Effect of Milling Time on Particle Size and Surface Morphology of Commercial Zeolite by Planetary Ball Mill

2013 ◽  
Vol 795 ◽  
pp. 711-715 ◽  
Author(s):  
N.Z.F. Mukhtar ◽  
M.Z. Borhan ◽  
Mohamad Rusop ◽  
Saifollah Abdullah
Keyword(s):  
Particle Size ◽  
Ball Milling ◽  
Ball Mill ◽  
Milling Time ◽  
Size Range ◽  
Synthetic Zeolite ◽  
Inorganic Materials ◽  
Planetary Ball Mill ◽  
Dry Grinding ◽  
Particle Sizer

Ball milling is a top down approach and a method to reduce size of particle while Zeolite is a valuable inorganic materials having wide variety of applications. In this paper, ball milling of commercial synthetic Zeolite powder was studied with their time varied. Wet ball milling was selected as a potential means to decrease the particle size of Zeolite over dry grinding. The parameters that included in this study were rotational speed, balls to powder ratio, water to powder ratio and milling time. These nanozeolite were characterized via Zeta-sizer nanoseries of particle sizer, FESEM, and also FTIR. Results showed that commercial synthetic Zeolite powder with particle size larger than 45 μm may be reduced into the size range between 0.2 0.3 μm by planetary ball mill.

Evaluation of particle size reduction and agglomeration in dry grinding of natural quartz in a planetary ball mill

2020 ◽  
Vol 368 ◽  
pp. 149-159 ◽  
Author(s):  
Pedro L. Guzzo ◽  
Filipe B. Marinho de Barros ◽  
Bruno R. Soares ◽  
Juliano B. Santos
Keyword(s):  
Particle Size ◽  
Ball Mill ◽  
Size Reduction ◽  
Planetary Ball Mill ◽  
Natural Quartz ◽  
Particle Size Reduction ◽  
Dry Grinding

Microwave Sintering and Electric Properties of ZnO Varistor Ceramics

2013 ◽  
Vol 833 ◽  
pp. 75-79 ◽  
Author(s):  
Xin Xin He ◽  
Guo You Gan ◽  
Ji Kang Yan ◽  
Jing Hong Du ◽  
Jia Ming Zhang ◽  
...  
Keyword(s):  
Particle Size ◽  
Ball Mill ◽  
Milling Time ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
Electric Properties ◽  
Planetary Ball Mill ◽  
Zno Varistor ◽  
C Doping ◽  
Zno Powder

The ZnO varistor ceramics were fabricated through microwave sintering at 800~1150°C using ZnO powder doped and undoped TiO2 prepared by planetary ball mill. And the effects of milling time, sintering temperature and doping on microwave sintering technique have been studied. The result shows that the powder is more homogeneously and with smaller particle size with the increasing of milling time, therefore the electric properties is improved. However the particle size and the electric properties tend towards stability after 20h milling time. The density and electric properties increase with the increasing of sintering temperature, but decrease sharply at 1100°C, so the best sintering temperature is 1100°C. Doping TiO2 improves the electric properties of ZnO, however the electric properties decrease with more than 2.5% doping.

Influence of Ball Milling Parameters on Preparation of Ti50Cu23Ni20Sn7 Amorphous Alloys Powder

2011 ◽  
Vol 55-57 ◽  
pp. 819-824
Author(s):  
Ge Wang ◽  
Qiang Li ◽  
Ying Gao ◽  
Jing Na Gao ◽  
Yu Ying Zhu ◽  
...  
Keyword(s):  
Mechanical Alloying ◽  
Ball Milling ◽  
Amorphous Alloys ◽  
Ball Mill ◽  
Milling Time ◽  
Rotational Velocity ◽  
Weight Ratio ◽  
High Energy ◽  
Planetary Ball Mill ◽  
Milling Parameters

Ti50Cu23Ni20Sn7 amorphous alloys powder was prepared by mechanical alloying (MA) in a high-energy planetary ball mill. Milling parameters such as rotational velocity of ball mill, ball to powder weight ratio as well as milling time were throughly investigated. Mechanism of mechanical alloying was throughly discussed.

Production of Dispersion-Strengthened Cu-TiB2 Alloys by Ball-Milling and Spark-Plasma Sintering

2007 ◽  
Vol 534-536 ◽  
pp. 1489-1492 ◽  
Author(s):  
Dae Hwan Kwon ◽  
Jong Won Kum ◽  
Thuy Dang Nguyen ◽  
Dina V. Dudina ◽  
Pyuck Pa Choi ◽  
...  
Keyword(s):  
Electrical Conductivity ◽  
Ball Milling ◽  
Spark Plasma Sintering ◽  
Ball Mill ◽  
Milling Time ◽  
Rotation Speed ◽  
Sintering Temperature ◽  
Milled Powder ◽  
Plasma Sintering ◽  
Spark Plasma

Dispersion-strengthened copper with TiB2 was produced by ball-milling and spark plasma sintering (SPS).Ball-milling was performed at a rotation speed of 300rpm for 30 and 60min in Ar atmosphere by using a planetary ball mill (AGO-2). Spark-plasma sintering was carried out at 650°C for 5min under vacuum after mechanical alloying. The hardness of the specimens sintered using powder ball milled for 60min at 300rpm increased from 16.0 to 61.8 HRB than that of specimen using powder mixed with a turbular mixer, while the electrical conductivity varied from 93.40% to 83.34%IACS. In the case of milled powder, hardness increased as milling time increased, while the electrical conductivity decreased. On the other hand, hardness decreased with increasing sintering temperature, but the electrical conductiviey increased slightly

Preparation of High Density BaZr0.97Y0.03O3-δ Ceramic and its Interaction with Titanium Melt

2018 ◽  
Vol 768 ◽  
pp. 261-266 ◽  
Author(s):  
Ju Yun Kang ◽  
Guang Yao Chen ◽  
Bao Tong Li ◽  
Zi Wei Qin ◽  
Xiong Gang Lu ◽  
...  
Keyword(s):  
Particle Size ◽  
Ball Milling ◽  
Milling Time ◽  
Sintered Pellet ◽  
Conventional Solid State Reaction ◽  
Industrial Grade ◽  
Minimum Particle Size ◽  
Ni Alloy ◽  
Improved Stability ◽  
Ball Milling Time

In this paper, the BaZrO3(BZ) and BaZr0.97Y0.03O3-δ(BZY3) powders were prepared by using the industrial grade BaCO3, ZrO2and Y2O3powders combining the conventional solid state reaction. The BaZrO3(BZ) and BaZr0.97Y0.03O3-δ(BZY3) ceramics were fabricated at 1750°C. The effect of ball milling time and sintering aid (TiO2) on the sinterability of BaZr0.97Y0.03O3-δ(BZY3) ceramics were investigated, and the improved stability of BaZrO3refractory with Y2O3additive were studied according to the refractory-metal interaction. The results revealed that the particle size of BZY3 powders decreased first and then increased with the increasing of ball milling time from 6h to 12h, and the minimum particle size was only 2.252μm at 8h. When 2wt.%TiO2was added, the sintered pellet of BZY3 was the most densest and the relative density was above 95%. After melting the Ti2Ni alloy on the BZY and BZ ceramics, the thickness erosion layer of BaZrO3and BZY3refractories and Ti2Ni alloy is approximately 50μm and 20μm respectively, showing that BZY3 was more stable than BaZrO3refractory.

High Energy Milling of WС-FeСr Cemented Carbide

2019 ◽  
Vol 799 ◽  
pp. 136-141
Author(s):  
Marek Tarraste ◽  
Jakob Kübarsepp ◽  
Kristjan Juhani ◽  
Märt Kolnes ◽  
Mart Viljus
Keyword(s):  
Particle Size ◽  
Ball Mill ◽  
Size Range ◽  
High Energy ◽  
Cemented Carbide ◽  
Cemented Carbides ◽  
Binder Phase ◽  
Metal Powders ◽  
Powder Mixtures ◽  
High Energy Milling

During production of cemented carbides hard and brittle tungsten carbide (WC) and ductile metal powders (mainly from Fe-group) are milled together. Complete milling results in a Gaussian distribution and narrow particle size range of the milled powder which promote the homogeneity and improve the properties of sintered composites. Cobalt, conventional metal employed in cemented carbides, possesses good comminution characteristics with WC powder. However, its toxicity and fluctuating price pushes researchers to find suitable alternatives and Fe-based alloys have shown most promising results. Cemented carbides with the Fe-Cr system as metal binder phase have potential to perform better than regular WC-Co composites in corrosive and oxidative environments. The goal of this paper was to prepare uniform cemented carbides powders with relatively high fraction of stainless Fe-Cr steel. To achieve a uniform powder mixture is a challenge at high ductile steel fraction. High energy milling (HEM) is a powerful technique for achieving (ultra) fine powder mixtures with narrow powder size range. HEM was carried out in a novel high energy ball mill RETSCH Emax. Milling in tumbling ball mill, which is the most widely used method, was employed for reference. Prepared powder mixtures were characterised in terms of particle size, size distribution and shape. In addition, powder mixtures were consolidated via spark plasma sintering to evaluate the effect of the milling method and the duration on the microstructure of final cemented carbide.

scholarly journals Synthesis of Nanocrystalline WC Single-Phase Refractory via Mechanical Milling

2011 ◽  
Vol 2011 ◽  
pp. 1-5 ◽  
Author(s):  
Mansour Razavi ◽  
Mohammad Reza Rahimipour ◽  
Rahim Yazdani-Rad
Keyword(s):  
Mechanical Milling ◽  
Ball Mill ◽  
Single Phase ◽  
Milling Time ◽  
Raw Materials ◽  
Planetary Ball Mill ◽  
Crystalline Size ◽  
Nanometer Scale

In this paper the possibility of production of nanocrystalline WC single-phase by mechanical milling has been investigated. The raw materials containing tungsten and carbon with WC as nucleation were milled in a planetary ball mill and sampled in different times. Studies showed that after 75 hours of milling the WC with W2C was produced and remained constant in higher milling time. Adding WC to raw materials at the beginning process leads to the fact that after 50 hours of milling only WC was synthesized without undesirable W2C phase. This material remained stable until higher times of milling too. From broadening of XRD peaks, the crystalline size in synthesized WC was estimated in nanometer scale which lower than the system containing primary WC, and it means that the strain in this system was lower than first system.

Different Cr Contents in Nanostructured Fe-Ni-Cr Alloys Prepared by Mechanical Alloying

2012 ◽  
Vol 531-532 ◽  
pp. 437-441 ◽  
Author(s):  
Qi He ◽  
Tao Liu ◽  
Jian Liang Xie
Keyword(s):  
Particle Size ◽  
Mechanical Alloying ◽  
Ball Milling ◽  
Lattice Distortion ◽  
Milling Time ◽  
Nanocrystalline Powders ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ball Milling Time ◽  
Scanning Electron

Fe-Ni-Cr alloy powders with the different components were prepared by Mechanical Alloying (MA). The phase structure, grain size, micro-strain and lattice distortion were determined with X-ray diffraction. The morphology and particle size of the powders were observed and analyzed using a field emission scanning electron microscopy. The results showed that the Fe-Ni-Cr nanocrystalline powders could be obtained by MA. The ball milling time could be reduced with increasing amount of Cr, resulting the formation of Fe-Ni-Cr powders. With the increasing amount of Cr, the speed of Ni diffusion to Fe lattice approaching saturation became more rapid. The particle size got smaller as the ball milling went further; the extent of micro-strain and distortion of lattice intensified; the solid solubility of Ni and Cr in Fe was increased. Finally the super-saturated solid solution of Fe was obtained.

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