scholarly journals Pullout Bond Strength of Fiber Posts Luted to Different Depths and Submitted to Artificial Aging

2013 ◽  
Vol 38 (4) ◽  
pp. E128-E133 ◽  
Author(s):  
VC Macedo ◽  
NAY Souza ◽  
AL Faria e Silva ◽  
C Cotes ◽  
C da Silva ◽  
...  
Keyword(s):  
Bond Strength ◽  
Artificial Aging ◽  
Composite Resin ◽  
Thermomechanical Cycling ◽  
Mechanical Cycling ◽  
Fiber Posts ◽  
Relyx Unicem ◽  
Different Depths ◽  
Bond Strengths ◽  
Post Hoc

SUMMARY Introduction The extension of fiber post cementation often does not seem to influence the fracture resistance of restorations. This study evaluated the effects of cementation depths on the retention of fiber posts submitted to artificial aging. Methods One hundred and sixty bovine incisors were selected to assess post retention. Following endodontic treatment, the canals were flared with diamonds burs. Postholes were prepared in lengths of 5 or 10 mm, after which fiber posts were relined with composite resin and luted with RelyX ARC or RelyX Unicem. The samples were then submitted to thermal and/or mechanical cycling before testing their pullout bond strengths. Absence of cycling was used as a control. The results of each cement were submitted to two-way and post hoc Tukey tests (α=0.05). Results Independent of the aging protocol, a depth of 10 mm showed higher pullout bond strength than did 5 mm, except for RelyX Unicem without cycling. For RelyX ARC, thermomechanical cycling resulted in lower values than in the absence of cycling. Mechanical cycling alone promoted the highest bond strength when the posts were luted with RelyX Unicem. Conclusion The effect of artificial aging on the pullout bond strength is dependent on the type of material and the depth.

scholarly journals Reliability of Fiber Post Bonding to Root Canal Dentin After Simulated Clinical Function In Vitro

2012 ◽  
Vol 37 (4) ◽  
pp. 397-405 ◽  
Author(s):  
K Bitter ◽  
J Perdigão ◽  
M Exner ◽  
K Neumann ◽  
AM Kielbassa ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
The Other ◽  
Hybrid Layer ◽  
Resin Cements ◽  
Anterior Teeth ◽  
Fiber Posts ◽  
Relyx Unicem ◽  
Bond Strengths

SUMMARY The aim of this study was to investigate the effect of thermomechanical loading (TML) on the bond strength of fiber posts luted with three different resin cements. Sixty-six extracted human anterior teeth were endodontically treated and restored with fiber posts (RelyX Fiber Posts, 3M ESPE) using three commercially available resin cements and three corresponding core build-up materials (n=22 each): Panavia F 2.0/Clearfil DC Core Automix (Kuraray), Variolink II/Multicore Flow (Ivoclar Vivadent), and RelyX Unicem/Filtek Z250 (3M ESPE). Twelve specimens of each group received all-ceramic crowns and were subjected to TML. The other 10 specimens were stored in saline solution for 24 hours. The roots were sectioned and bond strength was measured using a push-out test. Adhesive interfaces of two specimens of each group subjected to TML were analyzed using field emission scanning electron microscopy (FESEM). Bond strengths of fiber posts were significantly affected by the type of resin cement (p<0.0005) and TML (p<0.0005; two-way analysis of variance). TML significantly reduced bond strengths for all materials ((6.0 (6.2) MPa)) compared with initial bond strengths ((14.9 (10.4) MPa)). RelyX Unicem resulted in significantly higher bond strengths before ((18.3 (10.3) MPa)) and after TML ((9.8 (7.5) MPa)) compared with the other materials (p<0.0005; Tukey HSD). Using FESEM, Variolink II and Panavia F demonstrated a hybrid layer partly detached from the underlying resin cement, whereas no hybrid layer was observed for RelyX Unicem. The decrease in bond strength after TML suggests that retention of fiber posts may be reduced after clinical function. Therefore, endodontically treated teeth that are restored using fiber posts may benefit from additional reinforcement via coronal restorations using adequate ferrules and/or adhesive techniques.

The Effect of Dentin Desensitizer on Shear Bond Strength of Conventional and Self-adhesive Resin Luting Cements After Aging

2011 ◽  
Vol 36 (5) ◽  
pp. 492-501 ◽  
Author(s):  
B Stawarczyk ◽  
R Hartmann ◽  
L Hartmann ◽  
M Roos ◽  
M Özcan ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Water Storage ◽  
Acrylic Resin ◽  
Luting Cements ◽  
Relyx Unicem ◽  
Aging Conditions ◽  
Post Hoc ◽  
The Impact ◽  
Panavia 21

SUMMARY This study tested the impact of Gluma Desensitizer on the shear bond strength (SBS) of two conventional (RelyX ARC, Panavia 21) and two self-adhesive (RelyX Unicem, G-Cem) resin luting cements after water storage and thermocycling. Human third molars (N=880) were embedded in acrylic resin. The buccal dentin was exposed. Teeth were randomly divided into four main groups, and the following cements were adhered: 1) RelyX ARC, 2) Panavia 21, 3) RelyX Unicem, and 4) G-Cem. In half of the teeth in each group, dentin was treated with Gluma Desensitizer. In the conventional cement groups, the corresponding etchant and adhesive systems were applied. SBS of the cements was tested after 1 hour (initial); at 1, 4, 9, 16, and 25 days of water storage; and at 1, 4, 9, 16, and 25 days of thermocycling. SBS data were analyzed by one-way analysis of variance (ANOVA); this was followed by the post hoc Scheffé test and a t-test. Overall, the highest mean SBS (MPa) was obtained by RelyX ARC (ranging from 14.6 ± 3.9 to 17.6 ± 5.2) and the lowest by Panavia 21 in combination with Gluma Desensitizer (ranging from 0.0 to 2.9 ± 1.0). All tested groups with and without desensitizer showed no significant decrease after aging conditions compared with baseline values (p>0.05). Only the Panavia 21/Gluma Desensitizer combination showed a significant decrease after 4 days of thermocyling compared with initial values and 1 day thermocycling. Self-adhesive cements with Gluma Desensitizer showed increased SBS after aging conditions (ranging from 7.4 ± 1.4 to 15.2 ± 3) compared with groups without desensitizer (ranging from 2.6 ± 1.2 to 8.8 ± 2.9). No cohesive failures in dentin were observed in any of the test groups. Although self-adhesive cements with and without desensitizer presented mainly adhesive failures after water storage (95.8%) and thermocyling (100%), conventional cement (RelyX ARC) showed mainly mixed failures (90.8% and 89.2%, after water storage and thermocyling, respectively). Application of the Gluma Desensitizer to dentin before cementation had a positive effect on the SBS of self-adhesive cements.

Effects of Multipurpose, Universal Adhesives on Resin Bonding to Zirconia Ceramic

2015 ◽  
Vol 40 (1) ◽  
pp. 55-62 ◽  
Author(s):  
J-H Kim ◽  
S-Y Chae ◽  
Y Lee ◽  
G-J Han ◽  
B-H Cho
Keyword(s):  
Bond Strength ◽  
Artificial Aging ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Single Bond ◽  
Surface Conditioning ◽  
Universal Adhesives ◽  
Bond Strengths ◽  
Microshear Bond Strength ◽  
Composite Cylinders

SUMMARY This study evaluated the effects of single-bottle, multipurpose, universal adhesives on the bond strength of resin cement to zirconia ceramic. Polished zirconia ceramic (Cercon base) discs were randomly divided into four groups (n=40) according to the applied surface-conditioning agent: Single Bond 2, Single Bond Universal, All-Bond Universal, and Alloy Primer. Cured composite cylinders (Ø 0.8 mm × 1 mm) were cemented to the conditioned zirconia specimens with resin cement (RelyX ARC). The bonded specimens were subjected to a microshear bond-strength test after 24 hours of water storage and after 10,000 cycles of thermocycling. The surface-conditioning agent significantly influenced the bond strength (p<0.05). Single Bond Universal showed the highest initial bond strength (37.7 ± 5.1 MPa), followed by All-Bond Universal (31.3 ± 5.6 MPa), Alloy Primer (26.9 ± 5.1 MPa), and Single Bond 2 (8.5 ± 4.6 MPa). Artificial aging significantly reduced the bond strengths of all the test groups (p<0.05). After 10,000 cycles of thermocycling, All-Bond Universal showed the highest bond-strength value (26.9 ± 6.4 MPa). Regardless of artificial aging, Single Bond Universal and All-Bond Universal showed significantly higher bond strengths than Alloy Primer, a conventional metal primer.

scholarly journals Adhesion of Two Bonding Systems to Air-Abraded or Bur-Abraded Human Enamel Surfaces

2008 ◽  
Vol 02 (03) ◽  
pp. 167-175 ◽  
Author(s):  
Abdulkadir Sengun ◽  
Hasan Orucoglu ◽  
Ilknur Ipekdal ◽  
Fusun Ozer
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
In Vitro Study ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Bonding Performance ◽  
Human Enamel ◽  
Bond Strengths ◽  
Bonding Systems

ABSTRACTObjectives: The purpose of this in vitro study was to evaluate whether mechanical alteration of the enamel surfaces with air abrasion and bur abrasion techniques could enhance the bonding performance of a three step and a self etching adhesive resin systems to enamel.Methods: 126 extracted lower human incisor teeth were used. The teeth were divided into three groups including 40 teeth each. First group; teeth were used as control and no preparation was made on enamel surfaces, 2nd group; outer enamel surfaces were air abraded, 3rd group; outer enamel surfaces were abraded mechanically with a diamond fissure bur. Cylinder composite resin blocks were bonded to the buccal enamel surfaces with two bonding systems (20 specimens in each group). Bond strengths to enamel surfaces were measured at a cross-head speed of 1 mm/min. The data were analyzed by ANOVA and Duncan Tests. To examine interface composite resin/enamel surfaces at scanning electron microscopy, remaining 6 teeth were used. Fracture analysis was performed using an optical stereomicroscope.Results: Bond strengths values of Solid Bond were significantly higher than bond strengths of Clearfil SE Bond for all types of enamel (P<.05). Shear bond strength values obtained with Solid Bond (three step system) to three types of enamel surfaces [air-abraded (30.25±7.00 MPa), bur-abraded (29.07±3.53 MPa), control (31.74±7.35 MPa)] were close to each other (P>.05). The macroscopic mode of failures for bonding systems, SB and SE Bond appeared to be adhesive and cohesive in nature.Conclusions: In order to get better bond strength values with self etching systems, it is advisable to prepare enamel surfaces with bur or air abrasion, but it enamel preparation is not necessary for three step systems. (Eur J Dent 2008;2:167-175)

Effect of Artificial Aging and Surface Treatment on Bond Strengths to Dental Zirconia

2013 ◽  
Vol 38 (2) ◽  
pp. 168-176 ◽  
Author(s):  
J Perdigão ◽  
SD Fernandes ◽  
AM Pinto ◽  
FA Oliveira
Keyword(s):  
Surface Treatment ◽  
Artificial Aging ◽  
Testing Machine ◽  
Significance Level ◽  
Diamond Blade ◽  
Universal Testing ◽  
Bond Strengths ◽  
The Mean ◽  
Post Hoc ◽  
Adhesive Cement

SUMMARY The objective of this project was to study the influence of artificial aging and surface treatment on the microtensile bond strengths (μTBS) between zirconia and a phosphate monomer–based self-adhesive cement. Thirty zirconia disks (IPS e.max ZirCAD, Ivoclar Vivadent) were randomly assigned to two aging regimens: AR, used as received, which served as a control, and AG, artificial aging to simulate low-temperature degradation. Subsequently, the disks of each aging regimen were assigned to three surface treatments: NT, no surface treatment; CO, surface silicatization with CoJet sand (3M ESPE); and ZP, zirconia surface treated with Z-Prime Plus (Bisco Inc). Thirty discs were made of Filtek Z250 (3M ESPE) composite resin and luted to the zirconia discs using RelyX Unicem (3M ESPE). The specimens were sectioned with a diamond blade in X and Y directions to obtain bonded beams with a cross-section of 1.0 ± 0.2 mm. The beams were tested in tensile mode in a universal testing machine at a speed of 0.5 mm/min to measure μTBS. Selected beams were selected for fractographic analysis under the SEM. Statistical analysis was carried out with two-way analysis of variance and Dunnett T3 post hoc test at a significance level of 95%. The mean μTBS for the three AR subgroups (AR-NT, AR-CO, and AR-ZP) were significantly higher than those of the corresponding AG groups (p&lt;0.0001). Both AR-CO and AR-ZP resulted in statistically significant higher mean bond strengths than the group AR-NT (p&lt;0.006 and p&lt;0.0001, respectively). Both AG-CO and AG-ZP resulted in statistically significant higher mean bond strengths than the group AG-NT (both at p&lt;0.0001). Overall, AG decreased mean μTBS. Under the SEM, mixed failures showed residual cement attached to the zirconia side of the beams. CO resulted in a characteristic roughness of the zirconia surface. AR-ZP was the only group for which the amount of residual cement occupied at least 50% of the interface in mixed failures.

scholarly journals Adhesive Durability Inside the Root Canal Using Self-adhesive Resin Cements for Luting Fiber Posts

2017 ◽  
Vol 42 (6) ◽  
pp. E167-E176 ◽  
Author(s):  
K Bitter ◽  
A Maletic ◽  
K Neumann ◽  
L Breschi ◽  
G Sterzenbach ◽  
...  
Keyword(s):  
Bond Strength ◽  
Root Canal ◽  
Fiber Post ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Fiber Posts ◽  
Silver Deposits ◽  
Bond Strengths ◽  
One Year ◽  
Push Out

SUMMARY Objectives: The aim of the study was to investigate the effects of various self-adhesive resin cements on the push-out bond strengths and nanoleakage expression at the luting interfaces of fiber posts immediately and after one year of aging. Methods and Materials: One hundred forty-four extracted human anterior teeth were endodontically treated. After post space preparation, fiber posts were luted using five commercially available self-adhesive resin (SAR) cements and a core build-up material applied with a self-etch adhesive (BF: Bifix SE/Rebilda Post, VOCO; CSA: Clearfil SA Cement/Rely X Fiber Post, 3M ESPE; RX: RelyX Unicem 2/Rely X Fiber Post, 3M ESPE; SPC: Speed Cem/FRC Postec, Ivoclar Vivadent; SMC: Smart Cem/X Post, Dentsply; RB: Rebilda DC-Futurabond/Rebilda Post; n=22). For each group, half of the specimens were subjected to thermocycling (TC) (5°C-55°C, 10,000 cycles) and stored humid for one year at 37°C. Push-out bond strength data of six slices (thickness 1 mm) per root and nanoleakage expression of representative specimens were evaluated after 24 hours (baseline) and after TC and storage for one year (aging), respectively. Results: Bond strength differed significantly among resin cements (p&lt;0.0005) and the location inside the root canal (p&lt;0.0005), but not by aging (p=0.390; repeated-measures analysis of variance). SMC (14.6±5.8 MPa) and RX (14.1±6.8 MPa) revealed significantly higher bond strength compared to BF (10.6±5.4 MPa) and RB (10.0±4.6 MPa) but differed not significantly from SPC (12.8±4.8) MPa; CSA (6.1±4.6 MPa) revealed significantly lower bond strength compared to all other investigated materials (p&lt;0.05; Tukey Honestly Significantly Different). Qualitative nanoleakage analysis revealed more silver deposits at the interface in all groups after aging. For CSA, a large amount of silver deposits inside the cement was also observed at baseline and after aging. Conclusions: Fiber post luting using SAR cements demonstrated reliable bond strengths. Product-specific differences and initial degradation effects could be demonstrated.

A Fluoride-containing Composite Resin—An In Vitro Study of a New Material for Orthodontic Bonding

1989 ◽  
Vol 16 (3) ◽  
pp. 207-212 ◽  
Author(s):  
P. A. Cook ◽  
C. C. Youngson
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
Glass Ionomer Cement ◽  
In Vitro Study ◽  
The Other ◽  
Glass Ionomer ◽  
New Material ◽  
Bond Strengths ◽  
Ionomer Cement

The shear/peel bond strength of a new material, a ‘hybrid’ of a composite resin and a glass ionomer cement, was compared in vitro with the bond strengths of a composite resin and of a glass ionomer cement. The new material had a significantly greater bond strength than the other materials tested and its properties were very similar to the composite resin. Unlike the glass ionomer cement, etching of the enamel before applying the adhesive is required. The clinical indications for using this new cement are discussed.

scholarly journals Effects of Contamination by Hemostatic Agents and Use of Cleaning Agent on Etch-and-Rinse Dentin Bond Strength

2016 ◽  
Vol 27 (6) ◽  
pp. 688-692 ◽  
Author(s):  
César Rogério Pucci ◽  
Rodrigo Maximo de Araújo ◽  
Ana Julia Farias de Lacerda ◽  
Mirella Anjos de Souza ◽  
Maria Filomena Rocha Lima Huhtala ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Control Group ◽  
Hemostatic Agents ◽  
Diamond Bur ◽  
Mechanical Cycling ◽  
Etch And Rinse ◽  
Post Hoc ◽  
Push Out ◽  
Cleaning Protocol

Abstract The aim of this study was to evaluate the influence of contamination by hemostatic agents and rinsing with chlorhexidine on bond strength between dentin and resin composite. Ninety-six bovine teeth were sectioned to expose a flat dentin surface area. A standardized cavity with 2.0 mm in thickness, superficial diameter of 4.0 mm and bottom diameter of 3.0 mm was prepared with a diamond bur in each dentin specimen. The teeth were divided into four groups according to the hemostatic employed: G1: control; G2: use of ViscoStat, Ultradent; G3: Hemosthasegel, FGM; and G4: Hemostop, Dentsply. The groups were divided into two subgroups according to the cleaning protocol method (n=12): A: without any further cleaning; and B: cleaning with chlorhexidine at 0.2%. All cavities were filled using a dentin adhesive and a resin composite, following the manufacturer's instructions. After 24 h, the specimens were aged by thermal and mechanical cycling. The bond strength was determined by the push out bond test (MPa), Statistical analysis was performed using two-way ANOVA and Tukey test (p<0.05). Statistically significant differences were detected among all groups treated with hemostatic agents and the control group. The post-hoc test showed that cleaning the cavity with chlorhexidine significantly improves the bond strength between dentin and resin composite. Our results suggested that the use of chlorhexidine can reestablish the bond strength between dentin and resin composite when a hemostatic agent was applied.

scholarly journals The Effects of Cavity Preparation and Composite Resin on Bond Strength and Stress Distribution Using the Microtensile Bond Test

2018 ◽  
Vol 43 (1) ◽  
pp. 81-89 ◽  
Author(s):  
SSL Braga ◽  
LRS Oliveira ◽  
RB Rodrigues ◽  
AA Bicalho ◽  
VR Novais ◽  
...  
Keyword(s):  
Stress Distribution ◽  
Bond Strength ◽  
Failure Modes ◽  
Composite Resin ◽  
Shrinkage Stress ◽  
Cavity Preparation ◽  
Chi Square ◽  
Chi Square Test ◽  
Post Hoc ◽  
Made In

SUMMARY Objectives: To evaluate the effect of flowable bulk-fill or conventional composite resin on bond strength and stress distribution in flat or mesio-occlusal-distal (MOD) cavity preparations using the microtensile bond strength (μTBS) test. Methods: Forty human molars were divided into two groups and received either standardized MOD or flat cavity preparations. Restorations were made using the conventional composite resin Z350 (Filtek Z350XT, 3M-ESPE, St Paul, MN, USA) or flowable bulk-fill (FBF) composite resin (Filtek Bulk Fill Flowable, 3M-ESPE). Postgel shrinkage was measured using the strain gauge technique (n=10). The Z350 buildup was made in two increments of 2.0 mm, and the FBF was made in a single increment of 4.0 mm. Six rectangular sticks were obtained for each tooth, and each section was used for μTBS testing at 1.0 mm/min. Polymerization shrinkage was modeled using postgel shrinkage data. The μTBS data were analyzed statistically using a two-way analysis of variance (ANOVA), and the postgel shrinkage data were analyzed using a one-way ANOVA with Tukey post hoc test. The failure modes were analyzed using a chi-square test (α=0.05). Results: Our results show that both the type of cavity preparation and the composite resin used affect the bond strength and stress distribution. The Z350 composite resin had a higher postgel shrinkage than the FBF composite resin. The μTBS of the MOD preparation was influenced by the type of composite resin used. Irrespective of composite resin, flat cavity preparations resulted in higher μTBS than MOD preparations (p&lt;0.001). Specifically, in flat-prepared cavities, FBF composite resin had a similar μTBS relative to Z350 composite resin. However, in MOD-prepared cavities, those with FBF composite resin had higher μTBS values than those with Z350 composite resin. Adhesive failure was prevalent for all tested groups. The MOD preparation resulted in higher shrinkage stress than the flat preparation, irrespective of composite resin. For MOD-prepared cavities, FBF composite resin resulted in lower stress than Z350 composite resin. However, no differences were found for flat-prepared cavities. Conclusions: FBF composite resin had lower shrinkage stress than Z350 conventional composite resin. The μTBS of the MOD preparation was influenced by the composite resin type. Flat cavity preparations had no influence on stress and μTBS. However, for MOD preparation, composite resin with higher shrinkage stress resulted in lower μTBS values.

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