Effects of Stabilization Temperature on the Chemical and the Physical Properties of Polyacrylonitrile Stabilized Fibers

2015 ◽  
Vol 1112 ◽  
pp. 402-405
Author(s):  
Norhaniza Yusof ◽  
Ahmad Fauzi Ismail ◽  
Juhana Jaafar ◽  
W.N.W. Salleh ◽  
H. Hasbullah
Keyword(s):  
Tensile Strength ◽  
Physical Properties ◽  
Carbon Fibers ◽  
Chemical Structure ◽  
Young Modulus ◽  
Precursor Fiber ◽  
Stabilization Time ◽  
Ftir Studies ◽  
Stabilization Temperature ◽  
Mechanical Strengths

The present work dealt with the preparation of carbon fibers from Polyacrylonitrile (PAN)/ acrylamide (AM) fibers via a solvent-free coagulation process. The PAN/AM fibers were stabilized in an oxidizing atmosphere at various temperatures (200, 250, 275, and 300 °C), while the stabilization time was fixed at thirty minutes. The effects of stabilization temperature on the chemical and the physical properties of the prepared stabilized fibers were studied. The chemical structure evolutions of stabilized fibers (SFs) from the precursor fiber were observed with FTIR studies, whereas the microstructure properties were thoroughly characterized with SEM studies. The mechanical strengths of the SFs were obtained from the Young Modulus and the tensile strength analyses. Stabilization temperature at 275°C had been identified as the optimum stabilization temperature for the PAN/AM fibers.

scholarly journals Mesophase Pitch-Based Carbon Fibers: Accelerated Stabilization of Pitch Fibers under Effective Plasma Irradiation-Assisted Modification

Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6382
Author(s):  
Yuanshuo Peng ◽  
Ruixuan Tan ◽  
Yue Liu ◽  
Jianxiao Yang ◽  
Yanfeng Li ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Tensile Strength ◽  
Heating Rate ◽  
Carbon Fibers ◽  
High Performance ◽  
Low Cost ◽  
Tensile Modulus ◽  
Mesophase Pitch ◽  
Stabilization Time ◽  
Plasma Irradiation

Stabilization is the most complicated and time-consuming step in the manufacture of carbon fibers (CFs), which is important to prepare CFs with high performance. Accelerated stabilization was successfully demonstrated under effective plasma irradiation-assisted modification (PIM) of mesophase pitch fibers (PFs). The results showed that the PIM treatment could obviously introduce more oxygen-containing groups into PFs, which was remarkably efficient in shortening the stabilization time of PFs with a faster stabilization heating rate, as well as in preparing the corresponding CFs with higher performance. The obtained graphitized fiber (GF-5) from the PF-5 under PIM treatment of 5 min presented a higher tensile strength of 2.21 GPa, a higher tensile modulus of 502 GPa, and a higher thermal conductivity of 920 W/m·K compared to other GFs. Therefore, the accelerated stabilization of PFs by PIM treatment is an efficient strategy for developing low-cost pitch-based CFs with high performance.

scholarly journals Influence of boric acid on radial structure of oxidized polyacrylonitrile fibers

e-Polymers ◽  
2019 ◽  
Vol 19 (1) ◽  
pp. 79-86
Author(s):  
Xue-Fei Wang ◽  
Xiao-Long Zhu ◽  
Chi Jiang ◽  
Jian-Min Guan ◽  
Xin Qian ◽  
...  
Keyword(s):  
Boric Acid ◽  
Carbon Fibers ◽  
High Performance ◽  
Boron Content ◽  
Fiber Surface ◽  
Thermal Stabilization ◽  
Stabilization Time ◽  
Radial Structure ◽  
Stabilization Temperature ◽  
Pan Fibers

AbstractThe surface modification of polyacrylonitrile (PAN) fibers with boric acid was utilized to modulate the homogeneity of the radial structure of the PAN fibers during thermal stabilization. Exothermic peaks of the fibers were put off by boric acid, and unreacted nitrile groups of the oxidized PAN fibers increased with the boron content, indicating that boric acid on the fiber surface had an retardant effect on the thermal stabilization of PAN fibers. The relative skin thicknesses of the oxidized PAN fibers were quantitatively measured by sulfuric acid etching and SEM observation. The value increased obviously with the boron content, which could be further elevated by increasing stabilization time or decreasing stabilization temperature. Oxidized PAN fibers with more homogeneous radial structure can thus be obtained with the modification of boric acid, which might be beneficial for the preparation of high performance carbon fibers.

DURIMPHY

Alloy Digest ◽  
2007 ◽  
Vol 56 (2) ◽  
Keyword(s):  
Tensile Strength ◽  
Corrosion Resistance ◽  
Yield Strength ◽  
Physical Properties ◽  
Precipitation Hardening ◽  
Heat Treating ◽  
High Yield ◽  
High Yield Strength ◽  
Precision Alloys ◽  
Very High

Abstract Durimphy is a maraging steel with 1724 MPa (250 ksi) tensile strength and a very high yield strength due to precipitation hardening. This datasheet provides information on composition, physical properties, hardness, and tensile properties. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: FE-140. Producer or source: Metalimphy Precision Alloys.

CENTRI-CAST GRAY IRON 50

Alloy Digest ◽  
1981 ◽  
Vol 30 (8) ◽  
Keyword(s):  
Tensile Strength ◽  
Shear Strength ◽  
Physical Properties ◽  
Machine Tools ◽  
Heat Treating ◽  
Gray Iron ◽  
Centrifugally Cast ◽  
Wide Range ◽  
Nominal Tensile Strength ◽  
Cast Gray Iron

Abstract CENTRI-CAST GRAY IRON 50 is a centrifugally cast gray iron with a nominal tensile strength of 50,000 psi. It is cast in the form of tubing which has a wide range of uses in applications where size and shape are of paramount importance and freedom from pattern cost is an important consideration. Among its many applications are farm machinery, seals, bushings, machine tools and general machinery uses. This datasheet provides information on composition, physical properties, microstructure, hardness, elasticity, tensile properties, and compressive and shear strength as well as fatigue. It also includes information on casting, heat treating, machining, and surface treatment. Filing Code: CI-51. Producer or source: Federal Bronze Products Inc..

CENTRI-CAST GRAY IRON 55

Alloy Digest ◽  
1979 ◽  
Vol 28 (9) ◽  
Keyword(s):  
Tensile Strength ◽  
Shear Strength ◽  
Physical Properties ◽  
Surface Treatment ◽  
Heat Treating ◽  
Gray Iron ◽  
Centrifugally Cast ◽  
Wide Range ◽  
Nominal Tensile Strength ◽  
Cast Gray Iron

Abstract CENTRI-CAST GRAY IRON 55 is a centrifugally cast gray iron with a nominal tensile strength of 55,000 psi. It is produced in the form of tubing which has a wide range of uses in applications where size and shape are of paramount importance and freedom from pattern cost is an important consideration. Typical applications are seals, bushings, farm machinery, casings and general machinery uses. This datasheet provides information on composition, physical properties, microstructure, hardness, elasticity, tensile properties, and compressive and shear strength as well as fatigue. It also includes information on casting, heat treating, machining, and surface treatment. Filing Code: CI-48. Producer or source: Federal Bronze Products Inc..

WIELAND-FX9

Alloy Digest ◽  
2011 ◽  
Vol 60 (8) ◽  
Keyword(s):  
Tensile Strength ◽  
Corrosion Resistance ◽  
Physical Properties ◽  
Tensile Properties ◽  
Cold Work ◽  
Heat Treating ◽  
High Manganese ◽  
Bronze Alloy ◽  
Good Strength

Abstract Wieland-FX9 is a high-manganese bronze alloy that has good strength and is available in numerous cold work tempers related to its minimum tensile strength. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties. It also includes information on corrosion resistance as well as forming, heat treating, and joining. Filing Code: Cu-801. Producer or source: Wieland Metals Inc..

DOGAL 600 and 800 DP

Alloy Digest ◽  
2010 ◽  
Vol 59 (12) ◽  
Keyword(s):  
Tensile Strength ◽  
Physical Properties ◽  
Surface Treatment ◽  
Tensile Properties ◽  
High Strength Steels ◽  
High Strength

Abstract Dogal 600 and 800 DP are high-strength steels with a microstructure that contains ferrite, which is soft and formable, and martensite, which is hard and contributes to the strength of the steel. The designation relates to the lowest tensile strength. This datasheet provides information on composition, physical properties, hardness, and tensile properties. It also includes information on forming, joining, and surface treatment. Filing Code: CS-160. Producer or source: SSAB Swedish Steel Inc. and SSAB Swedish Steel.

LUCEFIN GROUP C30 (1.0528), C30E (1.1178), C30R (1.1179)

Alloy Digest ◽  
2020 ◽  
Vol 69 (9) ◽  
Keyword(s):  
Tensile Strength ◽  
Physical Properties ◽  
Tensile Properties ◽  
Heat Treating ◽  
High Tensile Strength ◽  
Medium Carbon ◽  
Alloy Steels ◽  
Cold Worked ◽  
Lower Carbon

Abstract Lucefin Group C30, C30E, and C30R are medium-carbon, non-alloy steels that are used in the normalized, cold worked, or quenched and tempered condition. C30E and C30R may also be flame or induction hardened. C30, C30E, and C30R are widely used for small, moderately stressed parts, where higher strength levels are needed than can be achieved in the lower carbon grades, and also where toughness is more important than high tensile strength. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties. It also includes information on forming, heat treating, machining, and joining. Filing Code: CS-206. Producer or source: Lucefin S.p.A.

TOUGHMET 2CX

Alloy Digest ◽  
2013 ◽  
Vol 62 (6) ◽  
Keyword(s):  
Tensile Strength ◽  
Wear Resistance ◽  
Corrosion Resistance ◽  
Physical Properties ◽  
Tensile Properties ◽  
Coefficient Of Friction ◽  
Loading Conditions ◽  
Severe Loading

Abstract ToughMet 2 CX is a Cu-9Ni-6Sn alloy that combines low coefficient of friction with wear resistance. ToughMet alloys are a line of spinodal hardened Cu-Ni antigalling alloys for bearings capable of performing with a variety of shafting materials and lubricants. The alloys combine a high lubricity with wear resistance in these severe loading conditions. ToughMet 2CX in the cast and spinodally hardened (CX) condition exhibits tensile strength in excess of 724 MPa (105 ksi) and hardness exceeding HRC 27 with excellent machinability. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties. It also includes information on corrosion resistance as well as forming. Filing Code: Cu-819. Producer or source: Materion Brush Performance Alloys.

BRUSH ALLOY 190

Alloy Digest ◽  
1968 ◽  
Vol 17 (12) ◽  
Keyword(s):  
Tensile Strength ◽  
Corrosion Resistance ◽  
Physical Properties ◽  
Surface Treatment ◽  
Tensile Properties ◽  
Heat Treating ◽  
Copper Strip ◽  
Beryllium Copper ◽  
Heat Treated

Abstract Brush Alloy 190 is a mill-heat treated beryllium copper strip with a tensile strength up to 190,000 psi. It eliminates the need of customer heat-treating by providing high properties combined with exceptional formability. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fatigue. It also includes information on corrosion resistance as well as forming, heat treating, joining, and surface treatment. Filing Code: Cu-194. Producer or source: Brush Beryllium Company.

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