Parameters Control for Properties of Ferrofluid Used in Series Ferrofluid Sensor

2012 ◽  
Vol 248 ◽  
pp. 594-598
Author(s):  
Gang Zhao ◽  
Hai Rong Cui ◽  
Qiu Li Ding ◽  
Xu Feng Wang ◽  
Shi Xi Tian ◽  
...  
Keyword(s):  
Magnetization Curve ◽  
Ph Value ◽  
Nano Particles ◽  
Molar Ratio ◽  
Magnetic Intensity ◽  
Iron Ion ◽  
Ferrous Chloride ◽  
Bivalent Iron ◽  
In Series ◽  
Magnetic Nano Particles

Series ferrofluid based sensors are novel sensors which use ferrofluid as inductive core to measure signals. The physical properties of ferrofluid affect mostly on performance parameter of these series sensors. There is several generality regularity for ferrofluid appliedd in series sensors. This paper analyses the generality of parameter controlling for properties of ferrofluid used in series ferrofluid sensors. The working area of magnetization curve of ferrofluid used in series sensors should be in its linear area where the permeability of ferrofluid is considered as a constant. The magnetic nano-particles generally obtained by reaction of ferrous chloride and ferric chloride. With the increment of viscosity and density of ferrofluid, the saturation magnetic intensity of ferrofluid increases. The concentration of reacted solution is better to be 0.6mol/L. Saturation magnet intensity of magnetic nano-partcles is highest as the molar ratio of trivalent iron ion to bivalent iron ion is equal to 1.75. The reacted temperature is better between 65~80°C while PH value of solution is in a weak alkaline state.

Kerosene Based Magnetic Fluid Used in Magnetic Fluid Inclination Sensor

2011 ◽  
Vol 211-212 ◽  
pp. 411-415 ◽  
Author(s):  
Hai Rong Cui ◽  
Ming Li Sun ◽  
Xue Feng Wang
Keyword(s):  
Saturation Magnetization ◽  
Ferric Chloride ◽  
Magnetic Fluid ◽  
Ph Value ◽  
Physical Property ◽  
Nano Particles ◽  
Molar Ratio ◽  
Iron Ion ◽  
Ferrous Chloride ◽  
Magnetic Nano Particles

Kerosene based magnetic fluid which use kerosene as carrier liquid is characterized by better liquidity and higher magnetization which is qualified enough to use in magnetic fluid based inclination sensor. This paper provides several preparative parameters to control the physical property of kerosene based magnetic fluid during manufacture processing which use ferrous chloride and ferric chloride as forerunner reaction mass. The results show that the proper consistency of ferrous chloride and ferric chloride is 0.6mol/L. Secondly, the saturation magnetization of magnetic nano-particles is highest when the molar ratio between trivalent iron ion and bivalent iron ion is equal to 1.75. Thirdly, the proper reacted temperature is between 60~80°C and pH value should be controlled in a weak alkaline situation while six hours should be necessary for surfactant encapsulated enough around the magnetic nano-particles surface. At last, the saturation magnetization of kerosene based magnetic fluid increases with the increment of density and viscosity of magnetic fluid.

Synthesis of Diester Based Magnetic Fluid

2012 ◽  
Vol 217-219 ◽  
pp. 721-724 ◽  
Author(s):  
Hai Rong Cui ◽  
Xue Feng Wang
Keyword(s):  
Magnetic Fluid ◽  
Magnetic Particles ◽  
Research Field ◽  
Nano Particles ◽  
Molar Ratio ◽  
Engineering Research ◽  
Carrier Liquid ◽  
Proper Size ◽  
Environment Temperature ◽  
Magnetic Nano Particles

Diester based magnetic fluid is a novel intelligent material which use diester as carrier liquid and magnetic iron ore as magnetic nano-particles combined together with proper surfactant. Its specially unique characteristic contributes to wide applications in engineering research field such as magnetic fluid based seals, magnetic fluid based dampers and so on. This paper provides a method of diester-based magnetic fluid synthesis and analysis for the properties of prepared diester magnetic fluid as well as effective influencing parameters. The results show that for getting proper size and magnetization of magnetic particles, the proper reacted temperature is around 60~80°C, appropriate molar ratio of reacted solution is 1.75 and concentration of forerunner is about 0.6 mol/L. It is also found that the viscosity of diester-based magnetic fluid is decreased with environment temperature while the viscosity as well as saturation magnetization increases with the increment of density.

Synthesis of LNF Nano Particles for Fuel Cell Applications

2009 ◽  
Vol 1230 ◽  
Author(s):  
Reza Bateni ◽  
Maryan Nasirpour ◽  
Olivera Kesler
Keyword(s):  
Ph Value ◽  
Thermo Gravimetric Analysis ◽  
Combustion Process ◽  
Precursor Solution ◽  
Nano Particles ◽  
Process Efficiency ◽  
Molar Ratio ◽  
Gravimetric Analysis ◽  
Metallic Ions ◽  
X Ray

AbstractThe aim of the present work is to understand the effect of different parameters such as the molar ratio of metallic ions to fuel in sol-gel solution, pH of the solution, and calcining temperature on the efficiency of the combustion synthesis technique in preparing submicron lanthanum nickel ferrite using metal nitrate-citrate/glycine mixtures. Scanning electron microscopy (SEM) coupled with energy-dispersive X-ray spectroscopy (EDS) was used to evaluate the powder morphology and elemental composition. The crystal structure of the calcined powders was evaluated by X-ray diffraction (XRD) and the thermal characteristics of the LNF precursors were examined by thermo-gravimetric analysis (TGA) in air, to identify suitable processing conditions. It was found that by increasing the molar ratio of fuel to metallic ions in the precursor solution, calcining could take place at lower temperatures. However, by increasing the molar ratio of fuel to metallic ions, the yield of the combustion process was decreased. Furthermore, the pH value of the precursor solution did not have any influence on the process efficiency over the range examined.

ON-LINE CHARACTERIZATION OF MAGNETIC NANO PARTICLES - SIMULATION VERSUS EXPERIMENT

2001 ◽  
Vol 32 ◽  
pp. 385-386
Author(s):  
TH. KAUFFELDT ◽  
E. KAUFFELDT ◽  
T. ZARUTSKAYA ◽  
M. SHAPIRO ◽  
A. SCHMIDT-OTT
Keyword(s):  
Nano Particles ◽  
On Line ◽  
Magnetic Nano Particles

Comparative study of three magnetic nano-particles (FeSO4, FeSO4/SiO2, FeSO4/SiO2/TiO2) in plasmid DNA extraction

2016 ◽  
Vol 513 ◽  
pp. 68-76 ◽  
Author(s):  
H. Rahnama ◽  
A. Sattarzadeh ◽  
F. Kazemi ◽  
N. Ahmadi ◽  
F. Sanjarian ◽  
...  
Keyword(s):  
Comparative Study ◽  
Dna Extraction ◽  
Plasmid Dna ◽  
Nano Particles ◽  
Magnetic Nano Particles

Effects of Fe3O4 Nano Particles Addition in High Temperature Superconductor YBa2Cu3O7-δ

2012 ◽  
Vol 501 ◽  
pp. 309-313 ◽  
Author(s):  
Siti Nurdalila Abd-Ghani ◽  
Roslan Abd-Shukor ◽  
Wei Kong
Keyword(s):  
Transport Properties ◽  
Solid State Reaction Method ◽  
Nano Particles ◽  
Magnetic Impurities ◽  
Oxide Powders ◽  
Nano Fe3o4 ◽  
Activated Flux ◽  
Average Size ◽  
Increasing Temperature ◽  
Magnetic Nano Particles

The effects of nano particles Fe3O4 addition on the superconducting and transport properties of YBa2Cu3O7-δ (YBCO) were studied. YBa2Cu3O7-δ superconductor powders were prepared by using high purity oxide powders via solid state reaction method. Nano Fe3O4 with 0.01 – 0.05 wt.% with average size 28 nm was added into YBCO. The transition temperatures (Tc) of the samples were measured by using four point probe method. The critical current (Ic) of the samples has been determined by using the 1 μV/cm criterion from 30 – 77 K. Sample with 0.02 wt.% nano Fe3O4 showed the highest Tc at 87 K. It is interesting to note the same sample also exhibited the highest Jc at 77 K up to 1683 mA/cm2. Nano Fe3O4 has acted as effective flux pinning centers in YBCO. A small amount of nano particles Fe3O4 addition has successfully improved the superconducting and transport properties of YBCO. The excessive addition of nano Fe3O4 (> 0.02 wt.%) suppressed the Tc and Jc. Overall, Jc decreases with increasing temperature (30 – 77 K) as a consequence of thermally activated flux creep. Magnetic impurities normally suppress superconductivity. However, by adding magnetic nano particles, current carrying capacity of superconductors YBCO was enhanced significantly.

Controlled Synthesis of Different Morphologies of SrWO4 Crystals via a Surfactant-Assisted Hydrothermal Precipitation Method

2013 ◽  
Vol 785-786 ◽  
pp. 449-454
Author(s):  
Yan Zhao ◽  
Chun Yan Wu ◽  
Dan Qin ◽  
Xin Lai ◽  
Si Wu ◽  
...  
Keyword(s):  
Ph Value ◽  
Precipitation Method ◽  
Molar Ratio ◽  
X Ray Diffraction ◽  
X Ray ◽  
Experimental Parameters ◽  
Infrared Spectrometer ◽  
Luminescent Spectra ◽  
Hydrothermal Precipitation ◽  
Surfactant Assisted

SrWO4 octahedrons, flowers, bundles, ellipsoids and dendrites had been successfully synthesized via surfactant-assisted method. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), photo-luminescent spectra techniques (PL) and fourier transrform infrared spectrometer (FTIR). By through various comparison experiments, it can be found that some related experimental parameters including the reagent concentration, [Sr2+]/[WO42-] molar ratio (R), aging temperature and the pH value had great influences on morphology of the products.

Study on Preparation and Photocatalytic Performance of Co-Doped TiO2 with Cu and Ce

2011 ◽  
Vol 399-401 ◽  
pp. 722-726 ◽  
Author(s):  
Jiang Ping Zhao ◽  
Xiao Ni Yang ◽  
Hao Zhang
Keyword(s):  
Photocatalytic Performance ◽  
Sol Gel ◽  
Test Chamber ◽  
Raw Material ◽  
Nano Particles ◽  
Molar Ratio ◽  
X Ray ◽  
Co Doping ◽  
Photocatalytic Activities ◽  
Environmental Test

In this paper, Cu-Ce/TiO2nano-particles, whose molar ratio account for 2%,2.5%,3%,3.5% and 4% respectively, were synthesized by sol-gel method, using Ti(C4H9O)4as the raw material, And the photocatalytic activities of the prepared samples were investigated by degrading formaldehyde gas under pure visible light through simulating indoor environment in the environmental test chamber. Moreover, X-Ray Powder Diffraction (XRD) and Ultraviolet-visible spectrophotometer were applied to analyze the crystallite size and optical properties of the samples. It is indicated that the sample of 2.5% performs best in the test. Besides, photocatalytic mechanism of co-doping of Cu-Ce was discussed.

scholarly journals Silver Cation Coordination Study to AsW9 Ligand – A Trilacunar Arsenotungstate Compound

2017 ◽  
Vol 63 (2) ◽  
pp. 70-72
Author(s):  
Lavinia Berta ◽  
Andrei Gâz ◽  
Francisc Boda ◽  
Augustin Curticapean
Keyword(s):  
Graphical Method ◽  
Ph Value ◽  
Building Blocks ◽  
Silver Cation ◽  
Molar Ratio ◽  
Equivalence Point ◽  
Tetrahedral Geometry ◽  
Sandwich Type ◽  
Preliminary Study ◽  
Cation Coordination

Abstract Objective: The main objective of this research is to find the coordination ratio between AsW9 and Ag+, as a preliminary study for synthesizing a new silver-arsenotungstate complex. Material and method: The ligand:cation molar ratio in complexes was determined by conductometric and potentiometric titrations of AsW9 with silver salts: CH3COOAg, AgNO3. Results: The ratio was obtained from the inflexion points of the curves when molar ratio was plotted versus conductivity, or from the equivalence point when silver added volume was plotted versus pH value. Each graphic shows one point of inflexion corresponding to 1:1.54 ratio of AsW9:Ag+. In the same manner, the equivalent volumes determined by graphical method gave the ratio 1:1.53. The spectral results confirmed that a AsW9:Ag+ complex was formed since the ligand absorption maxima values have been changed from 190 nm to 197 nm in the case of using AgNO3 and 196 nm for CH3COOAg corresponding to the W=Od bond, and from 246.5 nm to 274 nm (AgNO3) and 270 nm (CH3COO-Ag+) for the W-Ob,c-W bond. Conclusions: Silver cation exhibit a preference for AsW9 in a ratio of 3 to 2. This ratio can be associated to a sandwich type arrangement, with two trilacunary Keggin building blocks incorporating 3 metal cations in a tetrahedral geometry.

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