scholarly journals Strain Analysis on Electrochemical Failures of Nanoscale Silicon Electrode Based on Three-Dimensional In Situ Measurement

2020 ◽  
Vol 10 (2) ◽  
pp. 468 ◽  
Author(s):  
Zhifeng Qi ◽  
Zhongqiang Shan ◽  
Weihao Ma ◽  
Linan Li ◽  
Shibin Wang ◽  
...  
Keyword(s):  
Silicon Film ◽  
Three Dimensional ◽  
Strain Analysis ◽  
Image Correlation ◽  
Mechanical Parameters ◽  
Stress Strain ◽  
Full Field ◽  
Battery Capacity

Nanoscale silicon film electrodes in Li-ion battery undergo great deformations leading to electrochemical and mechanical failures during repeated charging-discharging cycles. In-situ experimental characterization of the stress/strain in those electrodes still faces big challenges due to remarkable complexity of stress/strain evolution while it is still hard to predict the association between the electrode cycle life and the measurable mechanical parameters. To quantificationally investigate the evolution of the mechanical parameters, we develop a new full field 3D measurement method combining digital image correlation with laser confocal profilometry and propose a strain criterion of the failure based on semi-quantitative analysis via mean strain gradient (MSG). The experimental protocol and results illustrate that the revolution of MSG correlates positively with battery capacity decay, which may inspire future studies in the field of film electrodes.

Novel Methods for Assessment of Three-Dimensional Constitutive Properties for Composites

2010 ◽  
Vol 452-453 ◽  
pp. 401-404 ◽  
Author(s):  
Paige Carpentier ◽  
Andrew Makeev
Keyword(s):  
Polymer Matrix Composites ◽  
Three Dimensional ◽  
Image Correlation ◽  
Stress Strain ◽  
Complex Deformation ◽  
Deformation And Failure ◽  
Full Field ◽  
Short Beam ◽  
Beam Shear ◽  
Constitutive Properties

Accurate three-dimensional stress-strain constitutive properties are essential for understanding of complex deformation and failure mechanisms for glass-fiber and carbon-fiber reinforced polymer-matrix composites. A large number of different methods and specimen types, which are currently required to generate three-dimensional allowables for structural design, slow down material characterization. Also, some of the material constitutive properties are never measured due to prohibitive cost of the specimens needed. This work shows that simple short-beam shear specimens are well-suited for measurement of 3D constitutive properties for composite systems. In particular, a methodology to measure tensile and compressive material properties, generate shear stress-strain curves and measure the shear strength in a simple short beam shear test will be presented. The methodology is based on the Digital Image Correlation (DIC) full-field deformation measurement. Short-beam and curved-beam tests are accomplished to generate 3D stress-strain response for glass/epoxy and carbon/epoxy tape composite material systems. Accuracy of constitutive properties is also verified using standard methods and data available in the public domain.

scholarly journals In Situ Creep Behavior Characterization of Single Crystal Superalloy by UV-DIC at 980 °C

Coatings ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 598
Author(s):  
Yong Shang ◽  
Yali Dong ◽  
Yanling Pei ◽  
Chaoli Ma ◽  
Shusuo Li ◽  
...  
Keyword(s):  
Single Crystal ◽  
Creep Behavior ◽  
Creep Deformation ◽  
Image Correlation ◽  
Surface Pattern ◽  
Full Field ◽  
Uv Imaging ◽  
65 H

High temperature creep resistance is a critical characteristic of Ni-based single crystal (SX) superalloys. In this work, the creep behavior of a Ni-based SX superalloy was in situ characterized at 980 °C by ultraviolet (UV) imaging combined two-dimensional digital image correlation (DIC) in vacuum environment. The surface pattern was fabricated to maintain stable over 65 h at 980 °C. The pattern images captured by UV imaging were analyzed using mean gray value and the full-field strain map of creep deformation was obtained. A laser displacement senor (LDS) was employed for measuring the creep strain on the specimen for comparison. The creep deformation result shows a good agreement between DIC and LDS, the microstructure of the different creep areas on the specimens also demonstrate that the results of DIC are reliable. The in situ creep characterization by UV-DIC shows a great potential for investigating creep behaviors at high temperatures.

scholarly journals IN SITU CHARACTERIZATION OF FIBER-MATRIX INTERFACE DEBONDING VIA FULL-FIELD MEASUREMENTS

2021 ◽  
Author(s):  
ROBERT LIVINGSTON ◽  
BEHRAD KOOHBOR
Keyword(s):  
Field Measurements ◽  
Image Correlation ◽  
Interface Debonding ◽  
Matrix Interface ◽  
Full Field ◽  
Transverse Tension ◽  
Fiber Matrix Interface ◽  
Fiber Matrix

Macroscopic mechanical and failure properties of fiber-reinforced composites depend strongly on the properties of the fiber-matrix interface. For example, transverse cracking behavior and interlaminar shear strength of composites can be highly sensitive to the characteristics of the fiber-matrix interface. Despite its importance, experimental characterization of the mechanical behavior of the fibermatrix interface under normal loading conditions has been limited. This work reports on an experimental approach that uses in situ full-field digital image correlation (DIC) measurements to quantify the mechanical and failure behaviors at the fiber-matrix interface. Single fiber model composite samples are fabricated from a proprietary epoxy embedding a single glass rod. These samples are then tested under transverse tension. DIC is used to measure the deformation and strain fields in the glass rod, epoxy, and their interface vicinity. Initiation and propagation of the fiber-matrix debond are discussed. Full-field measurements are shown to facilitate the quantitative analysis of the traction-separation laws at the fiber-matrix interface subjected to transverse tension.

In Situ Characterization of Soils for Prediction of Stress-Strain Relationship

1983 ◽  
Author(s):  
K. Arulanandan ◽  
Y. Dafalias ◽  
L. R. Herrmann ◽  
A. Anandarajah ◽  
N. Meegoda
Keyword(s):  
In Situ Characterization ◽  
Stress Strain ◽  
Strain Relationship

scholarly journals Experimental Evaluation of Shear Behavior of Stone Masonry Wall

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2313
Author(s):  
Maria Luisa Beconcini ◽  
Pietro Croce ◽  
Paolo Formichi ◽  
Filippo Landi ◽  
Benedetta Puccini
Keyword(s):  
Shear Behavior ◽  
Stone Masonry ◽  
Masonry Walls ◽  
Mechanical Parameters ◽  
In Situ Tests ◽  
Capacity Curves ◽  
Historical Structures ◽  
Definition Of

The evaluation of the shear behavior of masonry walls is a first fundamental step for the assessment of existing masonry structures in seismic zones. However, due to the complexity of modelling experimental behavior and the wide variety of masonry types characterizing historical structures, the definition of masonry’s mechanical behavior is still a critical issue. Since the possibility to perform in situ tests is very limited and often conflicting with the needs of preservation, the characterization of shear masonry behavior is generally based on reference values of mechanical properties provided in modern structural codes for recurrent masonry categories. In the paper, a combined test procedure for the experimental characterization of masonry mechanical parameters and the assessment of the shear behavior of masonry walls is presented together with the experimental results obtained on three stone masonry walls. The procedure consists of a combination of three different in situ tests to be performed on the investigated wall. First, a single flat jack test is executed to derive the normal compressive stress acting on the wall. Then a double flat jack test is carried out to estimate the elastic modulus. Finally, the proposed shear test is performed to derive the capacity curve and to estimate the shear modulus and the shear strength. The first results obtained in the experimental campaign carried out by the authors confirm the capability of the proposed methodology to assess the masonry mechanical parameters, reducing the uncertainty affecting the definition of capacity curves of walls and consequently the evaluation of seismic vulnerability of the investigated buildings.

Experimental Characterization and Finite Element Modeling of Film Capacitors for Automotive Applications

2016 ◽  
Author(s):  
D. Croccolo ◽  
T. M. Brugo ◽  
M. De Agostinis ◽  
S. Fini ◽  
G. Olmi
Keyword(s):  
Finite Element ◽  
Mechanical Response ◽  
High Reliability ◽  
Three Dimensional ◽  
Strain Analysis ◽  
Life Time ◽  
Element Model ◽  
Image Correlation ◽  
Thermal Loads ◽  
Mechanical Shock

As electronics keeps on its trend towards miniaturization, increased functionality and connectivity, the need for improved reliability capacitors is growing rapidly in several industrial compartments, such as automotive, medical, aerospace and military. Particularly, recent developments of the automotive compartment, mostly due to changes in standards and regulations, are challenging the capabilities of capacitors in general, and especially film capacitors. Among the required features for a modern capacitor are the following: (i) high reliability under mechanical shock, (ii) wide working temperature range, (iii) high insulation resistance, (iv) small dimensions, (v) long expected life time and (vi) high peak withstanding voltage. This work aims at analyzing the key features that characterize the mechanical response of the capacitor towards temperature changes. Firstly, all the key components of the capacitor have been characterized, in terms of strength and stiffness, as a function of temperature. These objectives have been accomplished by means of several strain analysis methods, such as strain gauges, digital image correlation (DIC) or dynamic mechanical analysis (DMA). All the materials used to manufacture the capacitor, have been characterized, at least, with respect to their Young’s modulus and Poisson’s ratio. Then, a three-dimensional finite element model of the whole capacitor has been set up using the ANSYS code. Based on all the previously collected rehological data, the numerical model allowed to simulate the response in terms of stress and strain of each of the capacitor components when a steady state thermal load is applied. Due to noticeable differences between the thermal expansion coefficients of the capacitor components, stresses and strains build up, especially at the interface between different components, when thermal loads are applied to the assembly. Therefore, the final aim of these numerical analyses is to allow the design engineer to define structural optimization strategies, aimed at reducing the mechanical stresses on the capacitor components when thermal loads are applied.

scholarly journals The Preparation and Characterization of Polyacrylonitrile-Polyaniline (PAN/PANI) Fibers

Materials ◽  
2019 ◽  
Vol 12 (4) ◽  
pp. 664 ◽  
Author(s):  
Iwona Karbownik ◽  
Olga Rac-Rumijowska ◽  
Marta Fiedot-Toboła ◽  
Tomasz Rybicki ◽  
Helena Teterycz
Keyword(s):  
Specific Resistance ◽  
Strong Interactions ◽  
Mechanical Parameters ◽  
Dsc Analysis ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Strength Tests ◽  
Pan Fibers

The paper presents a method of modifying polyacrylonitrile (PAN) fibers using polyaniline (PANI). The PAN fibers were doped with polyaniline that was obtained in two different ways. The first consisted of doping a spinning solution with polyaniline that was synthesized in an aqueous solution (PAN/PANI blended), and the second involved the synthesis of polyaniline directly in the spinning solution (PAN/PANI in situ). The obtained fibers were characterized by the methods: X-ray powder diffraction (XRD), scanning electron microscope (SEM), fourier-transform infrared spectroscopy (FTIR), thermogravimetry (TG) and differential scanning calorimetry (DSC). Analysis of the results showed strong interactions between the nitrile groups of polyacrylonitrile and polyaniline in the PAN/PANI in situ fibers. The results of mechanical strength tests indicated that the performance of the PAN/PANI mixture significantly improved the mechanical parameters of polyaniline, although these fibers had a weaker strength than the unmodified PAN fibers. The fibers obtained as a result of the addition of PANI to PAN were dielectric, whereas the PANI-synthesized in situ were characterized by a mass-specific resistance of 5.47 kΩg/cm2.

Sign in / Sign up

Export Citation Format

Share Document