Influence of Deformation Speed on Fatigue and Tensile Properties of a Ti-Ni-Cu Shape Memory Alloy

1999 ◽  
Vol 604 ◽  
Author(s):  
Y Kishi ◽  
Z. Yajima ◽  
K Shimizu ◽  
M. Asai

AbstractThe mechanical fatigue life and tensile property of a Ti-41at.%Ni-8.5at.%Cu alloy, which was solution-treated after some thermo-mechanical treatments, were investigated at 370±1 K as a function of deformation speed. The tensile properties were also investigated at 295±1 K as a function of deformation speed. The B2→B19 martensitic transformation start temperature, Ms, of the alloy was determined to be 338 K by a differential scanning calorimetry, while that of the as-rolled alloy could not be determined. Two types of fatigue tests were carried out by using plate-shaped specimens of 3.5 mm width and 1.5 mm thickness with sinusoidal waveform stresses of 20 Hz and 0.5 Hz frequencies being applied respectively. The fatigue life obtained from the 20 Hz tests was superior to that from the 0.5 Hz tests, the former being about 2 times longer than the latter at the same stress level. Tensile tests were performed at three tensilem speeds of 8.3 × 106, 8.3 × 10−5 and 8.3 × 10−3 m/s. In all the stress - strain curves obtained, an apparent yielding was observed after the liner elastic deformation. The apparent yielding is due to the occurrence of martensitic transformation. The critical stress for inducing martensite and tensile fracture stress increased with increasing tensile speed. Therefore, it is clear that fatigue and tensile properties of Ti-Ni-Cu shape memory alloys are strongly affected by not only test temperature but also deformation speed.

Author(s):  
A. Bauer ◽  
M. Vollmer ◽  
T. Niendorf

AbstractIn situ tensile tests employing digital image correlation were conducted to study the martensitic transformation of oligocrystalline Fe–Mn–Al–Ni shape memory alloys in depth. The influence of different grain orientations, i.e., near-〈001〉 and near-〈101〉, as well as the influence of different grain boundary misorientations are in focus of the present work. The results reveal that the reversibility of the martensite strongly depends on the type of martensitic evolving, i.e., twinned or detwinned. Furthermore, it is shown that grain boundaries lead to stress concentrations and, thus, to formation of unfavored martensite variants. Moreover, some martensite plates seem to penetrate the grain boundaries resulting in a high degree of irreversibility in this area. However, after a stable microstructural configuration is established in direct vicinity of the grain boundary, the transformation begins inside the neighboring grains eventually leading to a sequential transformation of all grains involved.


2018 ◽  
Vol 165 ◽  
pp. 21002 ◽  
Author(s):  
Antonio J. Abdalla ◽  
Douglas Santos ◽  
Getúlio Vasconcelos ◽  
Vladimir H. Baggio-Scheid ◽  
Deivid F. Silva

In this work 300M steel samples is used. This high-strength steel is used in aeronautic and aerospace industry and other structural applications. Initially the 300 M steel sample was submitted to a heat treatment to obtain a bainític structure. It was heated at 850 °C for 30 minutes and after that, cooled at 300 °C for 60 minutes. Afterwards two types of surface treatments have been employed: (a) using low-power laser CO2 (125 W) for introducing carbon into the surface and (b) plasma nitriding at a temperature of 500° C for 3 hours. After surface treatment, the metallographic preparation was carried out and the observations with optical and electronic microscopy have been made. The analysis of the coating showed an increase in the hardness of layer formed on the surface, mainly, among the nitriding layers. The mechanical properties were analyzed using tensile and fatigue tests. The results showed that the mechanical properties in tensile tests were strongly affected by the bainitic microstructure. The steel that received the nitriding surface by plasma treatment showed better fatigue behavior. The results are very promising because the layer formed on steel surface, in addition to improving the fatigue life, still improves protection against corrosion and wear.


2008 ◽  
Vol 584-586 ◽  
pp. 127-132 ◽  
Author(s):  
Anastasia E. Sergeeva ◽  
Daria Setman ◽  
Michael Zehetbauer ◽  
Sergey Prokoshkin ◽  
Vladimir V. Stolyarov

The aim of this paper is the investigation of electroplastic deformation (EPD) and subsequent annealing influence on martensitic transformation in the shape memory Ni50.7Ti49.3 alloy. Using differential scanning calorimetry method it was shown that EPD at the low strain stimulates structure relaxation and recovers martensitic transformation in cooling, which is usually suppressed by cold rolling.


2016 ◽  
Vol 30 (28) ◽  
pp. 1650286
Author(s):  
Dovchinvanchig Maashaa ◽  
Ulzii-Orshikh Dorj ◽  
Malrey Lee ◽  
Min Hi Lee ◽  
Chunwang Zhao ◽  
...  

The effect of rare earth element neodymium (Nd) addition on the microstructure and martensitic transformation behavior of Ni[Formula: see text]Ti[Formula: see text]Nd[Formula: see text] ([Formula: see text] = 0, 0.1, 0.3, 0.5 and 0.7 at.%) shape memory alloy was investigated by scanning electronic microscope, X-ray diffraction and differential scanning calorimetry. The results show that the microstructure of Ni–Ti–Nd ternary alloy consists of NiNd phase, NiTi2 and the NiTi matrix. A one-step martensitic transformation is observed in the alloys. The martensitic transformation temperature Ms increases sharply increasing 0.1–0.7 at.% Nd content is added.


2005 ◽  
Vol 297-300 ◽  
pp. 1770-1775 ◽  
Author(s):  
Young Woo Choi ◽  
Byeong Wook Noh ◽  
Kyung Chun Ham ◽  
Sung In Bae

The fatigue life of hexagon head and socket head bolts, attached to vehicle a wheel, is assessed and the estimation of the residual life of existing bolts in vehicle wheel is investigated. Field- measured load histories were applied in this test. Tensile tests and fatigue tests were performed to evaluate the effect of tightening torque and to obtain the basic experimental data. A three-dimensional finite element analysis was also performed to evaluate the local stress fields. Miner’s rule was used to predict the fatigue life of bolts. The results indicate the prediction of fatigue life of the bolts was in good agreement with the real life of vehicle wheel bolts in this test.


2007 ◽  
Vol 539-543 ◽  
pp. 3169-3172 ◽  
Author(s):  
Tae Hyun Nam ◽  
Cheol Am Yu ◽  
Yun Jung Lee ◽  
Yinong Liu

Shape memory characteristics and superelasticity of an temperature gradient annealing(TGA) treated equiatomic Ti-Ni alloy have been investigated by means of differential scanning calorimetry(DSC), thermal cycling tests under constant load and tensile tests. By annealing 25% cold worked alloy under the temperature gradient from 658 K to 466 K, 7 K variation in TR*and 19 K variation in Ms* were obtained along the length of sample(150mm). Temperature dependence of transformation elongation(dε/dT) of TGA treated Ti-Ni alloy wires was in the range of 0.05 %/K and 0.01 %/K depending on annealing temperature ranges. The dε/dT obtained from TGA treated sample under the temperature gradient from 658 K to 466 K was 0.03 %/K. TGA treated alloy showed the clear superelastic recovery.


2012 ◽  
Vol 476-478 ◽  
pp. 1504-1507
Author(s):  
Hai Bo Wang ◽  
Shang Shen Feng ◽  
Pei Yang Cai ◽  
Yan Qiu Huo

The martensitic transformation, crystalline structure, microstructure and shape memory effect of the Ni53.25Mn21.75Ga25 (at.%) alloy are investigated by means of Differential Scanning Calorimetry (DSC), X-ray diffraction (XRD), Transmission Electron Microscope (TEM) and the standard metal strain gauge technique. The XRD results showed that the Ni53.25Mn21.75Ga25 alloy is composed of cubic parent phase at room temperature. TEM observation proved that the typical twin martensite is tetragonal structure and tweed-like contrast which is typical image for the parent phase. A large reversible transformation strain, about 0.54%, is obtained in this undeformed polycrystalline alloy due to martensitic transformation and its reverse transformation. This transformation strain is also increased to 0.65% by the external magnetic field. It is believed that the effect of the magnetic field on the preferential orientation of martensitic variants increases the transformation strain.


Proceedings ◽  
2020 ◽  
Vol 38 (1) ◽  
pp. 15
Author(s):  
Andrade ◽  
Soares ◽  
Nobrega ◽  
Hilário ◽  
Santos

This paper presents a characterization processes study of metallic alloys, more specifically the shape memory alloys (SMA) composed by Nickel and Titanium (NiTinol). Two different wire suppliers were studied, starting with metallographic analysis until observe the contours of the grain wires. Differential scanning calorimetry (DSC) test was also performed to obtain phase transformation temperatures of the NiTinol alloys. Finally, after several tensile tests, some results were obtained for stresses, strains, elasticity modules and maximum rupture deformation.


2005 ◽  
Vol 475-479 ◽  
pp. 1973-1976 ◽  
Author(s):  
Ailian Liu ◽  
Xianglong Meng ◽  
Wei Cai ◽  
Lian Cheng Zhao

The effect of cerium addition on the martensitic transformation behavior and microstructure of Ti50-x/2Ni50-x/2Cex (x=0, 0.5, 2, 5 and 10at.%) alloys have been studied by differential scanning calorimetry (DSC) and energy dispersive spectroscopy (EDS). The results show that the addition of cerium affects the martensitic transformation temperature obviously. With the increase of Ce content, the phase transformation temperatures first increase rapidly and then decrease slightly, which may be attributed to the change of the Ni/Ti ratio in matrix. Moreover, the dispersed Ce-riched second particles with various morphologies are observed in TiNiCe alloys.


2006 ◽  
Vol 510-511 ◽  
pp. 262-265
Author(s):  
Tae Hyun Nam ◽  
Shin Goo Hur ◽  
Jae Hwa Lee ◽  
Gyu Bong Cho

Shape memory characteristics and superelasticity of an equiatomic Ti-Ni alloy with surface sulfide layers were investigated by means of thermal cycling tests under constant load, tensile tests, and scanning electron microscopy. Martensitic transformation start temperature (Ms) increased by sulfidation, which is ascribed to a compressive stress imposed by surface sulfide layers. Surface sulfide layers were found to make transformation elongation be small when their thickness was less than 5 ㎛. This is ascribed to the fact that the surface sulfide layers were not detached from substrates and constrained martensitic transformation. When thickness of the surface sulfide layers was 35 ㎛, transformation elongation was not affected by them because they were detached during transformation. Superelastic recovery decreased by the sulfide layers when their thickness was about 5 ㎛, while it did not change when the thickness was about 35 ㎛.


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