surface of teeth; however, it does confer notable antimicrobial properties when tested in vitro. Moreover, in vivo tests in Beagle dogs demonstrated the prevention of bone loss in ligature-induced plaque accumulation around teeth. Particularly, the glass-ceramic filler resin composite has shown excellent antimicrobial control since it displays the same bone loss as that of the negative control. The results obtained in the present investigation have shown that a conventional dental resin containing a fraction of glass/glass-ceramic (≥26 wt.%) can prevent periodontitis, which is considered to be a most serious dental disease.

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