Laser surface treatment of aluminum composite: surface characteristics

2016 ◽  
Vol 23 (5) ◽  
pp. 495-503 ◽  
Author(s):  
Bekir S. Yilbas ◽  
Ihsan-ul-Haq Toor ◽  
Jahanzaib Malik
Keyword(s):  
Corrosion Resistance ◽  
Laser Treatment ◽  
Large Scale ◽  
Pure Aluminum ◽  
Surface Characteristics ◽  
Surface Region ◽  
Dense Layer ◽  
Aluminum Composite ◽  
Composite Surface ◽  
Electron Microscopes

AbstractLaser treatment of an aluminum composite surface was carried out to improve tribological properties and corrosion resistance at the surface. The workpiece consists of 15% SiC and pure aluminum, and it is produced by hot pressing. The characteristics of the laser-treated surface were examined using optical and scanning electron microscopes, energy dispersive spectroscopy, X-ray diffraction, a micro-tribometer, and a potentiostat. Laser treatment was carried out by following a spiral scanning track at the surface. This provides a self-annealing effect of the lately formed laser tracks on the initially formed tracks while lowering the cooling rates at the surface. It was found that laser-treated surfaces are free from asperities such as large-scale cracks and voids. Laser treatment improves the hardness of the surface because of the dense layer formation in the surface region. The friction coefficient of the laser-treated surface attains lower values than that corresponding to the untreated surface. Laser treatment improves the corrosion resistance of the surface.

Laser Texturing of Plasma Electrolytically Oxidized Aluminum 6061 Surfaces for Improved Hydrophobicity

2014 ◽  
Vol 136 (5) ◽  
Author(s):  
B. S. Yilbas ◽  
A. Matthews ◽  
C. Karatas ◽  
A. Leyland ◽  
M. Khaled ◽  
...  
Keyword(s):  
Laser Treatment ◽  
Water Droplet ◽  
Treatment Process ◽  
Surface Characteristics ◽  
High Water ◽  
Contact Angles ◽  
Laser Surface Texturing ◽  
Dense Layer ◽  
Textured Surface ◽  
X Ray

Laser surface texturing of plasma electrolytically oxidized aluminum 6061 alloy has been carried out through a controlled surface ablation under a high pressure nitrogen gas assistance. Morphological and metallurgical changes in the laser-treated region were examined using optical, scanning electron, and atomic force microscopy, energy dispersive X-ray spectroscopy, and X-ray diffraction phase analysis. The hydrophobicity of the textured surface was assessed through water droplet contact angle measurements. It was found that a dense layer with a nanotexture/microtexture is developed at the surface after the laser treatment process. The assessment of the surface characteristics reveals that a superhydrophobic surface results from the laser treatment process; in which case, high water droplet contact angles are measured over the treated surface, which can be explained by known models of texture-induced superhydrophobicity.

ALUMINUM 1100

Alloy Digest ◽  
1974 ◽  
Vol 23 (2) ◽  
Keyword(s):  
Corrosion Resistance ◽  
Shear Strength ◽  
High Temperature ◽  
Physical Properties ◽  
Tensile Properties ◽  
Pure Aluminum ◽  
Heat Treating ◽  
Industrial Applications ◽  
Temperature Performance ◽  
Commercially Pure

Abstract ALUMINUM 1100 is commercially pure aluminum and is characterized by its excellent ability to be drawn, spun, stamped or forged. It has good weldability, excellent resistance to corrosion and many home, architectural and industrial applications. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and shear strength as well as fatigue. It also includes information on low and high temperature performance, and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Al-44. Producer or source: Various aluminum companies. Originally published October 1956, revised February 1974.

KYNAL P10

Alloy Digest ◽  
1957 ◽  
Vol 6 (10) ◽  
Keyword(s):  
Corrosion Resistance ◽  
Shear Strength ◽  
High Temperature ◽  
Physical Properties ◽  
Tensile Properties ◽  
Pure Aluminum ◽  
Heat Treating ◽  
High Corrosion Resistance ◽  
Temperature Performance ◽  
Commercially Pure

Abstract KYNAL P10 is a grade of commercially pure aluminum having high corrosion resistance and fabricating qualities. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and shear strength as well as fatigue. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Al-57. Producer or source: Imperial Chemical Industries Inc..

scholarly journals The Potential of Calcium/Phosphate Containing MAO Implanted in Bone Tissue Regeneration and Biological Characteristics

2021 ◽  
Vol 22 (9) ◽  
pp. 4706
Author(s):  
Shun-Yi Jian ◽  
Salim Levent Aktug ◽  
Hsuan-Ti Huang ◽  
Cheng-Jung Ho ◽  
Sung-Yen Lin ◽  
...  
Keyword(s):  
Corrosion Resistance ◽  
Calcium Phosphate ◽  
Soft Tissues ◽  
Salt Spray ◽  
Surface Characteristics ◽  
Corrosion Current ◽  
Biological Properties ◽  
Bone Tissue Regeneration ◽  
Additional Surgery

Micro arc oxidation (MAO) is a prominent surface treatment to form bioceramic coating layers with beneficial physical, chemical, and biological properties on the metal substrates for biomaterial applications. In this study, MAO treatment has been performed to modify the surface characteristics of AZ31 Mg alloy to enhance the biocompatibility and corrosion resistance for implant applications by using an electrolytic mixture of Ca3(PO4)2 and C10H16N2O8 (EDTA) in the solutions. For this purpose, the calcium phosphate (Ca-P) containing thin film was successfully fabricated on the surface of the implant material. After in-vivo implantation into the rabbit bone for four weeks, the apparent growth of soft tissues and bone healing effects have been documented. The morphology, microstructure, chemical composition, and phase structures of the coating were identified by SEM, XPS, and XRD. The corrosion resistance of the coating was analyzed by polarization and salt spray test. The coatings consist of Ca-P compounds continuously have proliferation activity and show better corrosion resistance and lower roughness in comparison to mere MAO coated AZ31. The corrosion current density decreased to approximately 2.81 × 10−7 A/cm2 and roughness was reduced to 0.622 μm. Thus, based on the results, it was anticipated that the development of degradable materials and implants would be feasible using this method. This study aims to fabricate MAO coatings for orthopedic magnesium implants that can enhance bioactivity, biocompatibility, and prevent additional surgery and implant-related infections to be used in clinical applications.

scholarly journals Effect of Microwave and Conventional Modes of Heating on Sintering Behavior, Microstructural Evolution and Mechanical Properties of Al-Cu-Mn Alloys

Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3675
Author(s):  
A. Muthuchamy ◽  
Muthe Srikanth ◽  
Dinesh K. Agrawal ◽  
A. Raja Annamalai
Keyword(s):  
Mechanical Properties ◽  
Corrosion Resistance ◽  
Aluminum Alloys ◽  
Sintered Sample ◽  
Sintering Behavior ◽  
Sintered Alloy ◽  
Conventional Radiation ◽  
Sintered Aluminum ◽  
Electron Microscopes ◽  
Mechanical Properties And Corrosion

In this research, we intended to examine the effect of heating mode on the densification, microstructure, mechanical properties, and corrosion resistance of sintered aluminum alloys. The compacts were sintered in conventional (radiation-heated) and microwave (2.45 GHz, multimode) sintering furnaces followed by aging. Detailed analysis of the final sintered aluminum alloys was done using optical and scanning electron microscopes. The observations revealed that the microwave sintered sample has a relatively finer microstructure compared to its conventionally sintered counterparts. The experimental results also show that microwave sintered alloy has the best mechanical properties over conventionally sintered compacts. Similarly, the microwave sintered samples showed better corrosion resistance than conventionally sintered ones.

scholarly journals Study on Interface Structure of Cu/Al Clad Plates by Roll Casting

Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 770 ◽  
Author(s):  
Qinghua Chang ◽  
Jingpei Xie ◽  
Aixia Mao ◽  
Wenyan Wang
Keyword(s):  
Molecular Dynamics ◽  
Electron Microscope ◽  
Molecular Dynamics Simulation ◽  
Large Scale ◽  
Aluminum Atom ◽  
Simulation Software ◽  
Dynamics Simulation ◽  
Aluminum Composite ◽  
Atom Diffusion ◽  
Heating And Cooling

Large scale Atomic/Molecular dynamic Parallel Simulator (LAMMPS) molecular dynamics simulation software was used to simulate the copper and aluminum atom diffusion and changes of interface during heating and cooling process of copper and aluminum composite panels. The structures of the interface were characterized through scanning electron microscope (SEM), X-ray diffraction (XRD), and transmission electron microscope (TEM), and the mechanical properties were also tested. The simulation results show that the diffusion rate of copper atom is higher than that of aluminum atom, and that the CuAl2 radial distribution function of the interface at 300 K is consistent with that of pure CuAl2 at room temperature. At 930 K, t = 50 ps Cu atoms spread at a distance of approximately four Al lattice constants around the Al layer, and Al atoms spread to about half a lattice constant distance to the Cu layer. The experimental results show that the thickness of the interface in copper–aluminum composite plate is about 1 μm, and only one kind of CuAl2 with tetragonal phase structure is generated in the interface, which corresponds with the result of molecular dynamics simulation.

scholarly journals Collecting large datasets of rotational electron diffraction with ParallEM and SerialEM

2020 ◽  
Author(s):  
Kiyofumi Takaba ◽  
Saori Maki-Yonekura ◽  
Koji Yonekura
Keyword(s):  
Electron Diffraction ◽  
Data Collection ◽  
Large Scale ◽  
General Purpose ◽  
Task Specialization ◽  
Camera Control ◽  
Combined Use ◽  
Electron Microscopes ◽  
Diffraction Patterns ◽  
Automated Protocol

AbstractA semi-automated protocol has been developed for rotational data collection of electron diffraction patterns by combined use of SerialEM and ParallEM, where SerialEM is used for positioning of sample crystals and ParallEM for rotational data collection. ParallEM calls standard camera control software through an AutoIt script, which adapts to software operational changes and to new GUI programs guiding other cameras. Development included periodic flashing and pausing of data collection during overnight or day-long recording with a cold field-emission beam. The protocol proved to be efficient and accurate in data collection of large-scale rotational series from two JEOL electron microscopes, a general-purpose JEM-2100 and a high-end CRYO ARM 300. Efficiency resulted from simpler steps and task specialization. It is possible to collect 12–20 rotational series from ∼ −68º to ∼ 68º at a rotation speed of 1º /s in one hour without human supervision.

Large-Scale Evaluation of Constrained Bearing Elements Made of Thermosetting Polyester Resin and Polyester Fabric Reinforcement

2006 ◽  
Vol 128 (4) ◽  
pp. 681-696 ◽  
Author(s):  
P. Samyn ◽  
W. Van Paepegem ◽  
J. S. Leendertz ◽  
A. Gerber ◽  
L. Van Schepdael ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
Large Scale ◽  
Elastic Recovery ◽  
Small Scale ◽  
Practical Implementation ◽  
Fiber Failure ◽  
Stick Slip ◽  
Composite Surface ◽  
Pull Out ◽  
Stable Sliding

Polymer composites are increasingly used as sliding materials for high-loaded bearings, however, their tribological characteristics are most commonly determined from small-scale laboratory tests. The static strength and dynamic coefficients of friction for polyester/polyester composite elements are presently studied on large-scale test equipment for determination of its bearing capacity and failure mechanisms under overload conditions. Original test samples have a diameter of 250 mm and thickness of 40 mm, corresponding to the practical implementation in the sliding surfaces of a ball-joint, and are tested at various scales for simulation of edge effects and repeatability of test results. Static tests reveal complete elastic recovery after loading to 120 MPa, plastic deformation after loading at 150 MPa and overload at 200 MPa. This makes present composite favorable for use under high loads, compared to, e.g., glass-fibre reinforced materials. Sliding tests indicate stick-slip for pure bulk composites and more stable sliding when PTFE lubricants are added. Dynamic overload occurs above 120 MPa due to an expansion of the nonconstrained top surface. A molybdenum-disulphide coating on the steel counterface is an effective lubricant for lower dynamic friction, as it favorably impregnates the composite sliding surface, while it is not effective at high loads as the coating is removed after sliding and high initial static friction is observed. Also a zinc phosphate thermoplastic coating cannot be applied to the counterface as it adheres strongly to the composite surface with consequently high initial friction and coating wear. Most stable sliding is observed against steel counterfaces, with progressive formation of a lubricating transfer film at higher loads due to exposure of PTFE lubricant. Composite wear mechanisms are mainly governed by thermal degradation of the thermosetting matrix (max. 162°C) with shear and particle detachment by the brittle nature of polyester rather than plastic deformation. The formation of a sliding film protects against fiber failure up to 150 MPa, while overload results in interlaminar shear, debonding, and ductile fiber pull-out.

scholarly journals Effects of Processing Parameters on the Corrosion Performance of Plasma Electrolytic Oxidation Grown Oxide on Commercially Pure Aluminum

Metals ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 394 ◽  
Author(s):  
Getinet Asrat Mengesha ◽  
Jinn P. Chu ◽  
Bih-Show Lou ◽  
Jyh-Wei Lee
Keyword(s):  
Surface Roughness ◽  
Corrosion Resistance ◽  
Oxide Layer ◽  
Layer Thickness ◽  
Surface Engineering ◽  
Electrochemical Impedance ◽  
Pure Aluminum ◽  
Corrosion Performance ◽  
Commercially Pure ◽  
Peo Coatings

The plasma electrolyte oxidation (PEO) process has been considered an environmentally friendly surface engineering method for improving the corrosion resistance of light weight metals. In this work, the corrosion resistance of commercially pure Al and PEO treated Al substrates were studied. The PEO layers were grown on commercially pure aluminum substrates using two different alkaline electrolytes with different addition concentrations of Si3N4 nanoparticles (0, 0.5 and 1.5 gL−1) and different duty cycles (25%, 50%, and 80%) at a fixed frequency. The corrosion properties of PEO coatings were investigated by the potentiodynamic polarization and electrochemical impedance spectroscopy test in 3.5 wt.% NaCl solutions. It showed that the weight gains, layer thickness and surface roughness of the PEO grown oxide layer increased with increasing concentrations of Si3N4 nanoparticles. The layer thickness, surface roughness, pore size, and porosity of the PEO oxide layer decreased with decreasing duty cycle. The layer thickness and weight gain of PEO coating followed a linear relationship. The PEO layer grown using the Na2B4O7∙10H2O contained electrolyte showed an excellent corrosion resistance and low surface roughness than other PEO coatings with Si3N4 nanoparticle additives. It is noticed that the corrosion performance of PEO coatings were not improved by the addition of Si3N4 nanoparticle in the electrolytic solutions, possibly due to its detrimental effect to the formation of a dense microstructure.

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