scholarly journals Residual Lattice Strain and Phase Distribution in Ti-6Al-4V Produced by Electron Beam Melting

Materials ◽  
2019 ◽  
Vol 12 (4) ◽  
pp. 667 ◽  
Author(s):  
Tuerdi Maimaitiyili ◽  
Robin Woracek ◽  
Magnus Neikter ◽  
Mirko Boin ◽  
Robert Wimpory ◽  
...  
Keyword(s):  
Residual Stress ◽  
Electron Beam ◽  
Electron Beam Melting ◽  
Phase Distribution ◽  
High Energy ◽  
Process Parameter ◽  
Electron Backscattered Diffraction ◽  
X Ray ◽  
Β Phase ◽  
Residual Strains

Residual stress/strain and microstructure used in additively manufactured material are strongly dependent on process parameter combination. With the aim to better understand and correlate process parameters used in electron beam melting (EBM) of Ti-6Al-4V with resulting phase distributions and residual stress/strains, extensive experimental work has been performed. A large number of polycrystalline Ti-6Al-4V specimens were produced with different optimized EBM process parameter combinations. These specimens were post-sequentially studied by using high-energy X-ray and neutron diffraction. In addition, visible light microscopy, scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD) studies were performed and linked to the other findings. Results show that the influence of scan speed and offset focus on resulting residual strain in a fully dense sample was not significant. In contrast to some previous literature, a uniform α- and β-Ti phase distribution was found in all investigated specimens. Furthermore, no strong strain variations along the build direction with respect to the deposition were found. The magnitude of strain in α and β phase show some variations both in the build plane and along the build direction, which seemed to correlate with the size of the primary β grains. However, no relation was found between measured residual strains in α and β phase. Large primary β grains and texture appear to have a strong effect on X-ray based stress results with relatively small beam size, therefore it is suggested to use a large beam for representative bulk measurements and also to consider the prior β grain size in experimental planning, as well as for mathematical modelling.

X-Ray Residual Stress Mapping in Industrial Materials By Energy Dispersive Diffractometry

1981 ◽  
Vol 25 ◽  
pp. 329-338 ◽  
Author(s):  
C. J. Bechtoldt ◽  
R. C. Placious ◽  
W. J. Boettinger ◽  
M. Kuriyama
Keyword(s):  
Residual Stress ◽  
Optical Resolution ◽  
High Energy ◽  
Energy Dispersive ◽  
Stress Distributions ◽  
X Ray ◽  
Transmission Geometry ◽  
Pipe Line ◽  
Residual Strains ◽  
Industrial Materials

AbstractAn application of energy dispersive diffractometry to the measurement of residual strains (stresses) in the interior of industrial materials is described with particular emphasis on the use of high energy (up to 250 keV) x-ray photons. The use of high energy photons permits better penetration into materials. Hence diffraction data for evaluating bulk residual strains can be obtained in the transmission geometry in contrast with the conventional angular dispersive diffractometry, which uses Bragg reflections from the surface of materials. The reliability and sensitivity (detectability of small strains) of the energy dispersive method are demonstrated through its application to mapping of residual stress distributions across weld zones in Alaskan pipe line segments (API5LX65). The detectability of strain variations within materials depends on x-ray optical resolution and statistics.

scholarly journals Impact Evaluation of High Energy Ball Milling Homogenization Process in the Phase Distribution of Hydroxyapatite-Barium Titanate Plasma Spray Biocoating

Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 728
Author(s):  
Roberto Gómez Batres ◽  
Zelma S. Guzmán Escobedo ◽  
Karime Carrera Gutiérrez ◽  
Irene Leal Berumen ◽  
Abel Hurtado Macias ◽  
...  
Keyword(s):  
Barium Titanate ◽  
Ball Milling ◽  
Plasma Spray ◽  
Bonding Strength ◽  
Phase Distribution ◽  
High Energy ◽  
High Energy Ball Milling ◽  
X Ray ◽  
Nanomechanical Properties ◽  
Energy Ball

Air plasma spray technique (APS) is widely used in the biomedical industry for the development of HA-based biocoatings. The present study focuses on the influence of powder homogenization treatment by high-energy ball milling (HEBM) in developing a novel hydroxyapatite-barium titanate (HA/BT) composite coating deposited by APS; in order to compare the impact of the milling process, powders were homogenized by mechanical stirring homogenization (MSH) too. For the two-homogenization process, three weight percent ratios were studied; 10%, 30%, and 50% w/w of BT in the HA matrix. The phase and crystallite size were analyzed by X-ray diffraction patterns (XRD); the BT-phase distribution in the coating was analyzed by backscattered electron image (BSE) with a scanning electron microscope (SEM); the energy-dispersive X-ray spectroscopy (EDS) analysis was used to determinate the Ca/P molar ratio of the coatings, the degree of adhesion (bonding strength) of coatings was determinate by pull-out test according to ASTM C633, and finally the nanomechanical properties was determinate by nanoindentation. In the results, the HEBM powder processing shows better efficiency in phase distribution, being the 30% (w/w) of BT in HA matrix that promotes the best bonding strength performance and failure type conduct (cohesive-type), on the other hand HEBM powder treatment promotes a slightly greater crystal phase stability and crystal shrank conduct against MSH; the HEBM promotes a better behavior in the nanomechanical properties of (i) adhesive strength, (ii) cohesive/adhesive failure-type, (iii) stiffness, (iv) elastic modulus, and (v) hardness properties.

scholarly journals Residual stress investigation on Ti-48Al-2Cr-2Nb samples produced by Electron Beam Melting process

Procedia CIRP ◽  
2021 ◽  
Vol 99 ◽  
pp. 336-341
Author(s):  
Manuela Galati ◽  
Giovanni Rizza ◽  
Alessandro Salmi ◽  
Sara Biamino ◽  
Cristian Ghibaudo ◽  
...  
Keyword(s):  
Residual Stress ◽  
Electron Beam ◽  
Electron Beam Melting ◽  
Melting Process ◽  
Electron Beam Melting Process

scholarly journals Can Appropriate Thermal Post-Treatment Make Defect Content in as-Built Electron Beam Additively Manufactured Alloy 718 Irrelevant?

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 536 ◽  
Author(s):  
Sneha Goel ◽  
Kévin Bourreau ◽  
Jonas Olsson ◽  
Uta Klement ◽  
Shrikant Joshi
Keyword(s):  
Electron Beam ◽  
Process Optimization ◽  
Electron Beam Melting ◽  
Phase Distribution ◽  
Hot Isostatic Pressing ◽  
Alloy 718 ◽  
Proof Of Concept ◽  
Defect Content ◽  
Enhancing Production ◽  
Hardness Values

Electron beam melting (EBM) is gaining rapid popularity for production of complex customized parts. For strategic applications involving materials like superalloys (e.g., Alloy 718), post-treatments including hot isostatic pressing (HIPing) to eliminate defects, and solutionizing and aging to achieve the desired phase constitution are often practiced. The present study specifically explores the ability of the combination of the above post-treatments to render the as-built defect content in EBM Alloy 718 irrelevant. Results show that HIPing can reduce defect content from as high as 17% in as-built samples (intentionally generated employing increased processing speeds in this illustrative proof-of-concept study) to <0.3%, with the small amount of remnant defects being mainly associated with oxide inclusions. The subsequent solution and aging treatments are also found to yield virtually identical phase distribution and hardness values in samples with vastly varying as-built defect contents. This can have considerable implications in contributing to minimizing elaborate process optimization efforts as well as slightly enhancing production speeds to promote industrialization of EBM for applications that demand the above post-treatments.

scholarly journals Tailoring Microstructure and Mechanical Properties of Additively-Manufactured Ti6Al4V Using Post Processing

Materials ◽  
2021 ◽  
Vol 14 (3) ◽  
pp. 658
Author(s):  
Yaron Itay Ganor ◽  
Eitan Tiferet ◽  
Sven C. Vogel ◽  
Donald W. Brown ◽  
Michael Chonin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Electron Beam ◽  
Fatigue Resistance ◽  
Electron Beam Melting ◽  
High Reliability ◽  
National Laboratory ◽  
Post Processing ◽  
Proof Stress ◽  
Β Phase ◽  
Microstructure And Mechanical Properties

Additively-manufactured Ti-6Al-4V (Ti64) exhibits high strength but in some cases inferior elongation to those of conventionally manufactured materials. Post-processing of additively manufactured Ti64 components is investigated to modify the mechanical properties for specific applications while still utilizing the benefits of the additive manufacturing process. The mechanical properties and fatigue resistance of Ti64 samples made by electron beam melting were tested in the as-built state. Several heat treatments (up to 1000 °C) were performed to study their effect on the microstructure and mechanical properties. Phase content during heating was tested with high reliability by neutron diffraction at Los Alamos National Laboratory. Two different hot isostatic pressings (HIP) cycles were tested, one at low temperature (780 °C), the other is at the standard temperature (920 °C). The results show that lowering the HIP holding temperature retains the fine microstructure (~1% β phase) and the 0.2% proof stress of the as-built samples (1038 MPa), but gives rise to higher elongation (~14%) and better fatigue life. The material subjected to a higher HIP temperature had a coarser microstructure, more residual β phase (~2% difference), displayed slightly lower Vickers hardness (~15 HV10N), 0.2% proof stress (~60 MPa) and ultimate stresses (~40 MPa) than the material HIP’ed at 780 °C, but had superior elongation (~6%) and fatigue resistance. Heat treatment at 1000 °C entirely altered the microstructure (~7% β phase), yield elongation of 13.7% but decrease the 0.2% proof-stress to 927 MPa. The results of the HIP at 780 °C imply it would be beneficial to lower the standard ASTM HIP temperature for Ti6Al4V additively manufactured by electron beam melting.

scholarly journals Microstructure of Oxide Dispersion Strengthened Steel With Cr Content Variation

2020 ◽  
Vol 21 (1) ◽  
pp. 35
Author(s):  
Marzuki Silalahi ◽  
Bernadus Bandriyana ◽  
Arbi Dimyati ◽  
Bambang Sugeng ◽  
Syahfandi Ahda ◽  
...  
Keyword(s):  
High Temperature ◽  
Phase Distribution ◽  
Oxide Dispersion Strengthened ◽  
High Energy ◽  
Oxide Dispersion ◽  
X Ray ◽  
Hardness Tester ◽  
Cr Content ◽  
Ods Steel ◽  
The Matrix

Microstructure and phase distribution of innovative Oxide Dispersion Strengthened (ODS) steel based on Fe-Cr-ZrO2 particularly for application at high temperature reactor with variation of Cr content was analysed. The alloy was synthesized with Cr composition variation of  15, 20 and 25 wt.% Cr, while zirconia dispersoid kept constant at 0.50 wt.%. The samples was synthesized by mechanical alloying comprising of high energy milling for 3 hours followed by vibrated compression with iso-static load at 20 ton. The final consolidation was performed via sintering process for 4 minutes using the Arc Plasma Sintering (APS) technique, a new method developed in BATAN especially for synthesizing high temperature materials. The samples were then characterized by means of scanning electron microscopy (SEM) with energy dispersed X-ray (EDX) analysis capability and X-ray diffraction. The mechanical property of hardness was measured using standard Vickers micro hardness tester to confirmed the microstructure analysis.  The results show that the microstructure of the ODS alloy samples in all variation of Cr content consists generally of cubic Fe-Cr matrix phase with small of porosity and  Zirconia particles distributed homogenously in and around the matrix grains. The achievable hardness was between 142 and 184 HVN dependent consistently on Cr content in which Cr element may cause grain refining that in turn increase the hardness.

Microstructures and Hardness Properties for β-Phase Ti–24Nb–4Zr–7.9Sn Alloy Fabricated by Electron Beam Melting

2013 ◽  
Vol 29 (11) ◽  
pp. 1011-1017 ◽  
Author(s):  
J. Hernandez ◽  
S.J. Li ◽  
E. Martinez ◽  
L.E. Murr ◽  
X.M. Pan ◽  
...  
Keyword(s):  
Electron Beam ◽  
Electron Beam Melting ◽  
Β Phase

Residual stresses in a SiC whisker-reinforced alumina composite by high-temperature X-ray diffraction

1994 ◽  
Vol 9 (1) ◽  
pp. 50-53 ◽  
Author(s):  
Benjamin L. Ballard ◽  
Paul K. Predecki ◽  
Camden R. Hubbard
Keyword(s):  
Residual Stress ◽  
Single Crystal Silicon ◽  
Linear Extrapolation ◽  
X Ray Diffraction ◽  
Crystal Silicon ◽  
X Ray ◽  
Fine Grained ◽  
Silicon Carbide Whiskers ◽  
Alumina Composite ◽  
Residual Strains

Residual strains and microstresses are evaluated for both phase of a hot-pressed, fine-grained α-alumina reinforced with 25 wt% (29 vol%) single-crystal silicon carbide whiskers at temperatures from 25 to 1000 °C. The sample was maintained in a nonoxidizing environment while measurements of the interplaner spacing of alumina (146) and SiC (511 + 333) were made using X-ray diffraction methods. The residual strains were profiled at temperature increments of 250 °C from which the corresponding microstresses were calculated. Linear extrapolation of the SiC ε33 profile indicates that the strains are completely relaxed at a temperature of approximately 1470 °C. These residual stress relaxation results suggest that elevated temperature toughness and fracture strength of this composite may result from cooperative mechanisms.

Ti6Al4V Parts Produced by Electron Beam Melting: Analysis of Dimensional Accuracy and Surface Roughness

2020 ◽  
Vol 19 (01) ◽  
pp. 107-130 ◽  
Author(s):  
R. Borrelli ◽  
S. Franchitti ◽  
C. Pirozzi ◽  
L. Carrino ◽  
L. Nele ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Electron Beam ◽  
Additive Manufacturing ◽  
Electron Beam Melting ◽  
Complex Shape ◽  
Electron Beam Welding ◽  
Raw Materials ◽  
Dimensional Accuracy ◽  
High Energy ◽  
Quality Certification

Additive manufacturing (AM), applied to metal industry, is a family of processes that allows complex shape components to be realized from raw materials in the form of powders. Electron beam melting (EBM) is a relatively new additive manufacturing (AM) technology. Similar to electron-beam welding, EBM utilizes a high-energy electron beam as a moving heat source to melt metal powder, and 3D parts are produced in a layer-building fashion by rapid self-cooling. By EBM, it is possible to realize metallic complex shape components, e.g. fine network structures, internal cavities and channels, which are difficult to make by conventional manufacturing means. This feature is of particular interest in titanium industry in which numerous efforts are done to develop near net shape processes. In the field of mechanical engineering and, in particular, in the aerospace industry, it is crucial for quality certification purpose that components are produced through qualified and robust manufacturing processes ensuring high product repeatability. The contribution of the present work is to experimentally identify the EBM job parameters (sample orientation, location of the sample in the layer and height in the build chamber) that influence the dimensional accuracy and the surface roughness of the manufactured parts in Ti6Al4V. The repeatability of EBM is investigated too.

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