Dynamics of Water in Crystal Hydrates
1967 ◽
Vol 22
(9)
◽
pp. 1440-1451
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Keyword(s):
X Ray
◽
The crystal structure of Na2S2O6·2 H2O has been refined by means of single crystal X-ray intensity data. The structure of the isotypic Li2S2O6·2 H20 was also determined by single crystal studies. Two dimensional differential FOURIER synthesis revealed the approximate positions of the hydrogen atoms. From 1H-NMR investigations, the crystal structure, and information gained by IR spectroscopy the complete atomic arrangement in these two substances was obtained. The influence of the dynamical behaviour of the water molecules is taken into account in determining the hydrogen positions.
Keyword(s):
2003 ◽
Vol 58
(10)
◽
pp. 971-974
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Keyword(s):
Keyword(s):