scholarly journals In Situ CT Tensile Testing of an Additively Manufactured and Heat-Treated Metastable ß-Titanium Alloy (Ti-5Al-5Mo-5V-3Cr)

2021 ◽  
Vol 11 (21) ◽  
pp. 9875
Author(s):  
Julius Hendl ◽  
Sina Daubner ◽  
Axel Marquardt ◽  
Lukas Stepien ◽  
Elena Lopez ◽  
...  

Additive manufacturing has been considered a suitable process for developing high-performance parts of medical or aerospace industries. The electron beam powder bed fusion process, EB‑PBF, is a powder bed fusion process carried out in a vacuum, in which the parts are melted using a highly focused electron beam. The material class of metastable β‑titanium alloys, and especially Ti‑5Al‑5Mo‑5V‑3Cr, show great potential for use as small and highly complex load-bearing parts. Specimens were additively manufactured with optimised process parameters and different heat treatments used in order to create tailored mechanical properties. These heat-treated specimens were analysed with regard to their microstructure (SEM) and their mechanical strength (tensile testing). Furthermore, in situ tensile tests, using a Deben CT5000 and a YXLON ff35 industrial µ‑CT, were performed and failure‑critical defects were detected, analysed and monitored. Experimental results indicate that, if EB‑PBF-manufactured Ti‑5553 is heat-treated differently, a variety of mechanical properties are possible. Regarding their fracture mechanisms, failure-critical defects can be detected at different stages of the tensile test and defect growth behaviour can be analysed.

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1067 ◽  
Author(s):  
Florian Huber ◽  
Thomas Papke ◽  
Christian Scheitler ◽  
Lukas Hanrieder ◽  
Marion Merklein ◽  
...  

The aim of this work is to investigate the β-Ti-phase-stabilizing effect of vanadium and iron added to Ti-6Al-4V powder by means of heterogeneous powder mixtures and in situ alloy-formation during laser powder bed fusion (L-PBF). The resulting microstructure was analyzed by metallographic methods, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). The mechanical properties were characterized by compression tests, both prior to and after heat-treating. Energy dispersive X-ray spectroscopy showed a homogeneous element distribution, proving the feasibility of in situ alloying by LPBF. Due to the β-phase-stabilizing effect of V and Fe added to Ti-6Al-4V, instead of an α’-martensitic microstructure, an α/β-microstructure containing at least 63.8% β-phase develops. Depending on the post L-PBF heat-treatment, either an increased upsetting at failure (33.9%) compared to unmodified Ti-6Al-4V (28.8%), or an exceptional high compressive yield strength (1857 ± 35 MPa compared to 1100 MPa) were measured. The hardness of the in situ alloyed material ranges from 336 ± 7 HV0.5, in as-built condition, to 543 ± 13 HV0.5 after precipitation-hardening. Hence, the range of achievable mechanical properties in dependence of the post-L-PBF heat-treatment can be significantly expanded in comparison to unmodified Ti-6Al-4V, thus providing increased flexibility for additive manufacturing of titanium parts.


Author(s):  
C. J. J. Torrent ◽  
P. Krooß ◽  
T. Niendorf

AbstractIn additive manufacturing, the thermal history of a part determines its final microstructural and mechanical properties. The factors leading to a specific temperature profile are diverse. For the integrity of a parameter setting established, periphery variations must also be considered. In the present study, iron was processed by electron beam powder bed fusion. Parts realized by two process runs featuring different build plate sizes were analyzed. It is shown that the process temperature differs significantly, eventually affecting the properties of the processed parts.


Author(s):  
Anton Du Plessis ◽  
Dean-Paul Kouprianoff ◽  
Ina Yadroitsava ◽  
Igor Yadroitsev

This paper reports on the production and mechanical properties of Ti6Al4V micro-lattice structures, with strut thickness nearing the single-track width of the laser-based powder bed fusion (LPBF) system used. Besides providing new information on the mechanical properties and manufacturability of such thin-strut lattices, this paper also reports on the in-situ deformation imaging of micro-lattice structures with 6 unit cells in every direction. LPBF lattices are of interest for medical implants, due to the possibility of creating structures with an elastic modulus close to that of the bones and small pore sizes which allow effective osseointegration. In this work four different cubes were produced by laser powder bed fusion and subsequently analyzed using microCT, compression testing and one selected lattice was subjected to in-situ microCT imaging during compression. The in-situ imaging was performed at 4 steps during yielding. The results indicate that mechanical performance (elastic modulus and strength) correlate well with actual density and that this performance is remarkably good, despite the high roughness and irregularity of the struts at this scale. In-situ yielding is visually illustrated.


Sign in / Sign up

Export Citation Format

Share Document