Laser Texturing of Plasma Electrolytically Oxidized Aluminum 6061 Surfaces for Improved Hydrophobicity

2014 ◽  
Vol 136 (5) ◽  
Author(s):  
B. S. Yilbas ◽  
A. Matthews ◽  
C. Karatas ◽  
A. Leyland ◽  
M. Khaled ◽  
...  
Keyword(s):  
Laser Treatment ◽  
Water Droplet ◽  
Treatment Process ◽  
Surface Characteristics ◽  
High Water ◽  
Contact Angles ◽  
Laser Surface Texturing ◽  
Dense Layer ◽  
Textured Surface ◽  
X Ray

Laser surface texturing of plasma electrolytically oxidized aluminum 6061 alloy has been carried out through a controlled surface ablation under a high pressure nitrogen gas assistance. Morphological and metallurgical changes in the laser-treated region were examined using optical, scanning electron, and atomic force microscopy, energy dispersive X-ray spectroscopy, and X-ray diffraction phase analysis. The hydrophobicity of the textured surface was assessed through water droplet contact angle measurements. It was found that a dense layer with a nanotexture/microtexture is developed at the surface after the laser treatment process. The assessment of the surface characteristics reveals that a superhydrophobic surface results from the laser treatment process; in which case, high water droplet contact angles are measured over the treated surface, which can be explained by known models of texture-induced superhydrophobicity.

Laser surface treatment of aluminum composite: surface characteristics

2016 ◽  
Vol 23 (5) ◽  
pp. 495-503 ◽  
Author(s):  
Bekir S. Yilbas ◽  
Ihsan-ul-Haq Toor ◽  
Jahanzaib Malik
Keyword(s):  
Corrosion Resistance ◽  
Laser Treatment ◽  
Large Scale ◽  
Pure Aluminum ◽  
Surface Characteristics ◽  
Surface Region ◽  
Dense Layer ◽  
Aluminum Composite ◽  
Composite Surface ◽  
Electron Microscopes

AbstractLaser treatment of an aluminum composite surface was carried out to improve tribological properties and corrosion resistance at the surface. The workpiece consists of 15% SiC and pure aluminum, and it is produced by hot pressing. The characteristics of the laser-treated surface were examined using optical and scanning electron microscopes, energy dispersive spectroscopy, X-ray diffraction, a micro-tribometer, and a potentiostat. Laser treatment was carried out by following a spiral scanning track at the surface. This provides a self-annealing effect of the lately formed laser tracks on the initially formed tracks while lowering the cooling rates at the surface. It was found that laser-treated surfaces are free from asperities such as large-scale cracks and voids. Laser treatment improves the hardness of the surface because of the dense layer formation in the surface region. The friction coefficient of the laser-treated surface attains lower values than that corresponding to the untreated surface. Laser treatment improves the corrosion resistance of the surface.

scholarly journals Operational Properties of the Cermet Electro-Spark Coatings after Laser Treatment – Technology and Application

2019 ◽  
Vol 1 (1) ◽  
pp. 797-804
Author(s):  
Norbert Radek ◽  
Jacek Pietraszek ◽  
Janusz Konstanty
Keyword(s):  
Laser Treatment ◽  
Treatment Process ◽  
Sliding Friction ◽  
Protective Coatings ◽  
Structure Refinement ◽  
X Ray Diffraction ◽  
Roughness Measurement ◽  
Treatment Technology ◽  
X Ray ◽  
Hardness Tests

AbstractThe paper is concerned with determining the influence of the laser treatment process on the properties of electro-spark coatings. The properties of the coatings after laser treatment were assessed based on following methods: microstructure and X-ray diffraction analysis, adhesion tests, roughness measurement, hardness tests, tribological properties and application tests. The tests were carried out on WC-Co coating (the anode) obtained by electro-spark deposition over carbon steel C45 (the cathode) and molten with a laser beam. The coatings were deposited by means of the EIL-8A and they were laser treated with the Nd:YAG. The tests show that the laser-treated electro-spark deposited WC-Co coatings are characterized by lower hardness, higher seizure resistance, roughness and adhesion. The laser treatment process causes the homogenization of the chemical composition, the structure refinement and the healing of microcracks and pores of the electro-spark deposited coatings. Laser treated electro-spark deposited coatings are likely to be applied in sliding friction pairs and as protective coatings.

scholarly journals Wetting Behavior and Tribological Properties of Polymer Brushes on Laser-Textured Surface

Polymers ◽  
2019 ◽  
Vol 11 (6) ◽  
pp. 981 ◽  
Author(s):  
Ming-xue Shen ◽  
Zhao-xiang Zhang ◽  
Jin-tao Yang ◽  
Guang-yao Xiong
Keyword(s):  
Wear Resistance ◽  
Photoelectron Spectroscopy ◽  
Polymer Brushes ◽  
Polymer Brush ◽  
Surface Texturing ◽  
Contact Angles ◽  
Friction Reduction ◽  
Laser Surface Texturing ◽  
Textured Surface ◽  
Water Contact

Polymer brush layers can act as effective lubricants owing to their low friction and good controllability. However, their application to the field of tribology is limited by their poor wear resistance. This study proposes a strategy combining grafting and surface texturing to extend the service life of polymer brushes. Surface microstructure and chemical composition were measured through scanning electron microscopy (SEM), atomic force microscopy (AFM), and X-ray photoelectron spectroscopy (XPS). Water contact angles were measured to evaluate the surface wettability of the grafted silicon-based surface texture. Results showed the distinct synergistic effect between polymer brushes and laser surface texturing (LST). The prepared polymer brushes on textured surface can be a powerful mechanism for friction reduction properties, which benefit from their strong hydration effect on the lubrication liquid and promote the formation of a local lubricating film. Moreover, the wear life of polymer brushes can be immensely extended, as micro-dimples on the textured surface can effectively protect the polymer brushes. This study presents a method to enhance the load-bearing capacity and wear resistance of the grafted surface of polymer brushes.

Photocatalytic activity of TiO2 synthesized by anodization and anodic spark deposition

MRS Advances ◽  
2020 ◽  
Vol 5 (61) ◽  
pp. 3141-3152
Author(s):  
Alma C. Chávez-Mejía ◽  
Génesis Villegas-Suárez ◽  
Paloma I. Zaragoza-Sánchez ◽  
Rafael Magaña-López ◽  
Julio C. Morales-Mejía ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Photocatalytic Activity ◽  
Surface Characteristics ◽  
Amorphous Solids ◽  
X Ray Diffraction ◽  
X Ray ◽  
Catalytic Activities ◽  
Anodic Spark Oxidation ◽  
Porous Surfaces ◽  
Scanning Electron

AbstractSeveral photocatalysts, based on titanium dioxide, were synthesized by spark anodization techniques and anodic spark oxidation. Photocatalytic activity was determined by methylene blue oxidation and the catalytic activities of the catalysts were evaluated after 70 hours of reaction. Scanning Electron Microscopy and X Ray Diffraction analysis were used to characterize the catalysts. The photocatalyst prepared with a solution of sulfuric acid and 100 V presented the best performance in terms of oxidation of the dye (62%). The electric potential during the synthesis (10 V, low potential; 100 V, high potential) affected the surface characteristics: under low potential, catalyst presented smooth and homogeneous surfaces with spots (high TiO2 concentration) of amorphous solids; under low potential, catalyst presented porous surfaces with crystalline solids homogeneously distributed.

Effect of Polymer, Road Surface, and Driving Conditions on Wear Surface Characteristics of Tire Treads

1973 ◽  
Vol 1 (4) ◽  
pp. 354-362 ◽  
Author(s):  
F. R. Martin ◽  
P. H. Biddison
Keyword(s):  
Wear Surface ◽  
Surface Characteristics ◽  
Road Surface ◽  
The Other ◽  
Mechanical Degradation ◽  
Textured Surface ◽  
Test Track ◽  
Driving Conditions ◽  
Styrene Butadiene ◽  
Cylindrical Particles

Abstract Treads made with emulsion styrene-butadiene copolymer (SBR), solution SBR, polybutadiene (BR), and a 60/40 emulsion SBR/BR mixture were built as four-way tread sections on G78-15 belted bias tires, which were driven over both concrete and gravel-textured highways and on a small, circular, concrete test track. The tires were front mounted. When driven on concrete highway, all except the BR tread had either crumbled- or liquid-appearing surfaces, thought to have been formed by mechanical degradation or fatigue. When cornered on concrete, these materials formed small cylindrical particles or rolls. The BR tread had a smooth, granular-textured surface when driven on concrete highway and a ridge or sawtooth abrasion pattern when cornered on concrete. All the materials appeared rough and torn when run on gravel-textured highway. The differences in wear surface formed on BR tread and the other three are thought to be due primarily to the relatively high resilience of BR.

scholarly journals Treatment of wood with atmospheric plasma discharge: study of the treatment process, dynamic wettability and interactions with a waterborne coating

Holzforschung ◽  
2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Jure Žigon ◽  
Matjaž Pavlič ◽  
Pierre Kibleur ◽  
Jan Van den Bulcke ◽  
Marko Petrič ◽  
...  
Keyword(s):  
Plasma Treatment ◽  
Treatment Process ◽  
Beech Wood ◽  
Treated Wood ◽  
Plasma Discharge ◽  
Contact Angles ◽  
Atmospheric Plasma ◽  
Waterborne Coating ◽  
Spruce Wood ◽  
The Impact

AbstractPlasma treatment is becoming a mature technique for modification of surfaces of various materials, including wood. A better insight in the treatment process and the impact of the plasma on properties of wood bulk are still needed. The study was performed on Norway spruce and common beech wood, as well as their thermally modified variations. The formations of the airborne discharge, as well as mass changes of the treated wood, were monitored. The impact of such treatment on wood-coating interaction was investigated by evaluating the dynamic wettability and penetration into wood. At the wood surface, plasma streamers were observed more intense on denser latewood regions. Wood mass loss was higher with increasing number of passes through the plasma discharge and was lower for thermally modified wood than for unmodified wood. Plasma treatment increased the surface free energy of all wood species and lowered the contact angles of a waterborne coating, these together indicating enhanced wettability after treatment. Finally, the distribution and penetration depth of the coating were studied with X-ray microtomography. It was found that the coating penetrated deeper into beech than into spruce wood. However, the treatment with plasma increased the penetration of the coating only into spruce wood.

Analysis of water droplet penetration in earth plasters using X-ray microtomography

2021 ◽  
Vol 283 ◽  
pp. 122651
Author(s):  
T. Mauffré ◽  
E. Keita ◽  
E. Contraires ◽  
F. McGregor ◽  
A. Fabbri
Keyword(s):  
Water Droplet ◽  
X Ray ◽  
Droplet Penetration

scholarly journals Does laser surface texturing really have a negative impact on the fatigue lifetime of mechanical components?

Friction ◽  
2021 ◽  
Author(s):  
Chia-Jui Hsu ◽  
Andreas Stratmann ◽  
Simon Medina ◽  
Georg Jacobs ◽  
Frank Mücklich ◽  
...  
Keyword(s):  
Boundary Lubrication ◽  
Surface Texturing ◽  
Contact Stresses ◽  
Laser Surface ◽  
Laser Surface Texturing ◽  
Wear Loss ◽  
Textured Surface ◽  
Periodic Patterns ◽  
Rolling Bearings ◽  
Fatigue Lifetime

AbstractLaser surface texturing (LST) has been proven to improve the tribological performance of machine elements. The micro-scale patterns manufactured by LST may act as lubricant reservoirs, thus supplying oil when encountering insufficient lubrication. However, not many studies have investigated the use of LST in the boundary lubrication regime, likely due to concerns of higher contact stresses that can occur with the increasing surface roughness. This study aims to examine the influence of LST on the fatigue lifetime of thrust rolling bearings under boundary lubrication. A series of periodic patterns were produced on the thrust rolling bearings, using two geometrically different designs, namely cross and dimple patterns. Base oil ISO VG 100 mixed with 0.05 wt% P of zinc dialkyldithiophosphate (ZDDP) was supplied. The bearings with cross patterns reduce the wear loss by two orders of magnitude. The patterns not only retain lubricant in the textured pockets but also enhance the formation of an anti-wear tribofilm. The tribofilm generation may be improved by the higher contact stresses that occur when using the textured surface. Therefore, in contrast to the negative concerns, the ball bearings with cross patterns were instead found to increase the fatigue life by a factor of three.

scholarly journals Enhanced Water Resistance of Recycled Newspaper/High Density Polyethylene Composite Laminates via Hydrophobic Modification of Newspaper Laminas

Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 421
Author(s):  
Binwei Zheng ◽  
Weiwei Zhang ◽  
Litao Guan ◽  
Jin Gu ◽  
Dengyun Tu ◽  
...  
Keyword(s):  
Stearic Acid ◽  
Photoelectron Spectroscopy ◽  
Composite Laminates ◽  
High Density Polyethylene ◽  
Water Resistance ◽  
Laminated Composite ◽  
High Strength ◽  
High Water ◽  
High Density ◽  
X Ray

A high strength recycled newspaper (NP)/high density polyethylene (HDPE) laminated composite was developed using NP laminas as reinforcement and HDPE film as matrix. Herein, NP fiber was modified with stearic acid (SA) to enhance the water resistance of the NP laminas and NP/HDPE composite. The effects of heat treatment and SA concentration on the water resistance and tensile property of NP and composite samples were investigated. The chemical structure of the NP was characterized with X-ray diffractometer, X-ray photoelectron spectroscopy and attenuated total reflectance Fourier transform infrared spectra techniques. The surface and microstructure of the NP sheets were observed by scanning electron microscopy. An expected high-water resistance of NP sheets was achieved due to a chemical bonding that low surface energy SA were grafted onto the modified NP fibers. Results showed that the hydrophobicity of NP increased with increasing the stearic acid concentration. The water resistance of the composite laminates was depended on the hydrophobicity of the NP sheets. The lowest value of 2 h water absorption rate (3.3% ± 0.3%) and thickness swelling rate (2.2% ± 0.4%) of composite were obtained when the SA concentration was 0.15 M. In addition, the introduction of SA can not only enhance the water resistance of the composite laminates, but also reduce the loss of tensile strength in wet conditions, which shows potential in outdoor applications.

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