scholarly journals Effects of Partitioning Time and Temperature on the Microstructure and Mechanical Properties of a High Strength Microalloyed Steel

Author(s):  
ali almasi ◽  
abbas kianvash ◽  
abolfazl tutunchi

Abstract In the present study, in a quenching-partitioning (Q-P) process, the effects of partitioning time (Pt) and partitioning temperature (PT) on the mechanical and microstructural properties of a microalloyed Fe-0.21C-1.5Si-2.2Mn-0.054Al-0.08Ti steel were studied. The XRD and SEM results confirmed increases in retained austenite (γR) volume fraction (VγR) and (γR)carbon concentration by increasing Pt and PT. XRD patterns confirmed reduction in (VγR)by further increasing the Pt and PT over 500 sec and 390°C, respectively, due to super-saturation of austenite (γ) with carbon. PT of 390°C and Pt of 500 sec were recorded as the optimum values for PTs and Pts, which allowed the present steel to obtain higher formability and higher fracture strain characteristics, while retaining higher hardness and strength. The highest yield and tensile strength, hardness and fracture elongation were obtained for the sample partitioned at 390°C for about 500 sec, which were about 741MPa, 1366 MPa, 424 HV and 25.2 %, respectively.

Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 887
Author(s):  
Olli Oja ◽  
Ari Saastamoinen ◽  
Madan Patnamsetty ◽  
Mari Honkanen ◽  
Pasi Peura ◽  
...  

The intercritical annealing and isothermal bainitic processing response was studied for three Nb and V microalloyed Transformation-Induced Plasticity (TRIP)-assisted 980 MPa grade steels. Their mechanical and microstructural properties were compared to industrially produced TRIP 800 steel. Depending on the isothermal holding temperature and microalloying, the experimental steels reached properties comparable to the reference steel. The retained austenite content did not show direct correlation to elongation properties. Niobium was found to be more effective microalloying element than vanadium in increasing the elongation properties, which were investigated by measuring true fracture strain from tensile test specimens.


2018 ◽  
Vol 115 (3) ◽  
pp. 311 ◽  
Author(s):  
Ningbo Zhou ◽  
Fan Zhao ◽  
Yiqun Liu ◽  
Bo Jiang ◽  
Chaolei Zhang ◽  
...  

The transformation behavior and intragranular ferrite formation in V–Ti microalloyed steel with a nitrogen content of 0.005 wt.% and 0.015 wt.% are studied by the DIL 805A dilatometer. The results show that increasing the nitrogen content has no significant effect on AC1, AC3and MStemperature. However, the continuous cooling transformation (CCT) diagrams are shifted to left side. The minimum cooling rates of bainitc and martensitic transformation are increased from 3 °C/s to 5 °C/s and from 5 °C/s to 10 °C/s, respectively. (Ti, V)(C, N) particles on MnS is the nuclei of intragranular ferrite, and (1 0 0)(Ti, V)(C, N)and (1̅ 0 1̅α) are just misoriented by 6.7°. With the increase of nitrogen content, the number of intragranular ferrite is increased from 73 to 170 per · mm2. The volume fraction of intragranular ferrite is increased from 0.23%∼0.79% to 0.79%∼4.6% at cooling rate of 1 °C/s∼0.1 °C/s. According to the industrial production experiment, the toughness of forging crankshaft is improved by increasing the nitrogen content. It is benefit for achieving fair matching of high strength and high toughness of crankshaft.


Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2302 ◽  
Author(s):  
Yilin Wang ◽  
Huicheng Geng ◽  
Bin Zhu ◽  
Zijian Wang ◽  
Yisheng Zhang

The application of the quenching and partitioning (Q-P) process on advanced high-strength steels improves part ductility significantly with little decrease in strength. Moreover, the mechanical properties of high-strength steels can be further enhanced by the stepping-quenching-partitioning (S-Q-P) process. In this study, a two-stage quenching and partitioning (two-stage Q-P) process originating from the S-Q-P process of an advanced high-strength steel 30CrMnSi2Nb was analyzed by the simulation method, which consisted of two quenching processes and two partitioning processes. The carbon redistribution, interface migration, and phase transition during the two-stage Q-P process were investigated with different temperatures and partitioning times. The final microstructure of the material formed after the two-stage Q-P process was studied, as well as the volume fraction of the retained austenite. The simulation results indicate that a special microstructure can be obtained by appropriate parameters of the two-stage Q-P process. A mixed microstructure, characterized by alternating distribution of low carbon martensite laths, small-sized low-carbon martensite plates, retained austenite and high-carbon martensite plates, can be obtained. In addition, a peak value of the volume fraction of the stable retained austenite after the final quenching is obtained with proper partitioning time.


2021 ◽  
Vol 1016 ◽  
pp. 732-737
Author(s):  
Junya Kobayashi ◽  
Hiroto Sawayama ◽  
Naoya Kakefuda ◽  
Goroh Itoh ◽  
Shigeru Kuraoto ◽  
...  

Various high strength steel sheets for weight reduction and safety improvement of vehicles have been developed. TRIP-aided steel with transformation induced plasticity of the retained austenite has high strength and ductility. Conventional TRIP-aided steels are subjected to austempering process after austenitizing. Generally, elongation and formability of TRIP-aided steel are improved by finely dispersed retained austenite in BCC phase matrix. The finely dispersed retained austenite and grain refinement of TRIP-aided steel can be achieved by hot rolling with heat treatment. Therefore, the improvement of mechanical properties of TRIP-aided steel is expected from the manufacturing process with hot rolling and then isothermal transformation process. In this study, thermomechanical heat treatment is performed by combining hot rolling and isothermal holding as the manufacturing process of TRIP-aided steel sheets. The complex phase matrix is obtained by hot rolling and then isothermal holding. Although the hardness of the hot rolled and isothermal held TRIP-aided steel is decreased, the volume fraction of retained austenite is increased.


2017 ◽  
Vol 270 ◽  
pp. 239-245
Author(s):  
Dagmar Bublíková ◽  
Štěpán Jeníček ◽  
Kateřina Opatová ◽  
Bohuslav Mašek

Today’s advanced steels are required to possess high strength and ductility. This can be accomplished by producing appropriate microstructures with a certain volume fraction of retained austenite. The resulting microstructure depends on material’s heat treatment and alloying. High ultimate strengths and sufficient elongation levels can be obtained by various methods, including quenching and partitioning (Q&P process). The present paper introduces new procedures aimed at simplifying this process with the use of material-technological modelling. Three experimental steels have been made and cast for this investigation, whose main alloying additions were manganese, silicon, chromium, molybdenum and nickel. The purpose of manganese addition was to depress the Ms and Mf temperatures. The Q&P process was carried out in a thermomechanical simulator for better and easier control. The heat treatment parameters were varied between the sequences and their effect on microstructure evolution was evaluated. They included the cooling rate, partitioning temperature and time at partitioning temperature. Microstructures including martensite with strength levels of more than 2000 MPa and elongation of 10–15 % were obtained.


2021 ◽  
Vol 36 (16) ◽  
pp. 3167-3181
Author(s):  
M. R. Jones ◽  
F. W. DelRio ◽  
J. W. Pegues ◽  
P. Lu ◽  
R. Puckett ◽  
...  

Abstract Ni-based superalloys have been studied extensively due to their impressive mechanical properties, including strength and creep resistance at high temperatures. Growing interest surrounding additive manufacturing (AM) methods has led to recent investigations of alloys that are traditionally difficult to process, including Ni-based superalloys. Recent work has shown that AM methods enable high-throughput materials discovery and optimization of difficult- or impractical-to-process alloys, including those with high or even majority refractory element compositions. This work focuses on AM-enabled investigations of composition-dependent mechanical and microstructural properties for Ni–Nb binary alloys. Specifically, we report on the mechanical behavior of compositionally-graded NixNb1−x and uniform composition Ni59.5Nb40.5 specimens made with AM. The AM fabrication process resulted in extraordinarily high strength, attributed to the formation of a dual-phase microstructure consisting of δ-Ni3Nb and µ-Ni6Nb7 intermetallic compounds with nanostructured and multimodal grain size and eutectic lamellar spacing. Graphic Abstract


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