scholarly journals A comparative study of biaxial flexural strength and Vickers microhardness of different zirconia materials: Effect of glazing and thermal cycling

2015 ◽  
Vol 18 (2) ◽  
pp. 19 ◽  
Author(s):  
Esra Salihoglu Yener ◽  
Mutlu Ozcan ◽  
Ender Kazazoglu
Keyword(s):  
Flexural Strength ◽  
Thermal Cycling ◽  
Vickers Hardness ◽  
Vickers Microhardness ◽  
Testing Machine ◽  
Clinical Importance ◽  
Zirconia Ceramics ◽  
Biaxial Flexural Strength ◽  
Monolithic Zirconia ◽  
One Way Anova

<p class="western" lang="en-GB" align="left"><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>Objective:</strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">This study evaluated the effect of glazing and thermal cycling on biaxial flexural strength and Vickers hardness of different zirconia core materials. </span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>Material and </strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>Methods: </strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">Disc shaped zirconia specimens (15 mm x </span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">1.15 mm</span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">) were fabricated out of three systems (ZirkonZahn, Cercon, </span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">Ceramill</span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">) according to each manufacturer`s instructions. The specimens of each system were randomly divided into initially 2 groups. While half of the specimens were glazed, the other half was left unglazed. Each group was further divided into 4 subgroups to be subjected to thermal cycling (0-control, 1000, 3000, 5000 cycles, 5-55 ºC). Biaxial flexural strength was tested in a universal testing machine (1 mm/min). Another set of unglazed zirconia specimens were made and tested for Vickers microhardness with and without thermocycling (0-control, 1000, 3000, 5000 cycles, 5-55 ºC). Data were statistically analyzed using one-way ANOVA, two-way ANOVA and Tukey’s test (</span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">p &lt;</span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"> 0.05). </span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>Results:</strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"> In non-aged conditions (11034-1388 MPa), glazing significantly decreased the biaxial flexural strength of all zirconia ceramics (845.65-897.35 MPa) (p = 0.000). While in the non-glazed groups, all thermal cycling regimens significantly decreased the biaxial flexural strength (864-1156 MPa) (p=0.000), in glazed groups thermal cycling did not affect the results (829.4-854.9 MPa) (p = 0.405). Compared to the non-aged group (1414.1 VHN), thermal cycling decreased the Vickers hardness significantly only for Cercon (1365.9 VHN) (p = 0.005). </span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>Conclusion:</strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"> Glazing decreased the biaxial flexural strength of the zirconia ceramics tested. Unglazed zirconia ceramics were weaker against thermal cycling compared to glazed ones. For monolithic zirconia restorations, this information may have clinical importance.</span></span></p><p class="western" align="justify"><span style="font-family: 'Times New Roman', serif;"><span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>K</strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB"><strong>eywords:</strong></span></span><span style="font-family: Arial, sans-serif;"><span lang="en-GB">Biaxial flexural strength; Glazing; Thermal cycling; Vickers microhardness; Zirconia.</span></span></span></span></p>

scholarly journals Effect of the Degree of Conversion on Mechanical Properties and Monomer Elution from Self-, Dual- and Light-Cured Core Composites

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5642
Author(s):  
Branislava Petronijevic Sarcev ◽  
Sebastian Balos ◽  
Dubravka Markovic ◽  
Ivan Sarcev ◽  
Marija Vukcevic ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Vickers Hardness ◽  
Modulus Of Elasticity ◽  
Testing Machine ◽  
Degree Of Conversion ◽  
Clinical Use ◽  
Universal Testing ◽  
Post Test ◽  
One Way Anova

The objective of this work was to measure and correlate the degree of conversion (DC), mechanical properties and monomer elution from self-, dual- and light-cured core composites. Five samples of each of the following materials were prepared for each test: Clearfil (Core, Photo Core, Automix), Bisco (Core-Flo, Light-Core and Bis-Core). DC was determined using FTIR, compressive and flexural strength and modulus of elasticity using a universal testing machine and microhardness using Vickers hardness. Elution was measured using HPLC. One-way ANOVA with Tukey’s post-test and Pearson’s correlation were used to statistically analyze the data. DC of Clearfil-Dual (70.1%) and Clerafil-Photo (66.8%) were higher than Clearfil-Self (55.4%) and all Bisco materials (51.4–55.3%). Flexural strength of Clearfilwas higher than that of Bisco composites. The Microhardness of Clearfil-Dual (119.8VHN) and Clearfil-Photo (118.0VHN) were higher compared to other materials. The greatest elution was detected from self-cured materials. DC positively correlated to microhardness and compressive/flexural strength and negatively to BisGMA elution. Clearfil-Photo and Automix showed higher conversion, lower monomer elution and, generally, better mechanical properties. Self-cured composites should not be recommended for routine clinical use as their performance was inferior to dual- and light-cured composites. Microhardness may be used as an indicator of elution.

scholarly journals Effects of Different Air Particle Abrasion Protocols on the Biaxial Flexural Strength and Fractography of High/Ultra-Translucent Zirconia

Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 244
Author(s):  
Reem AlMutairi ◽  
Hend AlNahedh ◽  
Ahmed Maawadh ◽  
Ahmed Elhejazi
Keyword(s):  
Standard Deviation ◽  
Flexural Strength ◽  
Control Sample ◽  
Zirconia Ceramic ◽  
Air Abrasion ◽  
Zirconia Ceramics ◽  
Biaxial Flexural Strength ◽  
Monolithic Zirconia ◽  
The Mean ◽  
Post Hoc

In this study, the biaxial flexural strength (BFS) and fractography of high/ultra-translucent monolithic zirconia ceramics subjected to different mechanical surface pretreatments were evaluated. A total of 108 disc-shaped samples (12 mm diameter, 1.2 mm thickness) of three zirconia materials (5Y-ZP KATANA Zirconia UTML (ML), 3Y-TZP DD Bio ZX2 (DB), and 5Y-ZP DD cube X2 (DC)) were used. The BFS was investigated after subjecting the samples to surface treatment using air abrasion particles of two types (aluminum oxide or glass microbeads). The data were analyzed using two-way analysis of variance, followed by Scheffe’s post hoc test for multiple comparisons. The mean ± standard deviation BFS for DB was highest after treatment with 50 µm Al2O3 (1626.05 ± 31.9 MPa), with lower values being observed following treatment with 50 µm glass microbeads (1399.53 ± 24.2 MPa) and in the control sample (1198.51 ± 21.1 MPa). The mean ± standard deviation (SD) BFSs for DC and ML were the highest in the control groups. Surface air abrasion with 50 µm Al2O3 particles and 2 bar pressure is recommended for 3Y-TZP translucent zirconia, while no abrasion of 5Y-ZP translucent zirconia ceramic.

scholarly journals Biaxial Flexural Strength of Different Monolithic Zirconia upon Post-Sintering Processes

2022 ◽  
Author(s):  
Niwut Juntavee ◽  
Apa Juntavee ◽  
Thipradi Phattharasophachai
Keyword(s):  
Flexural Strength ◽  
Testing Machine ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Heat Treated ◽  
Biaxial Flexural Strength ◽  
Monolithic Zirconia ◽  
Treatment Procedures ◽  
Post Hoc ◽  
Sintering Processes

Abstract Objective Different post-sintering processes are expected to be a reason for alteration in the strength of zirconia. This study evaluated the effect of post-sintering processes on the flexural strength of different types of monolithic zirconia. Materials and Methods A total of 120 classical- (Cz) and high-translucent (Hz) monolithic zirconia discs (1.2 mm thickness and 14 mm in Ø) were prepared, sintered, and randomly divided into four groups to be surface-treated with (1) as-glazed (AG); (2) finished and polished (FP); (3) finished, polished, and overglazed (FPOG); and (4) finished, polished, and heat-treated (FPHT) technique (n = 15). Biaxial flexural strength (σ) was determined on a piston-on-three ball in a universal testing machine at a speed of 0.5 mm/min. Statistical Analysis Analysis of variance, and post hoc Bonferroni multiple comparisons were determined for significant differences (α = 0.05). Weibull analysis was applied for survival probability, Weibull modulus (m), and characteristic strength (σ0). The microstructures were examined with a scanning electron microscope and X-ray diffraction. Results The mean ± standard deviation value of σ (MPa), m, and σ0 were 1,626.43 ± 184.38, 9.51, and 1,709.79 for CzAG; 1,734.98 ± 136.15, 12.83, and 1,799.17 for CzFP; 1,636.92 ± 130.11, 14.66, and 1,697.63 for CzFPOG; and 1,590.78 ± 161.74, 10.13, and 1,663.82 for CzFPHT; 643.30 ± 118.59, 5.59, and 695.55 for HzAG; 671.52 ± 96.77, 3.28, and 782.61 for HzFP; 556.33 ± 122.85, 4.76, and 607.01 for HzFPOG; and 598.36 ± 57.96, 11.22, and 624.89 for HzFPHT. The σ was significantly affected by the post-sintering process and type of zirconia (p < 0.05), but not by their interactions (p > 0.05). The Cz indicated a significantly higher σ than Hz. The FP process significantly enhanced σ more than other treatment procedures. Conclusion Post-sintering processes enabled an alteration in σ of zirconia. FP enhanced σ, while FPOG and FPHT resulted in a reduction of σ. Glazing tends to induce defects at the glazing interface, while heat treatment induces a phase change to tetragonal, both resulted in reducing σ. Finishing and polishing for both Cz and Hz monolithic zirconia is recommended, while overglazed or heat-treated is not suggested.

Impact of Silane-containing Universal Adhesive on the Biaxial Flexural Strength of a Resin Cement/Glass-ceramic System

2019 ◽  
Vol 44 (2) ◽  
pp. 200-209 ◽  
Author(s):  
F Murillo-Gómez ◽  
RB Wanderley ◽  
MF De Goes
Keyword(s):  
Flexural Strength ◽  
Glass Ceramic ◽  
Resin Cement ◽  
Weibull Analysis ◽  
Ceramic System ◽  
Universal Adhesive ◽  
Bonded Interface ◽  
Biaxial Flexural Strength ◽  
Digital Caliper ◽  
One Way Anova

SUMMARY The aim of this study was to determine whether using a silane-containing universal adhesive as a silane primer in glass-ceramic/resin cement systems affects biaxial flexural strength (BFS) and bonded interface integrity after loading. Glass-ceramic (IPS e.max CAD, Ivoclar/Vivadent, Schaan, Liechtenstein) disc-shaped specimens (6.5±0.1mm in diameter, 0.5±0.1mm thick) were etched with 5% hydrofluoric acid (HF) for 20 seconds and divided into four groups of 30 specimens, to be treated as follows: 1) One bottle silane primer (RCP); 2) Separate application of silane and adhesive (RCP+SB); 3) Silane-containing universal adhesive (SBU); 4) No treatment (C). After silanization, all specimens were resin cement– coated and polymerized for 40 seconds. Each specimen layer was measured, as well as each assembly's thickness, using a digital caliper and scanning electron microscope (SEM). Specimens were stored for 24 hours and submitted to a BFS test (1.27 mm/min). BFS values were calculated using the bilayer disc-specimen solution. Bonded interfaces were analyzed on fractured fragments using SEM. One-way ANOVA and Tukey tests (α=0.05) were applied, as well as the Weibull analysis. Factor “silane treatment” was statistically significant (p&lt;0.0001). RCP+SB (372.2±29.4 MPa) and RCP (364.2±29.5 MPa) produced significantly higher BFS than did the C (320.7±36.3 MPa) or SBU (338.0±27.1 MPa) groups. No differences were found in the Weibull modulus (m: RCP: 10.1-17.3; RCP+SB: 10.1-17.0; SBU: 12.3-22.4; C: 7.4-12.9). Bonded interface analysis exhibited ceramic-cement separation (SBU, C) and voids within the resin cement layer (all groups). Neither the ceramic/cement system's BFS nor its bonded interface stability were improved by SBU after loading.

scholarly journals Biaxial flexural strength of different types of monolithic zirconia

2019 ◽  
Vol 22 (1) ◽  
pp. Process
Author(s):  
Shereen Ahmed Nossair ◽  
Tarek Salah ◽  
Kamal Khaled Ebeid
Keyword(s):  
Flexural Strength ◽  
Zirconia Ceramic ◽  
Group 4 ◽  
Dental Esthetics ◽  
Biaxial Flexural Strength ◽  
Different Types ◽  
Monolithic Zirconia ◽  
Group 5 ◽  
Group 2 ◽  
Post Hoc

Objective: This study was designed to evaluate the biaxial flexural strength (BFS) of different types of unshaded and shaded monolithic zirconia. Material and Methods: 120 monolithic zirconia ceramic discs were fabricated. They were divided into twelve groups (n=10), Group 1; Bruxzir unshaded, Group 2; Bruxzir shaded A2, Group 3; Bruxzir anterior white, Group 4; Bruxzir anterior shade A2, Group 5; Prettau unshaded, Group 6; Prettau shaded with A2 coloring liquid, Group 7; Prettau anterior white, Group 8; Prettau anterior shaded with A2 coloring liquid, Group 9; Katana HT white, Group 10; Katana HT shade A2, Group 11; Katana ST white, Group 12; Katana ST shade A2. All discs were milled using a dental milling machine, and had final dimensions after sintering of 15 mm diameter and 1 mm thickness. BFS was tested using piston on three ball technique. Results:  One-way ANOVA revealed significant differences among the 12 groups. Tukey post-hoc tests revealed no significant differences between the groups 3, 4, ,7 ,8 11, and 12. However, they all had BFS values that are significantly lower than all other groups. Group 2 showed statistically significant higher BFS values when compared to group 3,4, 7, 8, 11, and 12 while it showed statistically significant lower values when compared to groups 1, 5, 6, 9, and 10. Conclusion: Increase in the yttria content in zirconia led to a decrease in its BFS. Shading of zirconia did not have a significant effect on the final strength of zirconia. KeywordsDental ceramics; Dental esthetics; Flexural strength; Shaded zirconia. 

scholarly journals Evaluation of Dual-Cure Resin Cement Polymerization under Different Types and Thicknesses of Monolithic Zirconia

2019 ◽  
Vol 2019 ◽  
pp. 1-9 ◽  
Author(s):  
Pinar Turkoglu ◽  
Deniz Sen
Keyword(s):  
Vickers Hardness ◽  
Resin Cement ◽  
Different Types ◽  
Monolithic Zirconia ◽  
Different Depths ◽  
Post Hoc ◽  
One Way Anova

Purpose. The aim of the present study was to investigate the effects of the type and thickness of the zirconia material on the microhardness of the underlying dual-cure resin cement. Materials and Methods. Eight disk-shaped zirconia specimens with a 4-mm diameter and four varying thicknesses (0.5, 1.0, 1.5, and 2.0 mm) were fabricated from two different monolithic zirconia materials: posterior monolithic zirconia (Prettau) and anterior monolithic zirconia (Prettau Anterior). Dual-cure resin cement specimens with a 4-mm diameter and 5-mm height were prepared using Teflon cylinder molds and activated by light beneath the eight zirconia disks and without any zirconia disk for 20 s (n=12). A total of 108 specimens were embedded in acrylic. Vickers hardness of each specimen was measured at three different depths using a microhardness device with a 50-g load. All data were statistically evaluated using three-way ANOVA, one-way ANOVA, independent samples t-tests, and Bonferroni corrected post hoc tests (α=.05). Results. Dual-cure resin cement’s microhardness was significantly higher for the samples polymerized beneath anterior monolithic zirconia compared to posterior monolithic zirconia. The hardness decreased as the thickness increased for both types of zirconia; the latter was attributed to an attenuated curing efficiency. Conclusion. Microhardness of the dual-cure resin cement is influenced by both the type and the thickness of the monolithic zirconia restoration. Polymerization efficiency for resin cement cured under anterior monolithic zirconia may be superior to cured beneath posterior monolithic zirconia.

Physical Property Evaluation of Four Composite Materials

2013 ◽  
Vol 38 (5) ◽  
pp. E144-E153 ◽  
Author(s):  
M Chang ◽  
J Dennison ◽  
P Yaman
Keyword(s):  
Flexural Strength ◽  
Physical Properties ◽  
Vickers Hardness ◽  
Dwell Time ◽  
Testing Machine ◽  
Surface Hardness ◽  
Composite Resins ◽  
Bending Test ◽  
Polymerization Shrinkage ◽  
Hardness Tests

SUMMARY Purpose The purpose of this study was to evaluate the physical properties of current formulations of composite resins for polymerization shrinkage, surface hardness, and flexural strength. In addition, a comparison of Knoop and Vickers hardness tests was made to determine if there was a correlation in the precision between the two tests. Materials and Methods Four composite resin materials were used: Filtek LS (3M-ESPE), Aelite LS (Bisco), Kalore (GC America), and Empress Direct (Ivoclar). Ten samples of each composite (shade Vita A2) were used. Polymerization shrinkage was measured with the Kaman linometer using 2-mm-thick samples, cured for 40 seconds and measured with digital calipers for sample thickness. Surface microhardness samples were prepared (2-mm thick × 12-mm diameter) and sequentially polished using 600-grit silicone carbide paper, 9 μm and 1 μm diamond polishing solutions. After 24 hours of dry storage, Knoop (200 g load, 15 seconds dwell time) and Vickers (500 g load, 15 seconds dwell time) hardness tests were conducted. Flexural strength test samples (25 × 2 × 2 mm) were stored in 100% relative humidity and analyzed using a three-point bending test with an Instron Universal Testing Machine (Instron 5565, Instron Corp) applied at a crosshead speed of 0.75 ± 0.25 mm/min. Maximum load at fracture was recorded. One-way analysis of variance and Tukey multiple comparison tests were used to determine significant differences in physical properties among materials. Results Filtek LS had significantly lower shrinkage (0.45 [0.39] vol%). Aelite LS demonstrated the greatest Knoop surface hardness (114.55 [8.67] KHN), followed by Filtek LS, Kalore, and Empress Direct (36.59 [1.75] KHN). Vickers surface hardness was significantly greater for Aelite LS (126.88 [6.58] VH), followed by Filtek LS, Kalore, and Empress Direct (44.14 [1.02] VH). Flexural strength (MPa) was significantly higher for Aelite LS and Filtek LS (135.75 [17.35]; 129.42 [9.48]) than for Kalore and Empress Direct (86.84 [9.04]; 92.96 [9.27]). There is a strong correlation between results obtained using Knoop and Vickers hardness tests (r=0.99), although Vickers values were significantly greater for each material. Conclusion Results suggest that Aelite LS possesses superior hardness and flexural strength, while Filtek LS has significantly less shrinkage compared with the other composites tested.

scholarly journals Biaxial Flexural Strength of High-Translucence Monolithic Ceramics upon Various Thicknesses

2021 ◽  
Vol 2021 ◽  
pp. 1-10
Author(s):  
Niwut Juntavee ◽  
Apa Juntavee ◽  
Sirintana Phetpanompond
Keyword(s):  
Flexural Strength ◽  
Testing Machine ◽  
Lithium Silicate ◽  
Stabilized Zirconia ◽  
Varying Thickness ◽  
Significant Difference ◽  
Biaxial Flexural Strength ◽  
Yttria Partially Stabilized Zirconia ◽  
The Mean ◽  
Monolithic Ceramics

Introduction. High-translucence ceramics have been used increasingly. This study evaluated the biaxial flexural strength of different ceramics as a result of varying thicknesses. Materials and Methods. Circular discs with varied thickness of 0.4, 0.6, 0.8, 1.0, 1.2, 1.4, 1.6, 1.8, and 2.0 mm were prepared from high-translucence yttria-partially stabilized zirconia (HTY-PSZ); Bruxzir® Anterior (Bc), and zirconia-reinforced lithium silicate (ZLS) including Celtra® DUO (Cc) and VITA Suprinity® (Vc) (n = 15 discs/group). Biaxial flexural strength (σ) was evaluated utilizing piston-on-three-balls in a testing machine at a speed of 0.5 mm/min. A scanning electron microscope (SEM) was used to determine the microscopic structure. ANOVA and multiple comparisons were analyzed for significant differences (a = 0.05). Results. The mean ± sd value of σ (MPa) for thickness 0.4, 0.6, 0.8, 1.0, 1.2, 1.4, 1.6, 1.8, and 2.0 mm was 672.66 ± 107.54, 655.93 ± 93.98, 589.01 ± 63.63, 624.89 ± 87.08, 618.82 ± 83.36, 672.64 ± 84.61, 659.81 ± 122.89, 632.79 ± 92.54, and 657.86 ± 73.17, for Bc; 477.64 ± 88.23, 496.39 ± 86.36, 461.56 ± 57.00, 450.26 ± 86.60, 468.28 ± 83.65, 472.45 ± 53.63, 453.05 ± 72.50, 462.67 ± 47.57, and 535.28 ± 84.33, for Cc; and 500.97 ± 76.36, 506.70 ± 87.76, 557.82 ± 62.78, 543.76 ± 87.29, 507.53 ± 86.09, 502.46 ± 64.75, 557.70 ± 80.91, 527.04 ± 80.78, and 499.88 ± 57.35, for Vc. A significant difference in flexural strength was indicated among groups ( p < 0.05 ). Bc was significantly stronger than Cc and Vc ( p < 0.05 ). Varying thickness did not have a significant influence on strength ( p > 0.05 ). SEM revealed a tight arrangement of crystals for Bc and needle-like crystals diffusing in glass for Vc and Cc. Conclusion. Flexural strength of ceramics varied among types, but each retained strength equitably with varying thickness. HTY-PSZ was stronger than ZLS, but each was equally strong for thickness in the range of 0.4–2.0 mm.

scholarly journals Influence of grinding procedures on the flexural strength of zirconia ceramics

2010 ◽  
Vol 21 (6) ◽  
pp. 528-532 ◽  
Author(s):  
Ufuk İşerı ◽  
Zeynep Özkurt ◽  
Ender Kazazoğlu ◽  
Davut Küçükoğlu
Keyword(s):  
Flexural Strength ◽  
High Speed ◽  
Testing Machine ◽  
Fracture Load ◽  
Bending Test ◽  
Control Group ◽  
Zirconia Ceramics ◽  
Significance Level ◽  
Universal Testing ◽  
Short Time

The surface of zirconia may be damaged during grinding, influencing the mechanical properties of the material. The purpose of this study was to compare the flexural strength of zirconia after different grinding procedures. Twenty bar-type zirconia specimens (21 x 5 x 2 mm) were divided into 4 groups and ground using a high-speed handpiece or a low-speed straight handpiece until the bars were reduced 1 mm using two different grinding times: continuous grinding and short-time grinding (n=5). Control specimens (n=5) were analyzed without grinding. The flexural strengths of the bars were determined by using 3-point bending test in a universal testing machine at a crosshead speed of 0.5 mm/min. The fracture load (N) was recorded, and the data were analyzed statistically by the Kruskal Wallis test at a significance level of 0.05. In the test groups, high-speed handpiece grinding for a short time had produced the highest mean flexural strength (878.5 ± 194.8 MPa), while micromotor continuous grinding produced the lowest mean flexural strength (733.8 ± 94.2 MPa). The control group was the strongest group (928.4 ± 186.5 MPa). However, there was no statistically significant differences among the groups (p>0.05). Within the limitations of the study, there was no difference in flexural strength of zirconia specimens ground with different procedures.

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