scholarly journals A Study of Low Young’s Modulus Ti–15Ta–15Nb Alloy Using TEM Analysis

Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5694
Author(s):  
Huey-Er Lee ◽  
Ju-Hui Wu ◽  
Chih-Yeh Chao ◽  
Yen-Hao Chang ◽  
Je-Kang Du ◽  
...  

The microstructural characteristics and Young’s modulus of the as-cast Ti–15Ta–15Nb alloy are reported in this study. On the basis of the examined XRD and TEM results, the microstructure of the current alloy is essentially a mixture (α + β+ α′ + α″ + ω + H) phase. The new H phase has not previously been identified as a known phase in the Ti–Ta–Nb alloy system. On the basis of examination of the Kikuchi maps, the new H phase belongs to a tetragonal structural class with lattice parameters of a = b = 0.328 nm and c = 0.343 nm, denoting an optimal presentation of the atomic arrangement. The relationships of orientation between these phases would be {0001}α//{110}β//{1¯21¯0}ω//{101¯}H and (011¯0)α//(11¯2)β//(1¯010)ω//(121)H. Moreover, the Young’s modulus of the as-cast Ti–15Ta–15Nb alloy is approximately E = 80.2 ± 10.66 GPa. It is implied that the Young’s modulus can be decreased by the mixing of phases, especially with the presence of the H phase.

2020 ◽  
Vol 10 (21) ◽  
pp. 7896
Author(s):  
Taekyung Lee

Ti-13Nb-13Zr alloy is an orthopedic implant material possessing good mechanical properties, corrosion resistance, and biocompatibility. An international standard suggests a heat treatment known as “capability aging” for this alloy. This study provides extensive data of mechanical properties under a wide temperature condition built around the capability-aging process. Specifically, it investigates the effect of annealing temperature (573–973 K) on mechanical properties (i.e., yield strength, tensile strength, hardness, Young’s modulus, and mechanical compatibility) of Ti-13Nb-13Zr alloys. Although these mechanical properties showed similar trends with respect to the annealing temperature, Young’s modulus exhibited the highest value at 873 K in contrast to those of the other properties shown at 773 K. Such a disparity was discussed in light of static spheroidization and phase decomposition based on microstructural characteristics of the annealed Ti-13Nb-13Zr alloys.


2013 ◽  
Vol 641-642 ◽  
pp. 479-482 ◽  
Author(s):  
Xiao Xiao Sun

First principles calculations have been performed to investigate the elastic and electronic behaviors of Li3Bi as a function of pressure from 0 GPa to 100 GPa with a step 10 GPa. Our calculations indicate that the lattice parameters and volume of cubic Li3Bi decrease with the increasing pressure. Cubic Fm-3m structure of Li3Bi is more mechanically stable at pressures of up to 100 GPa. The calculated results of the bulk, shear, Young’s modulus, B/G ratio of Li3Bi as a function of pressure show that Li3Bi has higher bulk, shear modulus and better ductility at 0 GPa than 50 GPa. The analysis of electronic properties reveals that the covalent Bi-Li bonding plays an important role in hardness and incompressibility of Li3Bi.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3210 ◽  
Author(s):  
Pedro Akira Bazaglia Kuroda ◽  
Fernanda de Freitas Quadros ◽  
Raul Oliveira de Araújo ◽  
Conrado Ramos Moreira Afonso ◽  
Carlos Roberto Grandini

Titanium and its alloys currently are used as implants, possessing excellent mechanical properties (more suited than stainless steel and Co-Cr alloys), good corrosion resistance and good biocompatibility. The titanium alloy used for most biomedical applications is Ti-6Al-4V, however, studies showed that vanadium and aluminum cause allergic reactions in human tissues and neurological disorders. New titanium alloys without the presence of these elements are being studied. The objective of this study was to analyze the influence of thermomechanical treatments, such as hot-rolling, annealing and solution treatment in the structure, microstructure and mechanical properties of the Ti-25Ta-Zr ternary alloy system. The structural and microstructural analyses were performed using X-ray diffraction, as well as optical, scanning and transmission electron microscopy. The mechanical properties were analyzed using microhardness and Young’s modulus measurements. The results showed that the structure of the materials and the mechanical properties are influenced by the different thermal treatments: rapid cooling treatments (hot-rolling and solubilization) induced the formation of α” and β phases, while the treatments with slow cooling (annealing) induced the formation of martensite phases. Alloys in the hot-rolled and solubilized conditions have better mechanical properties results, such as low elastic modulus, due to retention of the β phase in these alloys.


2019 ◽  
Vol 107 (2) ◽  
pp. 207 ◽  
Author(s):  
Jaroslav Čech ◽  
Petr Haušild ◽  
Miroslav Karlík ◽  
Veronika Kadlecová ◽  
Jiří Čapek ◽  
...  

FeAl20Si20 (wt.%) powders prepared by mechanical alloying from different initial feedstock materials (Fe, Al, Si, FeAl27) were investigated in this study. Scanning electron microscopy, X-ray diffraction and nanoindentation techniques were used to analyze microstructure, phase composition and mechanical properties (hardness and Young’s modulus). Finite element model was developed to account for the decrease in measured values of mechanical properties of powder particles with increasing penetration depth caused by surrounding soft resin used for embedding powder particles. Progressive homogenization of the powders’ microstructure and an increase of hardness and Young’s modulus with milling time were observed and the time for complete homogenization was estimated.


1981 ◽  
Vol 6 ◽  
Author(s):  
J.R. Mclaren ◽  
R.W. Davidge ◽  
I. Titchell ◽  
K. Sincock ◽  
A. Bromley

ABSTRACTHeating to temperatures up to 500°C, gives a reduction in Young's modulus and increase in permeability of granitic rocks and it is likely that a major reason is grain boundary cracking. The cracking of grain boundary facets in polycrystalline multiphase materials showing anisotropic thermal expansion behaviour is controlled by several microstructural factors in addition to the intrinsic thermal and elastic properties. Of specific interest are the relative orientations of the two grains meeting at the facet, and the size of the facet; these factors thus introduce two statistical aspects to the problem and these are introduced to give quantitative data on crack density versus temperature. The theory is compared with experimental measurements of Young's modulus and permeability for various rocks as a function of temperature. There is good qualitative agreement, and the additional (mainly microstructural) data required for a quantitative comparison are defined.


2020 ◽  
Vol 12 ◽  
Author(s):  
S.V. Kontomaris ◽  
A. Malamou ◽  
A. Stylianou

Background: The determination of the mechanical properties of biological samples using Atomic Force Microscopy (AFM) at the nanoscale is usually performed using basic models arising from the contact mechanics theory. In particular, the Hertz model is the most frequently used theoretical tool for data processing. However, the Hertz model requires several assumptions such as homogeneous and isotropic samples and indenters with perfectly spherical or conical shapes. As it is widely known, none of these requirements are 100 % fulfilled for the case of indentation experiments at the nanoscale. As a result, significant errors arise in the Young’s modulus calculation. At the same time, an analytical model that could account complexities of soft biomaterials, such as nonlinear behavior, anisotropy, and heterogeneity, may be far-reaching. In addition, this hypothetical model would be ‘too difficult’ to be applied in real clinical activities since it would require very heavy workload and highly specialized personnel. Objective: In this paper a simple solution is provided to the aforementioned dead-end. A new approach is introduced in order to provide a simple and accurate method for the mechanical characterization at the nanoscale. Method: The ratio of the work done by the indenter on the sample of interest to the work done by the indenter on a reference sample is introduced as a new physical quantity that does not require homogeneous, isotropic samples or perfect indenters. Results: The proposed approach, not only provides an accurate solution from a physical perspective but also a simpler solution which does not require activities such as the determination of the cantilever’s spring constant and the dimensions of the AFM tip. Conclusion: The proposed, by this opinion paper, solution aims to provide a significant opportunity to overcome the existing limitations provided by Hertzian mechanics and apply AFM techniques in real clinical activities.


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