Preparation and Wear Properties of (Al3Zr+ZrB2)P/2124 Composites Material with In Situ Process

2012 ◽  
Vol 616-618 ◽  
pp. 1736-1740
Author(s):  
Lei Jiao ◽  
Yu Tao Zhao ◽  
Zhong Zhong Zhang ◽  
Yan Wei Yang ◽  
Ming Rui Zhang

With pulse magnetic field, it is use 2124-K2ZrF6-KBF4 as matrix metal to produce chemical reaction to gain (Al3Zr+ZrB2) p/2124 composite materials in this paper. In this paper, For the sake of researching the microstructure, the morphology, the size and the matrix distribution characteristics of the reinforced grain of prepared composite material , those test methods are used, such as optical microscopy, scanning electron microscope, X-ray diffraction analysis and so on. We will research the magnetic field strength how to influence size and distribution of Al3Zr +ZrB2 particle and the abrasion performance of (Al3Zr+ZrB2)P/2124 composite materials in the room temperature. Wear experiment is proceeding in the CETR UMT 3-V the testing machine and sliding friction is friction way with pin-disc but without lubricant, then analyzes the wear mechanism.

2011 ◽  
Vol 189-193 ◽  
pp. 1647-1651
Author(s):  
Ying Wang ◽  
Yong Hong Zhang

Vanadium-Chromium composite layer is formed on the surface of cast steel by the method of V-EPC cast penetration. The dry sliding friction wear properties of composite layer are studied on MM200 friction wear testing machine in this paper. The wear surface feature of samples is also observed by SEM and the wear mechanism of samples is analyzed. The result has shown that comparing with the matrix, the wear resistance of composite layer is advanced evidently. The wear rate of composite layer is only eighth to matrix. With the increase of load and the decrease of Vanadium iron in penetrating regent, the wear rate of composite layer increase. The mechanism of composite layer is mainly oxidation and fatigue flake produced by the initiation and expansion of crack.


CrystEngComm ◽  
2020 ◽  
Vol 22 (34) ◽  
pp. 5606-5612
Author(s):  
Tsunehisa Kimura ◽  
Hayato Kashiwagi ◽  
Fumiko Kimura ◽  
Shigeru Horii ◽  
Kazuki Takeda ◽  
...  

The orientation loss of microcrystals during solidifying the matrix in a magnetic field was modeled. In situ X-ray diffraction results obtained for the consolidation process of DyBa2Cu3Oy microcrystal suspension were explained by the model presented.


2016 ◽  
Vol 25 (5-6) ◽  
pp. 165-169
Author(s):  
C. Rajaravi ◽  
P.R. Lakshminarayanan

AbstractThe paper describes a different condition of pouring temperature by sand and permanent mould to produce A356-6 wt% TiB2 metal matrix composites by in-situ method salt metal reaction route. The observation of SEM micrographs shows particle distribution of the TiB2 and it appears in hexagonal shape in Al matrix. The results of X-ray diffraction (XRD) analysis confirmed the formation of those TiB2 particulates and the results showed TiB2 particles are homogeneously dispersed throughout the matrix metal. Subsequent structure-property evaluation studies indicated sub-micron size reinforcement of in-situ formed TiB2 particles with improved physical and mechanical properties as compared to sand and permanent mould of Al-TiB2 composites. From, the permanent mould Al-TiB2 composite has an advantage of increase the properties over sand mould Al-TiB2 composite.


Author(s):  
Deepak Mehra ◽  
M.M. Mahapatra ◽  
S. P. Harsha

The purpose of this article is to enhance the mechanical properties and wear resistance of the RZ5 alloy used in the aerospace application by adding TiC particles. The present study discusses processing of in-situ RZ5-TiC composite fabricated by self-propagating high temperature (S.H.S.) method and its wear behavior. The effects of TiC particle on mechanical and microstructural properties of the composite are studied. The wear test is performed by varying the sliding distance and applied load. The composite is characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). The results exhibited the properties like strength and hardness of RZ5-10wt%TiC composite has been increased considerably, while grain size is decreased as compared to the RZ5 alloy. The fractography indicated mixed mode (quasi-cleavage and ductile feature) failure of the composites. The wear results showed improvement in wear resistance of the composite. The FESEM showed dominate wear mechanisms are abrasion, ploughing grooves.


2011 ◽  
Vol 415-417 ◽  
pp. 170-173
Author(s):  
Jing Wang ◽  
Si Jing Fu ◽  
Yi Chao Ding ◽  
Yi San Wang

A wear resistant TiC-Cr7C3/Fe surface composite was produced by cast technique and in-situ synthesis technique. The microstructure and dry-sliding wear behavior of the surface composite was investigated using scanning electron microscope(SEM), X-ray diffraction(XRD) and MM-200 wear test machine. The results show that the surface composite consists of TiC and Cr7C3as the reinforcing phase, α-Fe and γ-Fe as the matrix. The surface composite has excellent wear-resistance under dry-sliding wear test condition with heavy loads.


2012 ◽  
Vol 59 (2) ◽  
Author(s):  
Nurulhuda Bashirom ◽  
Nurzatil Ismah Mohd Arif

This paper presents a study on the effect of milling speed on the synthesis of Cu-WC nanocomposites by mechanical alloying (MA). The Cu-WC nanocomposite with nominal composition of 25 vol.% of WC was produced in-situ via MA from elemental powders of copper (Cu), tungsten (W), and graphite (C). These powders were milled in the high-energy “Pulverisette 6” planetary ball mill according to composition Cu-34.90 wt% W-2.28 wt% C. The powders were milled in different milling speed; 400 rpm, 500 rpm, and 600 rpm. The milling process was conducted under argon atmosphere by using a stainless steel vial and 10 mm diameter of stainless steel balls, with ball-to-powder weight ratio (BPR) 10:1. The as-milled powders were characterized by X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). XRD result showed the formation of W2C phase after milling for 400 rpm and as the speed increased, the peak was broadened. No WC phase was detected after milling. Increasing the milling speed resulted in smaller crystallite size of Cu and proven to be in nanosized. Based on SEM result, higher milling speed leads to the refinement of hard W particles in the Cu matrix. Up to the 600 rpm, the unreacted W particles still existed in the matrix showing 20 hours milling time was not sufficient to completely dissolve the W.


2011 ◽  
Vol 52-54 ◽  
pp. 842-845 ◽  
Author(s):  
Jian Feng Zhu ◽  
Wen Wen Yang ◽  
Yi Ping Gong

TiAl/Ti2AlC in situ composite was successfully fabricated by hot-press-assisted reaction process from the mixture of Ti, Al and carbon black. The phase formation and transformation were investigated in detail by X-ray diffraction (XRD) and the morphology characteristics were also studied by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The results show that when the mixed powders were hot pressed at 1300 °C for 1 h, full dense and highly pure TiAl/Ti2AlC composite was synthesized. The TiAl was the matrix phase and the in situ synthesized Ti2AlC was reinforcing phase. The reaction process was also discussed.


2013 ◽  
Vol 550 ◽  
pp. 107-113
Author(s):  
Xiao Lu Gong ◽  
Fei Zhao ◽  
Di Zhang

The tribological performances of in-situ (TiB + TiC) / Ti1100 composites prepared by casting and the matrix alloy were tested by pin-on disc mode. The worn surface and wear debris were investigated by SEM. The models of the composites during the wear process were simulated by ABAQUS FEA software. The analysis shows the stress distributions inside the composites under the different shear stress. The wear mechanism of the composites is probed.


JOM ◽  
2020 ◽  
Vol 73 (1) ◽  
pp. 223-232 ◽  
Author(s):  
Jan Čapek ◽  
Efthymios Polatidis ◽  
Michal Knapek ◽  
Christophe Lyphout ◽  
Nicola Casati ◽  
...  

AbstractThe deformation behavior of additively manufactured Alloy 718 in as-built condition and after annealing was studied in situ under tensile loading along the build direction. Pre-characterization by synchrotron X-ray diffraction and electron microscopy revealed a significant amount of γ″ precipitates in the as-built samples, whereas the γ″ phase was entirely consumed and needle-like δ precipitates appeared in the annealed sample. In situ neutron diffraction (ND) and acoustic emission (AE) enabled indirect observation of the role of the precipitates on the mechanical behavior. ND provided information on the load accommodation in the matrix, while AE detected a strong signal from the interaction of dislocations with the δ-phase precipitates during deformation of the annealed samples. The results imply that in the annealed samples the matrix sheds the load to the precipitates, while in the as-built material the matrix bares a significant load.


Author(s):  
Wei Jiang ◽  
Lida Shen ◽  
Kai Wang ◽  
Zhanwen Wang ◽  
Zongjun Tian

The Ni-Co/SiC composite coatings were prepared via jet electrodeposition in the presence of magnetic field. The microstructure and texture orientation of the composite coatings were analyzed via field emission scanning electron microscopy, three-dimensional profiling, and X-ray diffraction. The microhardness and wear resistance were characterized by a microhardness tester and a friction–abrasion testing machine. The results indicated that nano-SiC particles improved the surface morphology of the Ni-Co/SiC composite coating. In jet electrodeposition, globular structure aggregation began to form protrusions in the Ni-Co/SiC composite coating due to nanoparticle agglomeration when 6 g/L of nano-SiC was added. The Ni-Co/SiC (6 g/L) composite coating became uniform and densification by jet electrodeposition in magnetic field, with higher microhardness and better wear resistance. The microhardness of the Ni-Co/SiC composite coating increased to 626 ± 14 HV, and the corresponding friction coefficient was as low as 0.317.


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