Mechanical behaviour of powders using a medium pressure flexible boundary cubical triaxial tester

Author(s):  
F Li ◽  
V M Puri

A medium pressure (<21 MPa) flexible boundary cubical triaxial tester was designed to measure the true three-dimensional response of powders. In this study, compression behaviour and strength of a microcrystalline cellulose powder (Avicel® PH102), a spray-dried alumina powder (A16SG), and a fluid-bed-granulated silicon nitride based powder (KY3500) were measured. To characterize the mechanical behaviour, three types of triaxial stress paths, that is, the hydrostatic triaxial compression (HTC), the conventional triaxial compression (CTC), and the constant mean pressure triaxial compression (CMPTC) tests were performed. The HTC test measured the volumetric response of the test powders under isostatic pressure from 0 to 13.79MPa, during which the three powders underwent a maximum volumetric strain of 40.8 per cent for Avicel® PH102, 30.5 per cent for A16SG, and 33.0 per cent for KY3500. The bulk modulus values increased 6.4-fold from 57 to 367MPa for Avicel® PH102, 3.7-fold from 174 to 637 MPa for A16SG, and 8.1-fold from 74 to 597MPa for KY3500, when the isotropic stress increased from 0.69 to 13.79 MPa. The CTC and CMPTC tests measured the shear response of the three powders. From 0.035 to 3.45MPa confining pressure, the shear modulus increased 28.7-fold from 1.6 to 45.9MPa for Avicel® PH102, 35-fold from 1.7 to 60.5MPa for A16SG, and 28.5-fold from 1.5 to 42.8MPa for KY3500. In addition, the failure stresses of the three powders increased from 0.129 to 4.41 MPa for Avicel® PH102, 0.082 to 3.62 MPa for A16SG, and 0.090 to 4.66MPa for KY3500, respectively, when consolidation pressure increased from 0.035 to 3.45MPa. In addition, the shear modulus and failure stress values determined from the CTC test at 2.07, 2.76, and 3.45MPa confining pressures are consistently greater than those from the CMPTC test at the same constant mean pressures. This observation demonstrates the influence of stress paths on material properties. The CTT is a useful tool for characterizing the three-dimensional response of powders and powder mixtures.

Energies ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 5065
Author(s):  
Liming Zhang ◽  
Shengqun Jiang ◽  
Jin Yu

Failure tests on sandstone specimens were conducted under different confining pressures and seepage pressures by using an MTS triaxial rock testing machine to elucidate the corresponding correlations of permeability and characteristic stress with confining pressure and pore pressure during deformation. The results indicate that permeability first decreases and presents two trends, i.e., a V-shaped increase and an S-shaped trend during the non-linear deformation stage. The greater the seepage pressure, the greater the initial permeability and the more obvious the V-shaped trend in the permeability. As the confining pressure was increased, the trend in the permeability gradually changed from V- to S-shaped. Compared with the case at a high confining pressure, the decrease of permeability occurred more quickly, the rate of change becomes greater, and the sudden increase observed in the permeability happened earlier under lower confining pressures. Within the range tested, confining pressure exerted a greater effect on the permeability than the seepage pressure. In comparison with the axial strain, volumetric strain better reflected changes in permeability during compaction and dilation of sandstone. The ratio of crack initiation stress to peak strength ranged from 0.37 to 0.50, while the ratio of dilation stress to peak strength changed from 0.58 to 0.72. Permeabilities calculated based on Darcy and non-Darcy flow changed within the same interval, while the change in permeability was different.


Geofluids ◽  
2019 ◽  
Vol 2019 ◽  
pp. 1-14
Author(s):  
Lu Shi ◽  
Zhijiao Zeng ◽  
Zhiming Fang ◽  
Xiaochun Li

Injecting CO2 into a reservoir disturbs the geostress field, which leads to variations in the permeability of caprock and affects its sealing performance. In this paper, the evolution characteristics of the permeability of Yingcheng mudstone were experimentally studied during deviatoric compression under different confining pressures. As the confining pressure increased, the strength of the mudstone increased bilinearly, the angle between the fault and the maximum principle stress increased, and the fault became flatter. During compression, the permeability of mudstone first decreased and then increased and the turning point of the permeability was between the onset of dilatancy and the turning point of volumetric strain; when the fault formed, the permeability increased sharply and the fault-induced increment was reduced exponentially with increasing confining pressure. In addition, the mudstone transformed to the ductile failure mode when the effective confining pressure was greater than 35 MPa, which means that the permeability did not jump within a small strain. Finally, a practical strain-based model of permeability evolution that separately considers compaction and dilatancy was proposed, and the predicted permeability values were in good agreement with the experimental results. This study revealed the effect of confining pressure on permeability evolution during compression and can help evaluate the sealing ability of mudstone caprock.


2019 ◽  
Vol 56 (7) ◽  
pp. 983-991
Author(s):  
Hua Yu ◽  
Kam Ng ◽  
Dario Grana ◽  
John Kaszuba ◽  
Vladimir Alvarado ◽  
...  

The presence of compliant pores in rocks is important for understanding the stress–strain behaviors under different stress conditions. This paper describes findings on the effect of compliant pores on the mechanical behavior of a reservoir sandstone under hydrostatic and triaxial compression. Laboratory experiments were conducted at reservoir temperature on Weber Sandstone samples from the Rock Springs Uplift, Wyoming. Each experiment was conducted at three sequential stages: (stage 1) increase in the confining pressure while maintaining the pore pressure, (stage 2) increase in the pore pressure while maintaining the confining pressure, and (stage 3) application of the deviatoric load to failure. The nonlinear pore pressure – volumetric strain relationship governed by compliant pores under low confining pressure changes to a linear behavior governed by stiff pores under higher confining pressure. The estimated compressibilities of the matrix material in sandstone samples are close to the typical compressibility of quartz. Because of the change in pore structures during stage 1 and stage 2 loadings, the estimated bulk compressibilities of the sandstone sample under the lowest confining pressure decrease with increasing differential pressure. The increase in crack initiation stress is limited with increasing differential pressure because of similar total crack length governed by initial compliant porosity in sandstone samples.


2020 ◽  
Vol 2020 ◽  
pp. 1-12
Author(s):  
Jinlong Cai ◽  
Wei Zou

A conventional triaxial compression test of Jurassic-Cretaceous typical weakly consolidated sandstone from a mining area in Ordos, China, was conducted using an MTS816 tester. Results showed that, before the peak, the rock had a distinct yield stage. When the specimen reached its peak strength, the strength decreased rapidly and showed an obvious brittle failure. When the confining pressure was increased to 15 MPa, the decrease of strength was slow and the rock tended toward ductile failure. With the increase of confining pressure, the cyclic strain initially increased slightly, whereas the volumetric strain increased greatly and the rock sample was in a compression state. When the load reached a critical value, the curve was reversely bent, resulting in volume expansion, whereas the peak strength, residual strength, and elastic modulus increased with confining pressure, and Poisson’s ratio decreased with the confining pressure. In the model based on macroscopic failure rock, the expression of the relationship between fracture angle and confining pressure provided a solid theoretical basis for the direction and failure mode of the macroscopic crack. Based on the rock strength theory and Weibull random distribution assumption of rock element strength, the damage variable correction coefficient was introduced when the residual strength was considered. Then, the mathematical expression of the 3D damage statistical constitutive model was established. Finally, the theoretical curve of the established constitutive model was compared with the triaxial test curve, which showed a high degree of coincidence.


2011 ◽  
Vol 243-249 ◽  
pp. 2885-2888
Author(s):  
Xian Min Han ◽  
Shou Ding Li

Experiments of unloading confining pressure of rock were conducted to reveal deformation characteristics of rock mass under different excavation intension in thigh geostress condition. It were concluded from tests that volumetric strain of rock is inverse proportional to unloading rate. The smaller the unloading rate, the bigger the ductility of rock. Energy release are bigger under high unloading rate than that under low unloading rate. That means that tendency of rock burst turn smaller when unloading rates decrease.


1973 ◽  
Vol 12 (66) ◽  
pp. 469-481 ◽  
Author(s):  
Bernard D. Alkire ◽  
Orlando B. Andersland

Cylindrical samples containing 0.59 mm to 0.84 mm diameter silica sand at about 97% and 55% ice saturation (the ratio of ice volume to sand pore volume) were tested at a temperature of −12° C in triaxial compression. Both constant axial strain-rate tests and step-stress creep tests provide information on the influence of confining pressure on the shear strength and creep behavior of the sand–ice material. Changes in the degree of ice saturation help show the influence of the ice matrix versus the sand material on the mechanical behavior. Data are discussed in terms of the Mohr–Coulomb failure law and creep theories. It is shown that the cohesive component of strength depends on response of the ice matrix, whereas the frictional component of strength responds in a manner very similar to unfrozen sand tested at high confining pressures. Experimental data show that creep rates decrease exponentially and creep strength increases with an increase in confining pressure.


1994 ◽  
Vol 40 (135) ◽  
pp. 305-318 ◽  
Author(s):  
M.A. Rist ◽  
S.A.F Murrell

AbstractAn experimental investigation into the mechanical behaviour of polycrystalline ice in triaxial compression has been conducted using conditions generally favourable to brittle fracture and microcracking. Under triaxial stresses at high strain rate, ice failure occurs by abrupt shear fracturing, generally inclined at about 45° to the maximum principal stress. At −20°C, such failure is suppressed by the imposition of a small confining pressure, allowing a transition to ductile-type flow accompanied by distributed microcracking, but at —40°C shear fracture persists under confinement of up to at least 50 MPa. For low confining pressures (< 10 MPa), brittle strength is strongly pressure-dependent; above this it is pressure-independent. Evidence is presented that suggests this may reflect a change from a fracture process influenced by friction to fracture initiated by localized yielding. Ductile yield strength is found to be little influenced by confining pressure despite the inhibition of cracking that leads to greatly contrasting observed crack densities. Flow conforms to the well-known power law for ice withQ= 69 J mol−1andn= 4.2 over the temperature range −20° to −4-5° C Under these conditions, microcracking in ice appears to remain remarkably stable and non-interacting.


2021 ◽  
Vol 60 (1) ◽  
pp. 846-852
Author(s):  
Yang Yan-Shuang ◽  
Li Kai-Yue ◽  
Zhou Hui ◽  
Tian Hao-Yuan ◽  
Cheng Wei ◽  
...  

Abstract Computed tomography (CT) scanning technology is helpful in investigating rock materials as it can demonstrate the micro structure of rock clearly. Conventional triaxial compression tests and the corresponding graded triaxial loading tests were carried out to investigate the complex failure mechanism of the marble at the Jinping Hydropower Station. After that CT-scanning tests were done on the loaded marble specimens. The test results show that (1) the CT numbers of the specimens have a certain statistical regularity, that is, the CT numbers of the specimens under different confining pressures satisfy the Weibull distribution, as the confining pressure increases, the mean values rise while variances decrease; (2) in the two groups of tests, the average CT numbers corresponding to the conventional triaxial tests are higher than those corresponding to the graded loading tests, but the CT number variances are lower than those of the graded loading tests; and (3) according to meso-damage mechanics, the damage variables of the rock specimens were established based on the definition of CT numbers. The calculation results show that the damage variables decrease with the increase in confining pressure, the damage variables of the rock specimens in the graded loading tests are higher than those in the conventional triaxial test, and the differences between the two loading tests have grown with the increase in confining pressure.


2020 ◽  
Vol 2020 ◽  
pp. 1-14
Author(s):  
Yali Xu ◽  
Panpan Guo

This paper presents an investigation into the evolution law of the structural effects of Xi’an loess soil, based on the disturbed state concept. First, a series of consolidated and drained triaxial compression tests were performed on undisturbed and remoulded loess samples prepared at five different moisture contents and tested at four different confining pressures. Second, two disturbance functions with different parameters were proposed to quantify mathematically the structural effects of loess. Finally, the proposed disturbance functions were validated against documented test results by other researchers. The results indicated that the single-parameter disturbance function, with the deformation modulus as its parameter, provides convenience for application but takes no account of the respective contributions of deviatoric stress and mean stress to the disturbance evolution behavior of loess. The double-parameter disturbance function, with the shear and bulk moduli as its parameters, is capable of distinguishing these respective contributions and reflects well the disturbance evolution behavior of loess under various moisture contents and confining pressures. The effects of moisture content and confining pressure on the parameters of the disturbance functions were found to be unsteady. The proposed disturbance functions lay the foundation for establishing a constitutive model for loess accounting for the structural effect.


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