scholarly journals SYNTHESIS AND CHARACTERIZATION OF CALCIUM SILICATE FROM RICE HUSK ASH AND SNAIL SHELL

2019 ◽  
Vol 11 (2) ◽  
pp. 45
Author(s):  
Sadang Husain ◽  
Ninis Hadi Haryanti ◽  
Suryajaya Suryajaya ◽  
Antung Permitaria
Keyword(s):  
Rice Husk ◽  
Calcium Silicate ◽  
Rice Husk Ash ◽  
Wave Number ◽  
X Ray Diffraction ◽  
Solid Reaction ◽  
Snail Shell ◽  
X Ray ◽  
Infra Red

<p class="abstrak">Calcium silicate ceramics have been made using natural ingredients such as rice husk and snail shell with solid reaction techniques. The aim of this study to determine the characteristics of calcium silicate that have been sintered at a temperature of 900 <sup>°</sup>C, 1000 <sup>°</sup>C, and 1100 <sup>°</sup>C. Samples were characterized by X-Ray Diffraction (XRD), optical microscopy, and Fourier Transform Infra-Red (FTIR). The results of XRD characterization showed that CaSiO<sub>3</sub> (calcium silicate) along with the increase in calcination temperature and quantity was increased due to the increase of temperature of calcination. FTIR analysis showed that the Ca-Si-O bond was formed at wave number ranging from 848 cm<sup>-1</sup> and 999 – 1001 cm<sup>-1</sup>.</p>

Free Na and Less Fe Compositions of SiO2 Extracted from Rice Husk Ash as the Silica Source for Synthesis of White Mineral Trioxide Aggregate

2020 ◽  
Vol 840 ◽  
pp. 311-317
Author(s):  
Muhamad Ghadafi ◽  
Sri Juari Santosa ◽  
Yuichi Kamiya ◽  
Nuryono Nuryono
Keyword(s):  
Rice Husk ◽  
Rice Husk Ash ◽  
Mineral Trioxide Aggregate ◽  
Deionized Water ◽  
X Ray Diffraction ◽  
X Ray ◽  
Silica Source ◽  
Tricalcium Aluminate ◽  
White Mineral

In this research, we report the use of free sodium and less Fe ion silica (SiO2) for preparation of White Mineral Trioxide Aggregate (WMTA). SiO2 was extracted from rice husk ash (RHA) using NaOH 2 M and HCl 37% (v/v) and removal of Na was performed by washing the extracted SiO2 using deionized water with various volumes and techniques. Before extraction, RHA was calcined at a temperature of 700 °C for 3 h. Preparation of WMTA began with mixing the extracted SiO2 20%, CaO 60%, Al2O3 2%, and Bi2O3 18% (w/w). The mixture was calcined at temperatures of 1100 °C for 4 h, grounded to produce WMTA 200 mesh in size and then was characterized using Fourier Transformed Infrared (FTIR) spectrophotometer, X-ray Diffraction (XRD) and Scanning Electron Microscopy-Energy Dispersion X-ray (SEM-EDX). The WMTA characteristics were compared to that of the commercial WMTA ProRoot. The result shows that the silica that was potential as the silica source for WMTA preparation was extracted from RHA involving sonication and washing with 360 mL of deionized water per 10 g of RHA. It contained SiO2 of 94.2%, Fe2O3 of 0.03%, no Na2O, and the particle size of 1.51±0.46 µm. The characterization of WMTA shows that produced WMTA contained tricalcium silicate (C3S), dicalcium silicate (C2S), tricalcium aluminate (C3A) and BiO2, which is comparable to the commercial WMTA ProRoot.

Characterization of Cement-Rice Husk Ash Composites

2017 ◽  
Vol 866 ◽  
pp. 187-190
Author(s):  
Thossapon Jaihlong ◽  
Nittaya Jaitanong ◽  
Suparut Narksitipan
Keyword(s):  
Portland Cement ◽  
Rice Husk ◽  
Fiber Optic ◽  
Rice Husk Ash ◽  
Cementitious Materials ◽  
Cement Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Lime Water

In present research, the cement-rice husk ash composites were prepared and characterized. The samples were added fiber optic and rice husk ash was used as replacement cementitious materials at 10, 20, 30 and 40 wt% of portland cement. The samples were demolded after 24 h casting and cured in saturated lime water for 3 days. After these periods, the samples were wrapped with plastics films for 7 and 28 days. Then, samples were dried in air for 24 h. The chemical compositin of portland cement and rice husk ash were characterized by using x-ray fluorence spectrometry (XRF). Additionally, dried samples were analysized phase compositions and crystalline structure by using x-ray diffraction (XRD) technique. The chemical element compositions and microstructure were detected by scanning electron microscopy (SEM), respectively. Moreover, The effect of rice husk ash in these cement composites were investigated in this research.

Rice Husk Ash as a Raw Material to Produce Willemite Pigments

2018 ◽  
Vol 912 ◽  
pp. 44-49
Author(s):  
L.A. Vieira ◽  
Marilena Valadares Folgueras ◽  
M. Tomiyama ◽  
S.R. Prim
Keyword(s):  
Rice Husk ◽  
Rice Husk Ash ◽  
Synthesis Temperature ◽  
Raw Material ◽  
Ceramic Pigments ◽  
X Ray Diffraction ◽  
X Ray ◽  
Color Development ◽  
Ceramic Process

This study focuses in the synthesis of ceramic pigments based on the crystal structure of willemite (Zn2SiO4). The willemite obtained from the combination of commercial zinc oxide and rice husk ash is produced in a conventional ceramic process without the use of mineralizer agent and with the addition of cobalt oxide or nickel oxide as the source of chromophore ions. The synthesis temperature used was 1200°C. The characterization of pigments involves the use of X-ray diffraction and scanning electron microscopy. The pigments applied in matte enamel and sintered at 1100°C or 1200°C developed color between blue and beige. The construction of absorbance curves showed the color development behavior of each pigment. The results showed the possibility of obtaining willemite, from rice husk ash and the color development efficiency of the material, besides showing the interference of chromophore ion (Ni and Co) in color development.

Development of Ternary Concrete Utilizing Agricultural Waste Material

2022 ◽  
Author(s):  
Sunita Kumari ◽  
Dhirendra Singhal ◽  
Rinku Walia ◽  
Ajay Rathee
Keyword(s):  
Rice Husk ◽  
Rice Husk Ash ◽  
Agricultural Waste ◽  
Xrd Analysis ◽  
Sem Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Concrete Mix ◽  
Maize Cob

Abstract The present project proposes to utilize rice husk and maize cob husk ash in the cement to mitigate the adverse impact of cement on environment and to enhance the disposal of waste in a sustainable manner. Ternary concrete / MR concrete was prepared by using rise husk and maize cob ash with cement. For the present project, five concrete mixes MR-0 (Control mix), MR-1 (Rice husk ash 10% and MR-2.5%), MR-2 (Rice husk ash 10% and MR-5%), MR-3 (Rice husk ash 10% and MR-2.5%), MR-4 (Rice husk ash 10% and MR-2.5%) were prepared. M35 concrete mix was designed as per IS 10262:2009 for low slump values 0-25mm. The purpose is to find the optimum replacement level of cement in M35 grade ternary concrete for I – Shaped paver blocks.In order to study the effects of these additions, micro-structural and structural properties test of concretes have been conducted. The crystalline properties of control mix and modified concrete are analyzed by Fourier Transform Infrared Spectroscope (FTIR), Scanning Electron Microscopy (SEM), and X-Ray Diffraction (XRD). The results indicated that 10% Rice husk ash and 5% maize cob ash replaced with cement produce a desirable quality of ternary concrete mix having good compressive strength. The results of SEM analysis indicated that the morphology of both concrete were different, showing porous structure at 7 days age and become unsymmetrical with the addition of ashes. After 28 day age, the control mix contained more quantity of ettringite and became denser than ternary concrete. XRD analysis revealed the presence of portlandite in large quantity in controlled mix concrete while MR concrete had the partially hydrated particle of alite.

Comparison between Rice Husk Ash and Commercial Silica as Filler in Polymeric Composites

2016 ◽  
Vol 869 ◽  
pp. 209-214 ◽  
Author(s):  
Iara Janaína Fernandes ◽  
Daiane Calheiro ◽  
Emanuele Caroline Araújo dos Santos ◽  
Roxane Oliveira ◽  
Tatiana Louise Avila de Campos Rocha ◽  
...  
Keyword(s):  
Rice Husk ◽  
Rice Husk Ash ◽  
Polymeric Materials ◽  
Fluidized Bed Reactor ◽  
Specific Weight ◽  
High Energy ◽  
Loss On Ignition ◽  
X Ray Diffraction ◽  
X Ray ◽  
Different Sources

The use of rice husk ash (RHA) as filler in polymeric materials has been studied in different polymers. Research reported that RHA may successfully replace silica. The silica production process using ore demands high energy input and produces considerable amounts of waste. Therefore, the replacement of silica by RHA may be economically and environmentally advantageous, reducing environmental impact and adding value to a waste material. In this context, this study characterizes and compares RHA of different sources (moving grate and fluidized bed reactor) with commercially available silicas to assess performance as filler in polymeric materials. Samples were characterized by X-ray fluorescence, loss on ignition, X-ray diffraction, grain size, specific surface area, specific weight, and scanning electron microscopy. The results show that RHA may be used as a filler in several polymeric materials.

scholarly journals Preparation and characterization of rice husk ash (RHA)-TiO2 / ZnO composites and its application in treating effluents from textile industries

2013 ◽  
Vol 47 (4) ◽  
pp. 445-448 ◽  
Author(s):  
MH Kabir ◽  
MF Kabir ◽  
F Nigar ◽  
S Ahmed ◽  
AI Mustafa ◽  
...  
Keyword(s):  
Composite Materials ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Textile Dye ◽  
X Ray ◽  
Textile Dye Effluent ◽  
Degradation Reaction ◽  
D Values ◽  
Sun Light

Photocatalytic composite materials incorporating the photocatalysts (TiO2, ZnO) with rice husk ash (RHA) have been developed to investigate the photodegradation of real textile dye effluent. The structural characterization of the composite materials was performed using XRD (X-Ray Diffractometer). The characteristic XRD peaks together with the 2? values for both TiO2 and ZnO were in excellent agreement with the standard JCPDS d-values. The efficacy of these composites was examined through the degradation of a textile dye, collected from a local dye house. The sun light was used as the source of illumination for the preceding degradation reaction. Bangladesh J. Sci. Ind. Res. 47(4), 445-448, 2012 DOI: http://dx.doi.org/10.3329/bjsir.v47i4.14075

scholarly journals Solidification and Leachability of Cr (VI) in Rice Husk Ash-Blended Cement

2011 ◽  
Vol 2011 ◽  
pp. 1-6 ◽  
Author(s):  
Neeraj Jain
Keyword(s):  
Rice Husk ◽  
Rice Husk Ash ◽  
Setting Time ◽  
Blended Cement ◽  
X Ray Diffraction ◽  
Retention Capacity ◽  
Allowable Limit ◽  
X Ray ◽  
Curing Period ◽  
Leaching Procedure

Investigations carried out to study the effect of Cr (VI) (1000–3000 mg/l) on solidification and hydration behavior of Ordinary Portland cement (OPC) and rice husk ash (RHA) blended (10%, 20%, and 30%) cement show that addition of RHA accelerates final setting as compared to control samples (OPC) and retardation in setting time has been observed on increase in rice husk ash concentration (10%–30%). Solidification studies show that the compressive strength of controls and rice husk ash blended samples increases with increase in the curing period and maximum strength was observed with 20% RHA blended samples. With the increase in Cr (VI) concentrations, the strength of OPC and RHA blended samples decreases as compared to controls (without chromium). The results of Toxicity Characteristics Leaching Procedure (TCLP) test, (pH≅3), show that the retention capacity of OPC and RHA blended samples was in the range of 92% to 99% and the leached Cr (VI) concentration was under the allowable limit (5 mg/l) of U.S. EPA. The chemistry of influence of Cr (VI) on hydration of cement was examined by X-ray diffraction which shows the formation of various crystalline phases during solidification in rice hush ash blended cement.

scholarly journals Effects of Sintering Temperature Variation on Synthesis of Glass-Ceramic Phosphor Using Rice Husk Ash as Silica Source

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5413
Author(s):  
Rabiatul Adawiyah Abdul Wahab ◽  
Mohd Hafiz Mohd Zaid ◽  
Sidek Hj. Ab Aziz ◽  
Khamirul Amin Matori ◽  
Yap Wing Fen ◽  
...  
Keyword(s):  
Rice Husk ◽  
Glass Ceramic ◽  
Rice Husk Ash ◽  
Glass Ceramics ◽  
Xrd Analysis ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Silica Source ◽  
Quenching Method

In this study, the authors attempted to propose the very first study on fabrication and characterization of zinc-boro-silicate (ZBS) glass-ceramics derived from the ternary zinc-boro-silicate (ZnO)0.65(B2O3)0.15(RHA)0.2 glass system through a conventional melt-quenching method by incorporating rice husk ash (RHA) as the silica (SiO2) source, followed by a sintering process. Optimization of sintering condition has densified the sintered samples while embedded beta willemite (β-Zn2SiO4) and alpha willemite (α-Zn2SiO4) were proven in X-ray diffraction (XRD) analysis. Field emission scanning electron microscopy (FESEM) has shown the distribution of willemite crystals in rhombohedral shape crystals and successfully form closely-packed grains due to intense crystallization. The photoluminescence (PL) spectra of all sintered ZBS glasses presented various emission peaks at 425, 463, 487, 531, and 643 nm corresponded to violet, blue, green, and red emission, respectively. The correlation between the densification, phase transformation, microstructure, and photoluminescence of Zn2SiO4 glass-ceramic phosphor is discussed in detail.

Variables Involved in the Planting of Rice in the Rice Husk

2012 ◽  
Vol 517 ◽  
pp. 430-436
Author(s):  
J.L. Akasaki ◽  
E.J. Silva ◽  
L.C. Sousa ◽  
J.L.P. Melges ◽  
M.M. Tashima ◽  
...  
Keyword(s):  
Rice Husk ◽  
Large Scale ◽  
Rice Husk Ash ◽  
Scale Production ◽  
X Ray Diffraction ◽  
X Ray ◽  
Large Scale Production ◽  
Pozzolanic Materials ◽  
Different Strains ◽  
Different Origins

Rice production in Brazil in 2010 was approximately 12,2 million tons, and to reach that amount several planting techniques were used with different strains of rice in different rice-growing areas. Since Rice Husk Ash (RHA) is the pozzolan of vegetable origin most studied by researchers working in the area of pozzolanic materials, the present paper evaluates the influence that the form of planting, the climate, the soil, the strain of rice and the origin/amount of nitrogen-based fertilizers used in rice cultivation has on the chemical composition and crystallographic properties of RHA. The results obtained in this paper, confirm the importance of carrying out routine chemical analysis and X-Ray diffraction to maintain the quality control of the CCAs produced, because in situations of large-scale production, husks of different origins may be used.

scholarly journals Effects of Rice Husk Ash–Magnesium Oxide Addition on Wear Behavior of Aluminum Alloy Matrix Hybrid Composites

2018 ◽  
Vol 25 (4) ◽  
pp. 15-22
Author(s):  
Abbas Y. Awad ◽  
Mohammed N. Ibrahim ◽  
Mohamed K. Hussein
Keyword(s):  
Aluminum Alloy ◽  
Wear Rate ◽  
Apparent Density ◽  
Rice Husk ◽  
Applied Load ◽  
Rice Husk Ash ◽  
Hybrid Composites ◽  
Wear Behavior ◽  
X Ray Diffraction ◽  
X Ray

A336.0 aluminum alloy used to fabricate hybrid composites using rice husk ash (RHA) and MgO particles as reinforcement. The influence of the particles on the wear behavior of A336.0 aluminum alloy as a matrix that reinforced with MgO and RHA was investigated. Firstly, the rice husk burned at 700°C and then heat treated at 1100°C for 2 hrs. The ash characterized by X-ray florescence and X-ray diffraction. Less than 53 and 125 micron are the particle sizes of MgO and RHA respectively. The hybrid composites manufactured using stir casting method in two steps. A336.0 aluminum alloy reinforced with 4:0, 3:1, 2:2, 1:3 and 0:4 of RHA: MgO with 10 wt% total reinforcement phase. Optical microscope and X-ray diffraction were used to characterize the prepared hybrid composites. Dry sliding wear, hardness, apparent density, percentage of porosity and coefficient of friction were examined. Results indicated that porosity, apparent density and hardness enhanced with increasing MgO, while increasing wt% of RHA decreased the apparent density. Results indicated that with inceasing the applied load the wear rate of the composites was enhanced. Coefficient of friction varies inversely with applied load and wt% of RHA. Hardness increased with increasing RHA while the friction coefficient and the wear rate decreased. The minimum wear rates were at 10% RHA and Al-alloy-(RHA-MgO) [3:1] composites, while the minimum friction coefficients were at 10% RHA composites.

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