scholarly journals Optimization of Emprit Ginger Oil Yield through Operating Temperature with Microwave Ultrasonic Steam Diffusion Method

2022 ◽  
Vol 2 (2) ◽  
pp. 83
Author(s):  
Gilang Maulana Alif ◽  
Irfiani Nurul Mawaddah ◽  
Fikaputri Rohmatul ◽  
Zel Andesra
Keyword(s):  
Essential Oil ◽  
Solid Phase ◽  
Extraction Process ◽  
High Energy ◽  
Diffusion Method ◽  
Extraction Temperature ◽  
Long Time ◽  
Microwave Distillation ◽  
Time Required ◽  
The Cost

<h1><em>Essential oil of ginger (zingiberene oil (C<sub>15</sub>H<sub>24</sub>)) is one of the diversified products that have high selling value. Most of the essential ginger products available in the market haven’t allow the standard export products, based on the Essential Oil Association of USA (EOA) standards. The low quality of ginger essential oil products is due to its production process with conventional distillation. This method is most often used because it is easy to operate and produce a good enough product but takes a long time. Another extract method developed is Microwave Distillation and Simultaneous Solid-Phase Microexctraction (MDSS- PM). In this method the time required is faster but the resulting product is not as good as Hydrodistillation product and requires high energy. In this research, ginger extraction process using Microwave Distillation method is modified by ultrasonic addition technique (MUSDf). The variables used in this research are Steam Diffusion (SDF) method, Microwave Exctraction (ME), Microwave Steam Diffusion (MSDf), Microwave Ultrasonic Steam Diffusion (MUSDf) with 30, 50,70, 90 and 110 minutes extension time and extraction temperature variations of 90, 95, 100 and 1050C. From the result of the research, it is found that the best method to produce ginger oil extract is by using MUSDf method with yield of 0.952%, zingiberene level is 6.38%, and the cost per gram of oil is Rp 17,964.</em></h1>

Design Research on the Composite Process of Consecutive Perforation-Strong Pulse Fracturing for Multiple Oil Layers and Thick Interlayer

2012 ◽  
Vol 482-484 ◽  
pp. 343-346
Author(s):  
Jin Jun Wu ◽  
Li Cai Liu ◽  
Guo Hua Zhao ◽  
Xiao San Chu
Keyword(s):  
Design Research ◽  
High Energy ◽  
Oil Fields ◽  
Construction Technology ◽  
Oil Companies ◽  
Test Application ◽  
Long Time ◽  
Single Well ◽  
The Cost ◽  
Production Period

Currently, most of Chinese oil companies have getting in the later production period, the oil wells are processed frequently and the cost is increasing. In view of the higher problems existed popular in the oil fields such as multiple layers, big interlayer, the technology composited perforation and high energy gas fracturing has to construct with every layer alone, operate long time, cost high. The author puts forward the design research on the composite process of consecutive perforation-strong pulse fracturing for multiple oil layers and thick interlayer This paper introduces the basic design principle and technology method. The design is realized by using the technology of the perforation-symmetrical overpressure fracturing technology, the multi-pulse multistage fracturing, to efficiently guarantee the effect of perforating and pulse fracturing in every layer. The designed multistage detonating device makes the once completed construction technology used in the single well of the multiple oil layers with big interlayer come true. The field test application has gained good effects, greatly reduced the construction cost, and also promoted the application and generalization of the technology composited perforation and high energy gas fracturing.

The Influence of Purge Times on the Yields of Essential Oil Components Extracted from Plants by Pressurized Liquid Extraction

2014 ◽  
Vol 97 (5) ◽  
pp. 1310-1316 ◽  
Author(s):  
Dorota Wianowska
Keyword(s):  
Essential Oil ◽  
Extraction Process ◽  
Liquid Extraction ◽  
Time Dependent ◽  
Pressurized Liquid Extraction ◽  
Thymus Vulgaris ◽  
Extraction Temperature ◽  
Extraction Ability ◽  
Oil Components ◽  
Rosmarinus Officinalis L

Abstract The influence of different purge times on the yield of the main essential oil constituents of rosemary (Rosmarinus officinalis L.), thyme (Thymus vulgaris L.), and chamomile (Chamomilla recutita L.) was investigated. The pressurized liquid extraction process was performed by applying different extraction temperatures and solvents. The results presented in the paper show that the estimated yield of essential oil components extracted from the plants in the pressurized liquid extraction process is purge time-dependent. The differences in the estimated yields are mainly connected with the evaporation of individual essential oil components and the applied solvent during the purge; the more volatile an essential oil constituent is, the greater is its loss during purge time, and the faster the evaporation of the solvent during the purge process is, the higher the concentration of less volatile essential oil components in the pressurized liquid extraction receptacle. The effect of purge time on the estimated yield of individual essential oil constituents is additionally differentiated by the extraction temperature and the extraction ability of the applied solvent.

scholarly journals Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction

2019 ◽  
Vol 14 (5) ◽  
pp. 1934578X1984272 ◽  
Author(s):  
Tomáš Bajer ◽  
Jakub Šulc ◽  
Karel Ventura ◽  
Petra Bajerová
Keyword(s):  
Extraction Method ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Extraction Process ◽  
Volatile Components ◽  
Extraction Temperature ◽  
Stem Wood ◽  
Wide Range ◽  
Volatile Profiles

A method for isolation of volatile compounds from samples of stem wood by solid-phase microextraction was developed. The extraction method was optimized using a central composite design approach. Extraction temperature and extraction time were optimized in the ranges of 40°C to 120°C and 10 to 90 minutes, respectively. Final extraction method was combined with GC-MS for separation and identification of volatile components of wood samples of seven tree species, commonly occurring in Central Europe. All of them were deciduous (acacia, alder, beech, elm, larch, maple, and oak). In total 185 organic compounds were identified in volatile profiles of all the samples by the developed method. To facilitate the evaluation of the suitability of the proposed method for extraction of different compound types, all identified compounds were categorized into 16 groups. Percentage of compound groups in volatile profiles of individual wood samples shows that the developed method is suitable for evaluation of a wide range of volatile components from stem wood.

scholarly journals Optimization of Essential Oil Extraction Process of White Pepper (Piper nigrum L.) Harvested in Phu Quoc Island, Kien Giang Province, Vietnam

2020 ◽  
Vol 32 (11) ◽  
pp. 2707-2712
Author(s):  
Thien Hien Tran ◽  
Thi Cam Quyen Ngo ◽  
Hoang Duy Ngo ◽  
Nguyen Huu Thuan Anh ◽  
Ton Nu Thuy An ◽  
...  
Keyword(s):  
Essential Oil ◽  
Extraction Process ◽  
Black Pepper ◽  
Oil Extraction ◽  
Extraction Time ◽  
Gas Chromatography Mass Spectrometry ◽  
Piper Nigrum ◽  
Extraction Temperature ◽  
Green Pepper ◽  
White Pepper

Vietnam is a leading producer and exporter of products harvested from plants of the family Piperaceae such as green pepper, black pepper, red pepper and white pepper. In this study, an attempt is made to examine the essential oil extraction process with the material of white pepper grown and harvested in Phu Quoc island, Vietnam. To maximize essential oil production, three factors consisting the ratio of materials and solvents, extraction time and extraction temperature were selected and optimized. The surface response methodology optimization resulted the highest yield of 3.6%, achieved at the ratio of material and water ratio of 1:20 g/g, extraction time of 96 min and at 130 ºC. A high F values, low P values (< 0.0001), the determination coefficient (R2 = 0.9993) and a non-significant lack of fit suggested a strong correlation between actual and predicted values of the responses. The essential oil obtained was determined for chemical composition by gas chromatography-mass spectrometry (GC-MS) method. The GC-MS results showed that major constituents existing in the oil sample were limonene, 3-carene, sabinene, β-pinene, α-pinene and α-phellandrene, accounting for 27.059, 23.345, 17.903, 9.996, 5.167 and 4.588%, respectively.

scholarly journals THE EXTRACTION OF NATURAL DYES FROM JACKFRUIT WOOD WASTE (Artocarpus Heterophyllus Lamk) WITH WATER SOLVENT BY USING THE MICROWAVE METHOD

2018 ◽  
Vol 7 (2) ◽  
pp. 128-135
Author(s):  
Selfina Gala ◽  
Mahfud Mahfud ◽  
Sumarno Sumarno ◽  
Lailatul Qadariyah
Keyword(s):  
Structural Damage ◽  
Extraction Process ◽  
Natural Dyes ◽  
Wood Waste ◽  
Extraction Time ◽  
Process Technology ◽  
Water Solvent ◽  
Long Time ◽  
Time Required ◽  
Optimum Extraction

Currently, exploration of natural dyes is increasingly being activated and developed, especially to find natural sources of dyes from different plant species and also to develop natural dyestuff extraction process technology for textile applications. During this natural dye extraction process is done by conventional methods that require a long time and a large amount of solvent. Therefore, it is a necessary alternative to the use of "green techniques" are economical in its use. In this research, extraction of Jackfruit wood waste with the microwave by studying the extraction time required to produce the optimum yield and comparing with the conventional method (heat-reflux extraction). Both of these methods use water solvent. On the microwave-assisted extraction, the optimum extraction time at 30 minutes with the acquisition yield of 3.14% (microwave power 400 watt, the ratio of material to solvent 0.02 g/mL). whereas extraction with heat-reflux method showed the optimum extraction time of 180 minutes with a yield of 3.50%. Identification of groups of pigments contained in the Jackfruit wood waste is known categories tannins, flavonoids, and quinones. Fourier Transform Infrared Spectroscopy was used to identify the major chemical groups in the extracted dye. Description of the effects of extraction with microwave and conventional, structural damage shown in a solid surface material using by Scanning Electron Microscopy. Further, to test the application on the fabric dyeing.

scholarly journals Somatic Embryogenesis in Commercial Crops—An Overview

HortScience ◽  
1997 ◽  
Vol 32 (3) ◽  
pp. 549D-549
Author(s):  
Joseph Thomas ◽  
D. Sreedhar ◽  
S. Murali ◽  
S. Jose ◽  
K.Gopal Krishnan ◽  
...  
Keyword(s):  
Somatic Embryogenesis ◽  
Commercial Application ◽  
Free Living ◽  
Leaf Stage ◽  
Mature Embryos ◽  
Major Constraint ◽  
Long Time ◽  
Time Required ◽  
The Cost

Many researchers regard somatic embryogenesis as a system of choice for in vitro propagation of superior varieties of crops such as coffee, mango, datepalm, and rose. While there are advantages, commercialization has not been possible so far in coffee, mango, and rose. The work highlights some reasons for this and feasible alternatives. We have established somatic embryogenesis in four elite Indian arabica coffee genotypes. Plantlets (3500) of all the four varieties are now being field-evaluated. The cost of producing these propagules is 15 times the seedling cost at present. A major constraint is the long time (6 months) needed to reach the five-leaf stage in vitro prior to release for acclimatization. This period can be reduced to 2 months using exvitro development after the two leaf stage. There are many reports of somatic embryogenesis in mango. Results on establishing free-living plantlets have not been encouraging.We found a number of abnormalities in the shape of the somatic embryos in cv. Rumani. However, except for the “rod”-shaped ones (that lacked cotyledonary expansion), all embryos germinated satisfactorily (75% rooting).We have encouraging results in reducing the time required to generate suitable plantlets for field acclimatization and in standardizing the procedures for grafting. Our laboratory has developed methods for ex vitro germination of mature embryos in datepalm,which yield more numbers of free-living plantlets (50%–60%) in only 3 months with an average of four leaves per plant. This compared favorably with in vitro germination that takes 6 months and produces plantlets with one or two leaves only. A novel protocol for obtaining somatic embryogenesis in rose from petal derived calli was developed by us (Murali et al., 1996). The number of embryos induced was too low for commercial application. [Murali et al., 1996. Euphytica 91:271–275].

scholarly journals Yield Optimization and Supercritical CO2 Extraction of Essential Oil from Jasmine Flower

2019 ◽  
Vol 19 (2) ◽  
pp. 479
Author(s):  
Hesham Hussein Rassem ◽  
Abdurahman Hamid Nour ◽  
Rosli Mohammad Yunus ◽  
Yasmeen Hafiz Zaki ◽  
Hybat Salih Mohamed Abdlrhman
Keyword(s):  
Essential Oil ◽  
Oil Recovery ◽  
Chemical Compounds ◽  
Extraction Process ◽  
Gas Chromatography Mass Spectrometry ◽  
Chemical Compositions ◽  
Extraction Temperature ◽  
Optimal Conditions ◽  
Yield Optimization ◽  
Extraction Parameters

Supercritical fluid extraction (SFE) is an innovation that permits extraction of an extensive variety of different chemical composition from the plant grids. Extraction of essential oil from Jasmine flower was tentatively carried out using the supercritical CO2 technique. The effect of extraction parameters which include pressure (100–300 bar) and temperature (300–350 K) on the oil recovery was explored. The extraction process was optimized using the response surface methodology (RSM). At the SFE optimal conditions, the chemical compositions of the extracted oil were examined using gas chromatography-mass spectrometry (GC-MS) analysis. The obtained result reflected that the optimal yield of oil from Jasmine flower was 12.18% mg oil extracted/100 g dry flower, which was achieved through an SFE optimal conditions of pressure at 200 bar and extraction temperature at 325 K. A total number of six chemical compounds were tentatively identified in the Jasmine flower extracted oil at the optimal SFE conditions.

Production and Chemical Compounds of Gaharu Extract by Using Supercritical Fluid Extraction (SFE) of Unsoaked Gaharu at Different Pressure

2015 ◽  
Vol 1115 ◽  
pp. 337-340
Author(s):  
Mohd Radzi Haji Che Daud ◽  
Huzaifah Hamdan
Keyword(s):  
Essential Oil ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Chemical Compounds ◽  
Extraction Process ◽  
World Market ◽  
Gas Chromatography Mass Spectrometry ◽  
Fluid Extraction ◽  
Three Samples ◽  
Long Time

Aquilaria species from the family of Thymelaeceae are the main source of gaharu, which has been classified as one of the most highly valuable, non-timber products in the world market. Currently, the method used for extracting gaharu essential oil is by using hydrodistillation. However, this method is inefficient where it produced low yield of oil with long time of extraction and thus increasing the production cost. To overcome this problem, the extraction of gaharu essential oil using Supercritical Fluid Extraction (SFE) with pressure 20MPa, 30MPa and 40MPa at 65 °C for 2 hours was studied. Result obtained after 2 hours of experiment was 0.6% of yield, which was higher compared to 0.2% yield of gaharu essential oil obtained via 3 days of hydrodistillation. After an extraction process, the product will be analyzed by using Gas Chromatography-Mass Spectrometry (GC-MS) to determine the chemical compounds and composition in the Gaharu SFE’s extract. Over eighteen to thirty-one compounds were identified in SFE extract compared with fifty-five identified in the hydrodistillated oil. The mutual occurrence of chemical compounds in all three samples in SFE was dimethyl phthalate, 8-epi-.gama.-eudesmol, diethyl Phthalate and 2-3-Butanediol. In comparison, the major compounds identified in hydrodistillated oil were 4-phenyl-2-butanone, jinkoh-eremol and α-guaiene (Saiful Nizam & Mashitah, 2010). There were certain aromatic sesquiterpenes compounds that were identified in this study, such as Globulol, Alloaromadendrene Naphthalene, 10s, 11s-Himachala-3(12), 4-diene, .delta.-Selinene and (-) - Aristolene.

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