Possible Artefacts in Measurement of Hardness and Elastic Modulus on Superhard Coatings and the Verification of the Correctness of the Data

2002 ◽  
Vol 750 ◽  
Author(s):  
S. Veprek ◽  
S. Mukherjee ◽  
P. Karvankova ◽  
H.-D. Männling ◽  
J. L. He ◽  
...  

ABSTRACTMeasurements of the hardness and Young's modulus of superhard coatings (HV≥40 GPa) by means of automated load-depth-sensing indentation technique can be subject to a number of errors that are discussed and exemplified here. Only load-independent values of hardness for loads larger than 30–50 mN can be considered reliable when the technique of Doerner and Nix (linear extrapolation of the unloading curve) is used to determine the corrected indentation depth. The results are compared with values of Vickers hardness calculated from the contact area of the remaining plastic deformation which was measured by means of calibrated scanning electron microscope. The values of Young's modulus obtained from the indentation are close to the zero-pressure shear modulus of the coatings as measured by means of Vibrating Reed and surface Brillouin scattering techniques.

2006 ◽  
Vol 21 (1) ◽  
pp. 161-173 ◽  
Author(s):  
S. Bueno ◽  
C. Baudin

The adequacy of instrumented Vickers depth-sensing microindentation to determine Young's modulus of alumina-based ceramics was analyzed. Monophase alumina materials and alumina + 10 vol% aluminium titanate composites, with different microstructures, were tested to determine the effect of microcracking. The load–depth penetration of the indenter curves together with the observation of the imprints by scanning electron microscopy were used to analyze the behavior of the materials. Maximum stiffness was determined from the derivatives of the load-depth curves during unloading. The areas of the imprints measured optically were more representative of the behavior of the materials than the areas calculated from depth-penetration measurements. The formation of microcracks affected the shape of the unloading portion of the curves. Significant differences between the values of Young's modulus determined for different materials and definite relationships between the microstructural parameters of the materials and the Young's modulus were found.


2006 ◽  
Vol 514-516 ◽  
pp. 1472-1476
Author(s):  
Jorge M. Antunes ◽  
Nataliya A. Sakharova ◽  
José Valdemar Fernandes ◽  
Luís Filipe Menezes

Depth sensing indentation equipment allows the mechanical properties of thin films to be easily determined, particularly the hardness and Young’s modulus. In order to minimize the influence of the substrate on the measured properties, the indentation depth must be limited to a small fraction of the film’s thickness. However, for very thin films, the determination of the contribution of the substrate and the film to the measured mechanical properties becomes a hard task, because both deform plastically. The numerical simulation of ultramicrohardness tests can be a helpful tool towards better understanding of the influence of the parameters involved in the mechanical characterization of thin films. For this purpose, a three-dimensional numerical simulation home code, HAFILM, was used to simulate ultramicrohardness tests on coated substrates. Materials with different Young’s modulus film/substrate ratios were tested. Analyses of strain and stress distributions for several indentation depth values were performed, in order to clarify the composite behaviour.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3467
Author(s):  
Anna Nocivin ◽  
Doina Raducanu ◽  
Bogdan Vasile ◽  
Corneliu Trisca-Rusu ◽  
Elisabeta Mirela Cojocaru ◽  
...  

The present paper analyzed the microstructural characteristics and the mechanical properties of a Ti–Nb–Zr–Fe–O alloy of β-Ti type obtained by combining severe plastic deformation (SPD), for which the total reduction was of etot = 90%, with two variants of super-transus solution treatment (ST). The objective was to obtain a low Young’s modulus with sufficient high strength in purpose to use the alloy as a biomaterial for orthopedic implants. The microstructure analysis was conducted through X-ray diffraction (XRD), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) investigations. The analyzed mechanical properties reveal promising values for yield strength (YS) and ultimate tensile strength (UTS) of about 770 and 1100 MPa, respectively, with a low value of Young’s modulus of about 48–49 GPa. The conclusion is that satisfactory mechanical properties for this type of alloy can be obtained if considering a proper combination of SPD + ST parameters and a suitable content of β-stabilizing alloying elements, especially the Zr/Nb ratio.


SPE Journal ◽  
2017 ◽  
Vol 22 (06) ◽  
pp. 1893-1914 ◽  
Author(s):  
Weiwei Wu ◽  
Mukul M. Sharma

Summary Fluid flow in unpropped and natural fractures is critical in many geophysical processes and engineering applications. The flow conductivity in these fractures depends on their closure under stress, which is a complicated mechanical process that is challenging to model. The challenges come from the deformation interaction and the close coupling among the fracture geometry, pressure, and deformation, making the closure computationally expensive to describe. Hence, most of the previous models either use a small grid system or disregard deformation interaction or plastic deformation. In this study, a numerical model is developed to simulate the stress-driven closure and the conductivity for fractures with rough surfaces. The model integrates elastoplastic deformation and deformation interaction, and can handle contact between heterogeneous surfaces. Computation is optimized and accelerated by use of an algorithm that combines the conjugate-gradient (CG) method and the fast-Fourier-transform (FFT) technique. Computation time is significantly reduced compared with traditional methods. For example, a speedup of five orders of magnitude is obtained for a grid size of 512 × 512. The model is validated against analytical problems and experiments, for both elastic-only and elastoplastic scenarios. It is shown that interaction between asperities and plastic deformation cannot be ignored when modeling fracture closure. By applying our model, roughness and yield stress are found to have a larger effect on fracture closure and compliance than Young's modulus. Plastic deformation is a dominant contributor to closure and can make up more than 70% of the total closure in some shales. The plastic deformation also significantly alters the relationship between fracture stiffness and conductivity. Surfaces with reduced correlation length produce greater conductivity because of their larger apertures, despite more fracture closure. They have a similar fraction of area in contact as compared with surfaces with longer fracture length, but the pattern of area in contact is more scattered. Contact between heterogeneous surfaces with more soft minerals leads to increased plastic deformation and fracture closure, and results in lower fracture conductivity. Fracture compliance appears not to be as sensitive to the distribution pattern of hard and soft minerals. Our model compares well with experimental data for fracture closure, and can be applied to unpropped or natural fractures. These results are obtained for a wide range of conditions: surface profile following Gaussian distribution with correlation length of 50 µm and roughness of 4 to 50 µm, yield stress of 100 to 1500 MPa, and Young's modulus of 20 to 60 GPa. The results may be different for situations outside this range of parameters.


2005 ◽  
Vol 128 (2) ◽  
pp. 179-184 ◽  
Author(s):  
J. Perry ◽  
M. Perl ◽  
R. Shneck ◽  
S. Haroush

The Bauschinger effect (BE) was originally defined as the phenomenon whereby plastic deformation causes a loss of yield strength restraining in the opposite direction. The Bauschinger effect factor (BEF), defined as the ratio of the yield stress on reverse loading to the initial yield stress, is a measure of the magnitude of the BE. The aim of the present work is to quantitatively evaluate the influence of plastic deformation on other material properties such as Young’s modulus and Poisson’s ratio for gun barrel steel, thus extending the definition of the Bauschinger effect. In order to investigate the change in this material’s properties resulting from plastic deformation, several uniaxial tension and compression tests were performed. The yield stress and Young’s modulus were found to be strongly affected by plastic strain, while Poisson’s ratio was not affected at all. An additional result of these tests is an exact zero offset yield point definition enabling a simple evaluation of the BEF. A simple, triphase test sufficient to characterize the entire elastoplastic behavior is suggested. The obtained experimental information is readily useful for autofrettage residual stress field calculations.


2005 ◽  
Vol 475-479 ◽  
pp. 1471-1474 ◽  
Author(s):  
Se Hwan Chi ◽  
Gen-Chan Kim ◽  
Jun Hwa Hong ◽  
Sang Chul Kwon ◽  
Jong Hwa Chang

The changes in the microhardness and Young’s modulus of the 2 MeV C+ ion–irradiated IG-110 isotropic nuclear graphite were evaluated by a dynamic ultra-microhardness test. Indentation depth and load dependency of the hardness and elastic modulus were observed possibly due to the formation of a range. Both the hardness and Young’s modulus (E) – dpa curves have shown an incubation dose for about ı 0.3 mdpa. After the incubation dose, both the hardness and E showed a rapid increase with the dose. The doses that corresponds to these rapid increases in the hardness and E coincides with the dose that corresponds to the beginning of the irradiationinduced surface distortion, and the loss of the graphite crystallinity (amorphization).


2010 ◽  
Vol 90 (1) ◽  
pp. 9-22 ◽  
Author(s):  
J.V. Fernandes ◽  
J.M. Antunes ◽  
N.A. Sakharova ◽  
M.C. Oliveira ◽  
L.F. Menezes

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