scholarly journals Experimental and Numerical Analysis of Mold Filling in Rotational Molding

2021 ◽  
Vol 5 (11) ◽  
pp. 289
Author(s):  
Jonas Nieschlag ◽  
Julian Seuffert ◽  
Daniel Strack ◽  
Marco Friedmann ◽  
Luise Kärger ◽  
...  
Keyword(s):  
Capacitive Sensor ◽  
Mold Filling ◽  
Maximum Deviation ◽  
Rotational Molding ◽  
Molding Process ◽  
Average Deviation ◽  
Mean Values ◽  
The Matrix ◽  
Materials Used ◽  
Filling Simulation

This work focuses on the development of a numerical mold filling simulation for the rotational molding process. In the rotational molding process, a dry fiber preform is placed in a mold and impregnated with a thermoset matrix under rotation. Additionally, metallic load introduction elements can be inserted into the mold and joined with co-curing or form-fit, resulting in hybrid drive shafts or tie rods. The numerical model can be used to simulate the impregnation of the preform. Based on the resin transfer molding process, an OpenFOAM solver is extended for the rotational molding process. Permeability, kinetic and curing models are selected and adapted to the materials used. A wireless measurement solution with a capacitive sensor is developed to validate the model. Comparisons between measurements and numerically calculated impregnation times to reach the capacitive sensor with the matrix show good quality of the developed model. The average deviation between calculated result and measured mean values in the experiment is 43.8% the maximum deviation is 65.8% . The model can therefore be used to predict the impregnation progress and the curing state.

scholarly journals Influence of chloramine-T disinfection on elastomeric impression stability

2018 ◽  
Vol 12 (02) ◽  
pp. 232-236 ◽  
Author(s):  
Ricardo Danil Guiraldo ◽  
Sandrine Bittencourt Berger ◽  
Marilia Franco Punhagui ◽  
Thais Staut Moretto ◽  
Murilo Baena Lopes ◽  
...  
Keyword(s):  
Descriptive Analysis ◽  
Dental Materials ◽  
Optical Microscope ◽  
Scanning Tunneling ◽  
Mean Values ◽  
The Matrix ◽  
Disinfection Procedure ◽  
Chloramine T ◽  
Materials Used ◽  
The Stability

ABSTRACT Objective: The aim of this study was to evaluate the stability of elastomer through detail reproduction and its dimensional stability (DS) after disinfection with 0.2% chloramine-T. Materials and Methods: The elastomeric impression dental materials used in this study were polydimethylsiloxane (Oranwash L), polyvinyl siloxane (Express), polysulfide (Permlastic), and polyether (Impregum Soft). The entire press procedure was performed on a matrix in accordance with the ISO 4823. Detail reproduction was analyzed using an optical microscope (Stereozoom Microscope) over the 20-μm line with 25 mm of length at a magnification of ×4. DS was measured using an optical microscope (Scanning Tunneling Microscope) by subtracting the distance between the lines X and X’ over the 20-μm line on the matrix (DM) from the distance between the lines on the impression material (DI) divided by DM and multiplied by 100 establishing the equation: DS = ([DI – DM]/DM) ×100; then, 100% was added to the results of the equation. The detail reproduction values were subsequently subjected to descriptive analysis by percentage (%), and the DS values (%) were submitted to Kolmogorov–Smirnov test, two-way ANOVA (material × disinfectant), and Tukey’s test (α = 0.05). Results: All elastomeric impression materials showed 100% of detail reproduction, regardless of the disinfection procedure. Polysulfide (not disinfected) and polysulfide and polydimethylsiloxane (after disinfection with 0.2% chloramine-T) showed the smaller mean values of DS. Conclusion: According to the stability properties analyzed, chloramine-T can be used for disinfection of elastomer molds.

scholarly journals Development and Application of a Novel Pluri-Residue Method to Determine Polar Pesticides in Fruits and Vegetables through Liquid Chromatography High Resolution Mass Spectrometry

Foods ◽  
2020 ◽  
Vol 9 (5) ◽  
pp. 553
Author(s):  
Lorena Manzano-Sánchez ◽  
José Antonio Martínez-Martínez ◽  
Irene Domínguez ◽  
José Luis Martínez Vidal ◽  
Antonia Garrido Frenich ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
High Resolution ◽  
High Performance ◽  
Fruits And Vegetables ◽  
High Resolution Mass Spectrometry ◽  
Stationary Phases ◽  
Mean Values ◽  
Polar Pesticides ◽  
Relative Standard ◽  
The Matrix

Nowadays, highly polar pesticides are not included in multiresidue methods due to their physico-chemical characteristics and therefore, specific analytical methodologies are required for their analysis. Laboratories are still looking for a pluri-residue method that encompasses the largest number of polar pesticides. The aim of this work was the simultaneous determination of ethephon, 2-hydroxyethylphosphonic acid (HEPA), fosetyl aluminum, glyphosate, aminomethylphosphonic acid (AMPA), N-acetyl-glyphosate and N-acetyl-AMPA in tomatoes, oranges, aubergines and grapes. For that purpose, an ultra high performance liquid chromatography (UHPLC) coupled to a high resolution single mass spectrometer Orbitrap-MS were used. Different stationary phases were evaluated for chromatographic separation, and among them, the stationary phase Torus DEA provided the best separation of the selected compounds. The QuPPe method was used for the extraction of the analytes, but slight modifications were needed depending on the matrix. The developed method was validated, observing matrix effect in all matrices. Intra- and inter-day precision were estimated, and relative standard deviation were lower than 19%. Recoveries were satisfactory, and mean values ranged from 70% to 110%. Limits of quantification were between 25 and 100 µg kg−1. Finally, the analytical method was applied to different fruits and vegetables (oranges, tomatoes, aubergines and grapes).

Simplified Version of Polymer Rotational Molding Manufacturing Method

2016 ◽  
Vol 699 ◽  
pp. 97-103 ◽  
Author(s):  
Laurenţiu Slătineanu ◽  
Oana Dodun ◽  
Margareta Coteaţă ◽  
Gheorghe Nagîţ ◽  
Irina Beşliu
Keyword(s):  
Liquid Phase ◽  
Rotation Speed ◽  
Rotational Molding ◽  
Slow Speed ◽  
Molding Process ◽  
Manufacturing Method ◽  
Polyurethane Resin ◽  
Liquid Material ◽  
Complex Equipment ◽  
Plastic Parts

Rotational molding is a manufacturing method which supposes the rotation of the mold, during the solidification of the liquid phase material, so that finally a part having a hollow could be obtained. The method could be applied in manufacturing of metallic and nonmetallic parts. Usually, the equipment for rotational molding ensures slow speed rotating of the mold around two axes placed perpendicularly each other and this fact led to relatively complex equipment for achieving rotational molding. The capacity of the liquid material to entirely cover the internal walls of the mold depends essentially on the liquid material viscosity, on the rotation speed and on the movements applied to the mold. Simplified equipment including a single rotation movement could be materialized. In order to test such a solution, a preliminary experiment was designed and materialized, by using a device adapted on universal lathe. Thus, the objective of the research presented in the paper was to study if it is possible to achieve plastic parts made by rotational molding using a single rotation movement. A polyurethane resin obtained from two liquid components was used in order to obtain the liquid material that could be introduced in the mold. The research results proved the possibility to use simplified equipment for achieving a rotational molding process, at least in certain cases and with some technological limits.

Influence of Moisture on Flax Fiber in Polyethylene Composite Product Manufactured by Rotational Molding Process

2002 ◽  
Author(s):  
S. Panigrahi ◽  
L. G. Tabil ◽  
W. J. Crerar ◽  
S. Sokansanj ◽  
T. Powell ◽  
...  
Keyword(s):  
Flax Fiber ◽  
Rotational Molding ◽  
Molding Process ◽  
Polyethylene Composite ◽  
Composite Product
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