Preparation and Characterization of Homogeneous Grafted Cellulose in DMAc/LiCl System
2013 ◽
Vol 312
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pp. 332-336
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Keyword(s):
The homogeneous grafting of methyl methacrylate (MMA) onto cellulose was carried out by using ammonium persulfate as an initiator. DMAc/LiCl was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of MMA onto cellulose. The efficient reaction conditions of the grafting reaction were confirmed by weighing methods. The results showed that the efficient reaction conditions were as follows: reaction time, 2h; mass ratio of MMA/cellulose, 1/1(g/g); mass ratio of initiator/cellulose, 6/50 (g/g); and reaction temperature, 80°C. Under these conditions, the GP of homogeneous grafted cellulose can reach 76%. The grafted polymer was characterized by FTIR, SEM and TG-DTA.
2013 ◽
Vol 781-784
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pp. 526-530
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Keyword(s):
2012 ◽
Vol 581-582
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pp. 164-167
2011 ◽
Vol 396-398
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pp. 2342-2345
2012 ◽
Vol 581-582
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pp. 301-304
2012 ◽
Vol 624
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pp. 252-255
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Keyword(s):
2012 ◽
Vol 535-537
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pp. 2340-2344
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2014 ◽
Vol 670-671
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pp. 148-152