scholarly journals Synthesis of Tin(II) Oxide (SnO) Nanoparticle by Hydrothermal Method

2019 ◽  
Vol 4 (3) ◽  
pp. 145
Author(s):  
Saddam Husein ◽  
Endang Tri Wahyuni ◽  
Mudasir Mudasir
Keyword(s):  
Hydrothermal Method ◽  
Low Temperatures ◽  
Xrd Analysis ◽  
X Ray Diffraction ◽  
Simple Hydrothermal Method ◽  
X Ray ◽  
Chloride Dihydrate ◽  
Synthesis Parameters ◽  
Tetragonal Crystal ◽  
Potential Applications

<p>This study aims to prepare nanomaterial tin(II) oxide (SnO) by using a simple hydrothermal method at low temperatures. The precursors used were tin(II) chloride dihydrate and sodium hydroxide pellets. Solid tin(II) chloride dihydrate and natrium hydroxide pellets are firstly dissolved in ethanol solvents separately and stirred for 3 h for each solution at a constant temperature 26<sup>o</sup>C. Characterization in this study were carried out by using X-ray diffraction (XRD) and Scanning Electron Microscopy-Energy Dispersive X-ray Spectroscopy (SEM-EDX). The results of the XRD analysis shows that the sample of SnO nanoparticle is in accordance with the standard JCPDS SnO structure. SnO nanoparticle has tetragonal crystal structures and PSC: tp4 groups. It can be concluded that the tetragonal SnO nanostructure can be produced by a simple hydrothermal method at low temperatures by optimizing several synthesis parameters. The structure of SnO nanostructure has several potential applications i.e the absorption of heavy metals, optics, and as a catalyst for dye photodegradation.</p>

Synthesis and Characterization of Strontium Carbonate Nanostructures via Simple Hydrothermal Method

2016 ◽  
Vol 35 (2) ◽  
pp. 215-220
Author(s):  
Zahra Asgari-Fard ◽  
Mohammad Sabet ◽  
Masoud Salavati-Niasari
Keyword(s):  
Hydrothermal Method ◽  
Strontium Carbonate ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Product Size ◽  
Simple Hydrothermal Method ◽  
X Ray ◽  
Ft Ir ◽  
Size And Morphology

AbstractStrontium carbonate (SrCO3) nanostructures were synthesized via simple hydrothermal method by Sr(NO3)2, ethylenediamine and hydrazine as reagents. The products were characterized with X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX) and Fourier transform infrared spectroscopy (FT-IR). Different parameter’s effects on the product size and morphology were investigated. It was found that reagent concentration, reaction time and temperature play key roles in morphology of the obtained product.

Synthesis of CuO Microspheres by the Simple Hydrothermal Method and their Optical Absorption Properties

2012 ◽  
Vol 562-564 ◽  
pp. 490-493
Author(s):  
Xiao Ming Fu
Keyword(s):  
Optical Absorption ◽  
Hydrothermal Method ◽  
Xrd Analysis ◽  
Sem Analysis ◽  
X Ray Diffraction ◽  
Absorption Properties ◽  
Visible Absorption ◽  
X Ray ◽  
Cuo Microspheres ◽  
Visible Absorption Spectroscopy

CuO microspheres with a diameter range of 1~3 μm are successfully synthesized with 1 m mol CuCl2 as copper source and 3 m mol Na2CO3 as auxiliary salt at 180 °C for 24 h via the easy hydrothermal method. The phase, the morphologies and optical absorption properties of the samples have been characterized and analyzed by XRD (X-ray diffraction), SEM (Scanning electron microscope) and ultraviolet-visible absorption spectroscopy (UV-VIS), respectively. XRD analysis shows that the phase of as obtained samples is CuO. SEM analysis confirms that the increase of the the auxiliary salt is in favor of the synthesis of CuO microrods. And UV-VIS measurements show that CuO microspheres have a good optical absorption property.

CuO Microspheres Synthesized via the Easy Hydrothermal Method

2012 ◽  
Vol 159 ◽  
pp. 84-87
Author(s):  
Xiao Ming Fu
Keyword(s):  
Electron Microscope ◽  
Reaction Time ◽  
Scanning Electron Microscope ◽  
Hydrothermal Method ◽  
Xrd Analysis ◽  
Sem Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cuo Microspheres ◽  
Scanning Electron

CuO microspheres are successfully synthesized with CuCl2 as copper source and Na2CO3 as auxiliary salt at 240 °C for 24 h via the easy hydrothermal method. The phase and the morphologies of the samples have been characterized and analyzed by XRD (X-ray diffraction) and SEM (Scanning electron microscope), respectively. XRD analysis shows that the phase of as obtained samples is CuO. SEM analysis confirms that the increase of the reaction time, the reaction temperature and the auxiliary salt is propitious to synthesize CuO microspheres.

Synthesis of CuO Flower-Nanostructure via the Hydrothermal Method

2013 ◽  
Vol 873 ◽  
pp. 131-134
Author(s):  
Xiao Ming Fu ◽  
Jie Ren
Keyword(s):  
Electron Microscope ◽  
Reaction Time ◽  
Scanning Electron Microscope ◽  
Hydrothermal Method ◽  
Reaction Temperature ◽  
Xrd Analysis ◽  
Sem Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

CuO flower-nanostructures are successfully synthesized with CuCl2 as copper source and Na2CO3 as auxiliary salt at 180 °C for 24 h via the simple hydrothermal method. The phase and the morphologies of the samples have been characterized and analyzed by XRD (X-ray diffraction) and SEM (Scanning electron microscope), respectively. XRD analysis shows that the phase of as obtained samples is CuO. SEM analysis confirms that the increase of the reaction temperature is propitious to synthesize CuO flower-nanostructures while the increase of the reaction time is not in favor of their synthesis. The influence of the increase of the auxiliary salt on the morphology of CuO flower-nanostructures is not remarkable. The mechanism of the formation of CuO flower-nanostructure is discussed.

Effect of CeO2 Nanoparticle on the Structural and Electrical Properties of BSCCO-2223 High Temperature Superconductor

2020 ◽  
Vol 307 ◽  
pp. 104-109
Author(s):  
E.S. Nurbaisyatul ◽  
Hashim Azhan ◽  
Azman Kasim ◽  
Norazila Ibrahim
Keyword(s):  
High Temperature Superconductor ◽  
Xrd Analysis ◽  
Solid State Reaction Method ◽  
X Ray Diffraction ◽  
Critical Transition Temperature ◽  
X Ray ◽  
Tetragonal Crystal ◽  
Tetragonal Crystal Structure ◽  
Structural And Electrical Properties ◽  
Oxide Nanoparticle

A study of the effects of Cerium oxide nanoparticle doped with BSCCO-2223 on the microstructure and superconducting properties was carried out. All samples were synthesized using solid state reaction method. Ce concentration is varied from x = 0.0 up to 0.1 in a general stoichiometry of Bi1.6Pb0.4Sr2Ca1-xCexCu3Oy. The samples were characterized structurally and electrically by X-Ray Diffraction (XRD) and four-point probe method respectively. XRD analysis shows that both (Bi,Pb)-2212 and (Bi,Pb)-2223 phases coexist in the samples having tetragonal crystal structure but changed to orthorhombic when x=0.10. The values of critical transition temperature, TC and critical current density, JC of the samples decreased with the increase in Ce concentration. The possible reasons for the observed degradation in superconducting and structural properties of Bi-2223 due to Ce nanoparticles addition were discussed.

Characterization of Nanostructured Titania and Titanate Materials Synthesized by Simple Hydrothermal Method

2017 ◽  
Vol 889 ◽  
pp. 229-233
Author(s):  
Nur Arifah Ismail ◽  
Mohd Hasmizam Razali ◽  
Khairul Anuar ◽  
Mat Amin
Keyword(s):  
Hydrothermal Method ◽  
Hydrothermal Treatment ◽  
Deformation Mode ◽  
Xrd Analysis ◽  
Treatment Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Shaped Particle ◽  
Nanostructured Titania

In this research, the effect of different hydrothermal treatment temperature (100, 150, and 200 °C) on the products obtained by hydrothermal method was studied. Various characterization techniques was carried out such as X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), energy dispersive of x-ray spectroscopy (EDX) and fourier transform infrared spectroscopy (FTIR). XRD analysis shows that titanate phase was formed at 150 and 200 °C hydrothermal treatment. On the other hand, at 100 °C anatase TiO2 phase structured was gained which is similar with the TiO2 precursor. Morphological study using FESEM revealed that nanofibers and nanorods samples obtained at 150 °C and 200 °C, respectively. At 100°C, irregular shaped particle was attained similar with TiO2 precursors. FTIR spectra for the all studied sample displayed three main broad peaks at the range of 3700-2800, and 1800-1400 assigned to –OH stretching and deformation mode due to H2O molecules and M-O stretching mode at 900-400 cm-1 assigned to Ti-O bond.

Identification of acid-insoluble filter-plugging compounds and optimal acid-washing procedures for tubular backpulse pressure filters

TAPPI Journal ◽  
2011 ◽  
Vol 10 (1) ◽  
pp. 17-23
Author(s):  
KEVIN TAYLOR ◽  
RICH ADDERLY ◽  
GAVIN BAXTER
Keyword(s):  
Calcium Sulfate ◽  
Membrane Filter ◽  
Sulfamic Acid ◽  
Xrd Analysis ◽  
Metal Sulfides ◽  
X Ray Diffraction ◽  
X Ray ◽  
Gypsum Formation ◽  
Acid Washing ◽  
Hydrolysis Of

Over time, performance of tubular backpulse pressure filters in kraft mills deteriorates, even with regular acid washing. Unscheduled filter replacement due to filter plugging results in significant costs and may result in mill downtime. We identified acid-insoluble filter-plugging materials by scanning electron microscope/energy-dispersion X-ray spectroscopy (SEM/EDS) and X-ray diffraction (XRD) analysis in both polypropylene and Gore-Tex™ membrane filter socks. The major filter-plugging components were calcium sulfate (gypsum), calcium phosphate (hydroxylapatite), aluminosilicate clays, metal sulfides, and carbon. We carried out detailed sample analysis of both the standard acid-washing procedure and a modified procedure. Filter plugging by gypsum and metal sulfides appeared to occur because of the acid-washing procedure. Gypsum formation on the filter resulted from significant hydrolysis of sulfamic acid solution at temperatures greater than 130°F. Modification of the acid-washing procedure greatly reduced the amount of gypsum and addition of a surfactant to the acid reduced wash time and mobilized some of the carbon from the filter. With surfactant, acid washing was 95% complete after 40 min.

A study on using expanded perlite with hydroxyapatite: Reinforced bio-composites

2021 ◽  
pp. 095441192199656
Author(s):  
Erdoğan Karip ◽  
Mehtap Muratoğlu
Keyword(s):  
Body Fluid ◽  
Xrd Analysis ◽  
Cold Isostatic Pressing ◽  
Expanded Perlite ◽  
X Ray Diffraction ◽  
Pressing Method ◽  
X Ray ◽  
Infra Red ◽  
Ft Ir

People are exposed to different kinds of diseases or various accidents in life. Hydroxyapatite (HA) has been widely employed for bone treatment applications. In this study, HA was extracted from sheep bones. Bio-composites were doped with 1, 5, and 10 wt.% of expanded perlite and 5 wt.% of ZrO2–MgO-P2O5. The bio-composites were prepared by the cold isostatic pressing method (250 MPa) and sintered at 900°C for 1 h. In order to evaluate the characteristics of the bio-composites, microhardness, density, X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were carried out on them. Additionally, the specimens whose characteristics were determined were kept in synthetic body fluid (SBF), and their in vitro behavior was examined. As a result, it was observed that microhardness increased as both the weight and the grain size of the expanded perlite were increased. Calcium silicate, tri-calcium phosphate, and hydroxyapatite were observed in the XRD analysis of all samples, and the formation of apatite structures was increased by addition of ZrO2–MgO–P2O5.

scholarly journals Laser-Induced Deposition of Plasmonic Ag and Pt Nanoparticles, and Periodic Arrays

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 10
Author(s):  
Daria V. Mamonova ◽  
Anna A. Vasileva ◽  
Yuri V. Petrov ◽  
Denis V. Danilov ◽  
Ilya E. Kolesnikov ◽  
...  
Keyword(s):  
Substrate Surface ◽  
Pt Nanoparticles ◽  
Single Step ◽  
X Ray Diffraction ◽  
Ag Nps ◽  
X Ray ◽  
Periodic Arrays ◽  
Potential Applications ◽  
Surface Decoration ◽  
Wide Potential

Surfaces functionalized with metal nanoparticles (NPs) are of great interest due to their wide potential applications in sensing, biomedicine, nanophotonics, etc. However, the precisely controllable decoration with plasmonic nanoparticles requires sophisticated techniques that are often multistep and complex. Here, we present a laser-induced deposition (LID) approach allowing for single-step surface decoration with NPs of controllable composition, morphology, and spatial distribution. The formation of Ag, Pt, and mixed Ag-Pt nanoparticles on a substrate surface was successfully demonstrated as a result of the LID process from commercially available precursors. The deposited nanoparticles were characterized with SEM, TEM, EDX, X-ray diffraction, and UV-VIS absorption spectroscopy, which confirmed the formation of crystalline nanoparticles of Pt (3–5 nm) and Ag (ca. 100 nm) with plasmonic properties. The advantageous features of the LID process allow us to demonstrate the spatially selective deposition of plasmonic NPs in a laser interference pattern, and thereby, the formation of periodic arrays of Ag NPs forming diffraction grating

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