scholarly journals Influences of Process Parameters on the Microstructure and Mechanical Properties of CoCrFeNiTi Based High-Entropy Alloy in a Laser Powder Bed Fusion Process

Crystals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 549
Author(s):  
Takafumi Ikeda ◽  
Makiko Yonehara ◽  
Toshi-Taka Ikeshoji ◽  
Tohru Nobuki ◽  
Minoru Hatate ◽  
...  

Recently, high-entropy alloys (HEAs) have attracted much attention because of their superior properties, such as high strength and corrosion resistance. This study aimed to investigate the influences of process parameters on the microstructure and mechanical properties of CoCrFe NiTiMo HEAs using a laser-based powder bed fusion (LPBF) process. In terms of laser power and scan speed, a process map was constructed by evaluating the density and surface roughness of the as-built specimen to optimize the process parameters of the products. The mechanical properties of the as-built specimens fabricated at the optimum fabrication condition derived from the process map were evaluated. Consequently, the optimum laser power and scan speed could be obtained using the process map evaluated by density and surface roughness. The as-built specimen fabricated at the optimum fabrication condition presented a relative density of more than 99.8%. The microstructure of the as-built specimen exhibited anisotropy along the build direction. The tensile strength and elongation of the as-built specimen were around 1150 MPa and more than 20%, respectively.

2019 ◽  
Vol 25 (3) ◽  
pp. 433-447 ◽  
Author(s):  
Mahmoud Elsayed ◽  
Mootaz Ghazy ◽  
Yehia Youssef ◽  
Khamis Essa

PurposeTi6Al4V alloy has received a great deal of attention in medical applications due to its biomechanical compatibility. However, the human bone stiffness is between 10 and 30 GPa while solid Ti6Al4V is several times stiffer, which would cause stress shielding with the surrounding bone, which can lead to implant and/or the surrounding bone’s failure.Design/methodology/approachIn this work, the effect of selective laser melting (SLM) process parameters on the characteristics of Ti6Al4V samples, such as porosity level, surface roughness, elastic modulus and compressive strength (UCS), has been investigated using response surface method. The examined ranges of process parameters were 35-50 W for laser power, 100-400 mm/s for scan speed and 35-120 µm for hatch spacing. The process parameters have been optimized to obtain structures with properties very close to that in human bones.FindingsThe results showed that the porosity percentage of a SLM component could be increased by reducing the laser power and/or increasing the scan speed and hatch spacing. It was also shown that there was a reverse relationship between the porosity level and both the modulus of elasticity and UCS of the SLM part. In addition, the increased laser power was resulted into a substantial decrease of the surface roughness of SLM parts. Results from the optimization study revealed that the interaction between laser process parameters (i.e. laser power, laser speed, and the laser spacing) have the most significant influence on the mechanical properties of fabricated samples. The optimized values for the manufacturing of medical implants were 49 W, 400 mm/s and 99 µm for the laser power, laser speed and laser spacing, respectively. The corresponding porosity, surface roughness, modulus of elasticity and UCS were 23.62 per cent, 8.68 µm, 30 GPa and 522 MPa, respectively.Originality/valuePrevious investigations related to additive manufacturing of Ti alloys have focused on producing fully dense and high-integrity structures. There is a clear gap in literature regarding the simultaneous enhancement and adjustment of pore fraction, surface and mechanical properties of Ti6Al4V SLM components toward biomedical implants. This was the objective of the current study.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 87
Author(s):  
Faiyaz Ahsan ◽  
Jafar Razmi ◽  
Leila Ladani

The powder bed fusion additive manufacturing process has received widespread interest because of its capability to manufacture components with a complicated design and better surface finish compared to other additive techniques. Process optimization to obtain high quality parts is still a concern, which is impeding the full-scale production of materials. Therefore, it is of paramount importance to identify the best combination of process parameters that produces parts with the least defects and best features. This work focuses on gaining useful information about several features of the bead area, such as contact angle, porosity, voids, melt pool size and keyhole that were achieved using several combinations of laser power and scan speed to produce single scan lines. These features are identified and quantified using process learning, which is then used to conduct a comprehensive statistical analysis that allows to estimate the effect of the process parameters, such as laser power and scan speed on the output features. Both single and multi-response analyses are applied to analyze the response parameters, such as contact angle, porosity and melt pool size individually as well as in a collective manner. Laser power has been observed to have a more influential effect on all the features. A multi-response analysis showed that 150 W of laser power and 200 mm/s produced a bead with the best possible features.


Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 538 ◽  
Author(s):  
Fabrizia Caiazzo ◽  
Vittorio Alfieri ◽  
Giuseppe Casalino

Laser powder bed fusion (LPBF) can fabricate products with tailored mechanical and surface properties. In fact, surface texture, roughness, pore size, the resulting fractional density, and microhardness highly depend on the processing conditions, which are very difficult to deal with. Therefore, this paper aims at investigating the relevance of the volumetric energy density (VED) that is a concise index of some governing factors with a potential operational use. This paper proves the fact that the observed experimental variation in the surface roughness, number and size of pores, the fractional density, and Vickers hardness can be explained in terms of VED that can help the investigator in dealing with several process parameters at once.


Author(s):  
Massimiliano Bonesso ◽  
Pietro Rebesan ◽  
Claudio Gennari ◽  
Simone Mancin ◽  
Razvan Dima ◽  
...  

AbstractOne of the major benefits of the Laser Powder Bed Fusion (LPBF) technology is the possibility of fabrication of complex geometries and features in only one-step of production. In the case of heat exchangers in particular, this is very convenient for the fabrication of conformal cooling channels which can improve the performance of the heat transfer capability. Yet, obtaining dense copper parts printed via LPBF presents two major problems: the high reflectivity of 1 μm (the wavelength of commonly used laser sources) and the high thermal conductivity of copper that limits the maximum local temperature that can be attained. This leads to the formation of porous parts.In this contribution, the influence of the particle size distribution of the powder on the physical and mechanical properties of parts produced via LPBF is studied. Three copper powders lots with different particle size distributions are used in this study. The effect on densification from two laser scan parameters (scan speed and hatching distance) and the influence of contours scans on the lateral surface roughness is reported. Subsequently, samples manufactured with the optimal process parameters are tested for thermal and mechanical properties evaluation.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Shimin Dai ◽  
Hailong Liao ◽  
Haihong Zhu ◽  
Xiaoyan Zeng

Purpose For the laser powder bed fusion (L-PBF) technology, the side surface quality is essentially important for industrial applicated parts, such as the inner flow parts. Contour is generally adopted at the parts’ outline to enhance the side surface quality. However, the side surface roughness (Ra) is still larger than 10 microns even with contour in previous studies. The purpose of this paper is to study the influence of contour process parameters, laser power and scanning velocity on the side surface quality of the AlSi10Mg sample. Design/methodology/approach Using L-PBF technology to manufacture AlSi10Mg samples under different contour process parameters, use a laser confocal microscope to capture the surface information of the samples, and obtain the surface roughness Ra and the maximum surface height Rz of each sample after analysis and processing. Findings The results show that the side surface roughness decreases with the increase of the laser power at the fixed scanning velocity of 1,000 mm/s, the side surface roughness Ra stays within the error range as the contour velocity increases. It is found that the Ra increases with the scanning velocity increasing and the greater the laser power with the greater Ra increases when the laser power of contour process parameters is 300 W, 350 W and 400 W. The Rz maintain growth with the contour scanning velocity increasing at constant laser power. The continuous uniform contour covers the pores in the molten pool of the sample edge and thus increase the density of the sample. Two mechanisms named “Active adhesion” and “Passive adhesion” cause sticky powder. Originality/value Formation of a uniform and even contour track is key to obtain the good side surface quality. The side surface quality is determined by the uniformity and stability of the contour track when the layer thickness is fixed. These research results can provide helpful guidance to improve the surface quality of L-PBF manufactured parts.


Author(s):  
J. C. Heigel ◽  
B. M. Lane

This work presents high speed thermographic measurements of the melt pool length during single track laser scans on nickel alloy 625 substrates. Scans are made using a commercial laser powder bed fusion machine while measurements of the radiation from the surface are made using a high speed (1800 frames per second) infrared camera. The melt pool length measurement is based on the detection of the liquidus-solidus transition that is evident in the temperature profile. Seven different combinations of programmed laser power (49 W to 195 W) and scan speed (200 mm/s to 800 mm/s) are investigated and numerous replications using a variety of scan lengths (4 mm to 12 mm) are performed. Results show that the melt pool length reaches steady state within 2 mm of the start of each scan. Melt pool length increases with laser power, but its relationship with scan speed is less obvious because there is no significant difference between cases performed at the highest laser power of 195 W. Although keyholing appears to affect the anticipated trends in melt pool length, further research is required.


Author(s):  
Salah Eddine Brika ◽  
Yaoyao Fiona Zhao ◽  
Mathieu Brochu ◽  
Justin Mezzetta

This paper proposes an integrated approach to determine optimal build orientation for powder bed fusion by laser (PBF-L), by simultaneously optimizing mechanical properties, surface roughness, the amount of support structure (SUPP), and build time and cost. Experimental data analysis has been used to establish the objective functions for different mechanical properties and surface roughness. Geometry analysis of the part has been used to estimate the needed SUPP and thus evaluate the build time and cost. Normalized weights are assigned to different objectives depending on their relative importance allowing solving the multi-objective optimization problem using a genetic optimization algorithm. A study case is presented to demonstrate the capabilities of the developed system. The major achievements of this work are the consideration of multiple objectives and the establishment of objective function considering different load direction and heat treatments. A user-friendly graphical user interface was developed allowing to control different optimization process factors and providing different visualization and evaluation tools.


Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 450
Author(s):  
Johan Lindwall ◽  
Andreas Lundbäck ◽  
Jithin James Marattukalam ◽  
Anders Ericsson

The development of process parameters and scanning strategies for bulk metallic glass formation during additive manufacturing is time-consuming and costly. It typically involves trials with varying settings and destructive testing to evaluate the final phase structure of the experimental samples. In this study, we present an alternative method by modelling to predict the influence of the process parameters on the crystalline phase evolution during laser-based powder bed fusion (PBF-LB). The methodology is demonstrated by performing simulations, varying the following parameters: laser power, hatch spacing and hatch length. The results are compared in terms of crystalline volume fraction, crystal number density and mean crystal radius after scanning five consecutive layers. The result from the simulation shows an identical trend for the predicted crystalline phase fraction compared to the experimental estimates. It is shown that a low laser power, large hatch spacing and long hatch lengths are beneficial for glass formation during PBF-LB. The absolute values show an offset though, over-predicted by the numerical model. The method can indicate favourable parameter settings and be a complementary tool in the development of scanning strategies and processing parameters for additive manufacturing of bulk metallic glass.


Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 3927
Author(s):  
Eo Ryeong Lee ◽  
Se Eun Shin ◽  
Naoki Takata ◽  
Makoto Kobashi ◽  
Masaki Kato

This study provides a novel approach to fabricating Al/C composites using laser powder bed fusion (LPBF) for a wide range of structural applications utilizing Al-matrix composites in additive manufacturing. We investigated the effects of LPBF on the fabrication of aluminum/multiwalled carbon nanotube (Al/MWCNT) composites under 25 different conditions, using varying laser power levels and scan speeds. The microstructures and mechanical properties of the specimens, such as elastic modulus and nanohardness, were analyzed, and trends were identified. We observed favorable sintering behavior under laser conditions with low energy density, which verified the suitability of Al/MWCNT composites for a fabrication process using LPBF. The size and number of pores increased in specimens produced under high energy density conditions, suggesting that they are more influenced by laser power than scan speed. Similarly, the elastic modulus of a specimen was also more affected by laser power than scan speed. In contrast, scan speed had a greater influence on the final nanohardness. Depending on the laser power used, we observed a difference in the crystallographic orientation of the specimens by a laser power during LPBF. When energy density is high, texture development of all samples tended to be more pronounced.


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