scholarly journals An Experimental Study on Preparation of Reconstituted Tectonic Coal Samples: Optimization of Preparation Conditions

Energies ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2846
Author(s):  
Jishi Geng ◽  
Liwen Cao ◽  
Congyu Zhong ◽  
Shuai Zhang

The uniquely soft and fragile nature of tectonic coal makes it difficult to obtain core samples suitable for laboratory experimentation. Preparation of reconstituted tectonic coal (RTC) samples generally adopts the secondary forming method. Reliable coal samples are needed to obtain credible permeability and mechanical parameters that can guide Coalbed Methane (CBM) extraction and improve mining safety. In this study, the compaction mechanism of coal particles is analyzed based on the Kawakita model, and optimal sample preparation conditions are systemically investigated, particularly particle size and particle size distribution, forming pressure, and moisture content. The density and P-wave velocity of coal samples were used to test whether the RTC samples were realistic. Finally, the mechanical properties and deformation characteristics of the RTC samples were determined. The results indicate that RTC samples prepared for laboratory testing of mechanical properties require (1) the original particle size of the tectonic coal to be retained as much as possible; (2) a forming pressure that compacts the sample similar to the original tectonic coal; and (3) an optimum moisture content.

Energies ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 2303
Author(s):  
Congyu Zhong ◽  
Liwen Cao ◽  
Jishi Geng ◽  
Zhihao Jiang ◽  
Shuai Zhang

Because of its weak cementation and abundant pores and cracks, it is difficult to obtain suitable samples of tectonic coal to test its mechanical properties. Therefore, the research and development of coalbed methane drilling and mining technology are restricted. In this study, tectonic coal samples are remodeled with different particle sizes to test the mechanical parameters and loading resistivity. The research results show that the particle size and gradation of tectonic coal significantly impact its uniaxial compressive strength and elastic modulus and affect changes in resistivity. As the converted particle size increases, the uniaxial compressive strength and elastic modulus decrease first and then tend to remain unchanged. The strength of the single-particle gradation coal sample decreases from 0.867 to 0.433 MPa and the elastic modulus decreases from 59.28 to 41.63 MPa with increasing particle size. The change in resistivity of the coal sample increases with increasing particle size, and the degree of resistivity variation decreases during the coal sample failure stage. In composite-particle gradation, the proportion of fine particles in the tectonic coal sample increases from 33% to 80%. Its strength and elastic modulus increase from 0.996 to 1.31 MPa and 83.96 to 125.4 MPa, respectively, and the resistivity change degree decreases. The proportion of medium particles or coarse particles increases, and the sample strength, elastic modulus, and resistivity changes all decrease.


Energies ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3618 ◽  
Author(s):  
Longlong Pang ◽  
Yuzhong Yang ◽  
Liyun Wu ◽  
Fei Wang ◽  
Han Meng

The particle size of coal particles is an important factor affecting the physical and mechanical properties of coal. In this study, uniaxial and triaxial compression tests were conducted to investigate the effects of coal particle size on the physical and mechanical properties of briquettes and their impact mechanism using a rock mechanics test-150B servo system (RMT-150B). The results showed that the uniaxial compression strength, elastic modulus and deformation modulus of briquettes increase when particle size is decreased. The deformation characteristics of the briquettes directly prepared by raw tectonic coal were similar to those of coal specimens with a particle size of 0.18–0.25 mm. The cohesion and strength of coal specimens increased when particle size was decreased, and the plastic deformation capacity decreased when particle size was decreased, showing a strong correlation. The f briquette directly prepared by the raw tectonic coal had a strength between that of coal specimens with a particle size of 2–6 mm and those with a particle size of 0.18–0.25 mm. The mechanical properties of briquettes mainly depend on the meshing force between the coal particles. The smaller the particles, the greater the mechanical meshing force. The “floating particles”, generated in the voids between coal particles during the preparation process, are a significant factor affecting the plasticity characteristics. The research results may be used as a basic reference in the study of the mechanical properties of tectonic coal, gas migration and coal and gas outburst mechanisms.


Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-22
Author(s):  
Yunjiang Sun ◽  
Jianping Zuo ◽  
Yue Shi ◽  
Zhengdai Li ◽  
Changning Mi ◽  
...  

Ultrasonic wave velocity is effective to evaluate anisotropy property and predict rock failure. This paper investigates the correlation between dynamic ultrasonic and mechanical properties of sandstones with different buried depths subjected to uniaxial compression tests. The circumferential anisotropy and axial wave velocity of sandstone are obtained by means of ultrasonic wave velocity measurements. The mechanical properties, including Young’s modulus and uniaxial compressive strength, are positively correlated with the axial P wave velocity. The average angles between the sandstone failure plane and the minimum and maximum wave directions are 35.8° and 63.3°, respectively. The axial P wave velocity almost keeps constant, and the axial S wave velocity has a decreasing trend before the failure of rock specimen. In most rock samples under uniaxial compression, shear failure occurs in the middle and splitting appears near both sides. Additionally, the dynamic Young’s modulus and dynamic Poisson’s ratio during loading are obtained, and the negative values of the Poisson’s ratio occur at the initial compression stage. Distortion and rotation of micro/mesorock structures may be responsible for the negative Poisson’s ratio.


2020 ◽  
Vol 2020 ◽  
pp. 1-10
Author(s):  
Ruonan Zhu ◽  
Jianyong Pang ◽  
Tingya Wang ◽  
Xin Huang

Chloride corrosion test was carried out in 4% NaCl solution to study the chloride corrosion resistance of rubber concrete. Rubber concrete was prepared by using 20 mesh, 1∼3 mm, and 3∼6 mm rubber particles instead of sand by 5%, 10%, 15%, and 20% of the cementitious material mass. The P-wave velocity and compressive strength of rubber concrete were measured. The microstructure of rubber concrete corroded by chloride was analyzed by SEM. The micromorphology was compared with the macrofailure characteristics under uniaxial compression. The results show that the rubber concrete was still in the early stage of erosion. With the increase of immersion time at the age of 110 days, the P-wave velocity and compressive strength of concrete were generally on the rise. Furthermore, during the period of erosion, the mechanical properties of rubber concrete increased with the increase of rubber particle size and decreased with the increase of the content. Therefore, when the rubber particle size was 3∼6 mm and the content was 5%, the antierosion performance was the best. This study has a certain guiding significance for the chloride corrosion resistance of rubber concrete.


Materials ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 4617
Author(s):  
Shun Ding ◽  
Hailiang Jia ◽  
Fan Zi ◽  
Yuanhong Dong ◽  
Yuan Yao

Low-porosity tight rocks are widely used as building and engineering materials. The freeze–thaw cycle is a common weathering effect that damages building materials in cold climates. Tight rocks are generally supposed to be highly frost-resistant; thus, studies on frost damage in tight sandstone are rare. In this study, we investigated the deterioration in mechanical properties and changes in P-wave velocity with freeze–thaw cycles in a tight sandstone. We also studied changes to its pore structure using nuclear magnetic resonance (NMR) technology. The results demonstrate that, with increasing freeze–thaw cycles, (1) the mechanical strength (uniaxial compressive, tensile, shear strengths) exhibits a similar decreasing trend, while (2) the P-wave velocity and total pore volume do not obviously increase or decrease. (3) Nanopores account for >70% of the pores in tight sandstone but do not change greatly with freeze–thaw cycles; however, the micropore volume has a continuously increasing trend that corresponds to the decay in mechanical properties. We calculated the pressure-dependent freezing points in pores of different diameters, finding that water in nanopores (diameter <5.9 nm) remains unfrozen at –20 °C, and micropores >5.9 nm control the evolution of frost damage in tight sandstone. We suggest that pore ice grows from larger pores into smaller ones, generating excess pressure that causes frost damage in micropores and then nanopores, which is manifested in the decrease in mechanical properties.


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