Fabrication and Characterization of Superhydrophobic Film on Titanium Substrate

2013 ◽  
Vol 834-836 ◽  
pp. 29-32
Author(s):  
Dong Ping Long ◽  
Jian Rong Xue ◽  
Zhi Xin Yan
Keyword(s):  
Contact Angle ◽  
Titanium Substrate ◽  
Electrochemical Anodization ◽  
Porous Structures ◽  
Test Results ◽  
Nano Structure ◽  
Low Surface Energy ◽  
Nano Structures ◽  
Fluorinated Silane

TiO2 nano film with different nano structure were prepared on the surfaces of titanium TA1 and titanium alloy TC4 via electrochemical anodization. The surface morphology was observed with SEM, and it is found that TiO2 films prepared on TA1 surface have porous structures, while the TiO2 films synthesized on TC4 surface look like nano rod. The contact angle(CA) test results show that the TiO2 nano film prepared on TA1 is hydrophilicity and the CA is about 19°,the film on the TC4 is super hydrophilicity and its CA is smaller than 2°. After combined with fluorinated silane the self-assembled film synthesized on the surfaces and they are superhy- drophobic and the Contact angle is 150° and 158° respectively. It is concluded that both nano- structures and fluoroalkysilanes with low surface energy have play an important role in the wettability with the contact angle is more than 150°. The surface only have nano roughness without the low energy does not show superhydrophobicity.

Fabrication and Characterization of a Superhydrophobic Low-Density Polyethylene Film

2012 ◽  
Vol 557-559 ◽  
pp. 1834-1837
Author(s):  
Jun Liang Wu ◽  
Hui Ping Zhang ◽  
Xu Nan Wang
Keyword(s):  
Contact Angle ◽  
Water Contact Angle ◽  
Energy Materials ◽  
Water Contact ◽  
Simple Method ◽  
Ldpe Film ◽  
Low Surface Energy ◽  
Special Surface ◽  
Superhydrophobic Property

A superhydrophobic LDPE film was obtained by a simple method in atmosphere without addition of low-surface-energy materials. The water contact angle of the superhydrophobic LDPE film are 155±1.9º. SEM shows that compared with common smooth LDPE film, a porous structure was obviously observed on the superhydrophobic LDPE film. Such a special surface microstructure may result in the superhydrophobic property. The effect of drying temperature and concentration on water contact angle were studied.

Effect of Etching and Modification on the Hydrophobic Angle of Epoxy/Poss Nanomaterials

2020 ◽  
Vol 15 (12) ◽  
pp. 1502-1507
Author(s):  
Yanhong Fang ◽  
Ping Wang ◽  
Lifang Sun ◽  
Linhong Wang
Keyword(s):  
Surface Roughness ◽  
Contact Angle ◽  
Hydrochloric Acid ◽  
Surface Energy ◽  
Stearic Acid ◽  
Acid Etching ◽  
Energy Materials ◽  
Nano Structure ◽  
Low Surface Energy ◽  
Long Time

In this study, simple and feasible methods are used to increase the hydrophobicity of EP-POSS, that is, etching with concentrated hydrochloric acid and concentrated ammonia water, followed by modification with polytetrafluoroethylene and stearic acid. The principle of the study is to increase the hydrophobic angle of EP-POSS by immersion in concentrated hydrochloric acid and concentrated ammonia for a sufficiently long time, followed by modification with low-surface-energy materials, i.e., polytetrafluoroethylene and stearic acid. The contact angle of EP-POSS increased from 100° to 133° after immersing in 3 mol/L hydrochloric acid for 12 min. Compared to hydrochloric acid, the surface roughness and contact angel were not changed significantly by immersing in concentrated ammonia for 4 hours. The contact angle was not changed obviously after immersing in 0.1 mol/L polytetrafluoroethylene for 24 h, and only changed from 135° to 136° when immersed in 0.1 mol/L stearic acid. It shows that PTFE and stearic acid hasn?t effectively grafted to the surface of EP-POSS, and has no effect to the micro-nano structure of EP-POSS. According to the experimental results, hydrochloric acid etching is the proper way to enhance EP-POSS contact angel. According to further investigates, it can be determined that treating EP-POSS at 40 °C for 12 min with 3 mol/L hydrochloric acid can significantly improve its hydrophobicity, thus, the hydrophobic performance of EP-POSS is considerably improved.

Preparation and Characterization of the Hydrophilic Polysulfone Ultrafiltration Membrane

2018 ◽  
Vol 1145 ◽  
pp. 85-89 ◽  
Author(s):  
Xi Wang ◽  
Zhi Ping Zhao ◽  
Peng Lu
Keyword(s):  
Contact Angle ◽  
Fourier Transform ◽  
Pore Size ◽  
Water Flux ◽  
Ultrafiltration Membrane ◽  
Test Results ◽  
Grafting Modification ◽  
Amination Reaction ◽  
Hydrophilic Monomer

In this study, the certain chloromethylated polysulfone ultrafiltration membrane (CMPSF) was prepared via nonsolvent-induced phase separation (NIPS) method. Then the hydrophilic monomer was grafted on the CMPSF membrane through quaternary amination reaction. The structure of membrane was characterized by Fourier transform infrared and the properties were measured by pore size, contact angle and membrane water flux. The contact angle test results show that the hydrophilic performance of the membrane is improved due to the grafting modification. Meanwhile, water flux has a tendency to decrease with the increase of the reaction time due to the decrease in pore size. This indicates the rejection of membrane will be improved.

Optimization and characterization of flavonoids extracted from Cannabis sativa fibers

2021 ◽  
pp. 004051752110277
Author(s):  
Qilu Cui ◽  
Jiawei Li ◽  
Chongwen Yu
Keyword(s):  
Chemical Structure ◽  
Cannabis Sativa ◽  
Ethanol Concentration ◽  
Extraction Process ◽  
Test Results ◽  
Hemp Fiber ◽  
Hemp Fibers ◽  
Structure Surface ◽  
Degumming Process

In this paper, the extraction process of flavonoids from hemp fibers was studied. Response surface methodology (RSM) analysis of the extraction parameters indicated that optimized results would be ethanol concentration 76 vol.%, bath ratio 1:50, and reaction time 139 min; therefore, an optimal extraction rate of flavonoids of 0.2275% can be obtained. The chemical structure, surface morphology and element composition of flavonoid extracts were analyzed. The test results indicated that hemp extract contains flavonoids, which can be used to extract flavonoids from hemp fiber, so as to comprehensively develop hemp fiber and reduce the discharge of waste liquid in the traditional degumming process.

scholarly journals Design and Experimental Characterization of L-CADEL v2, an Assistive Device for Elbow Motion

Sensors ◽  
2021 ◽  
Vol 21 (15) ◽  
pp. 5149
Author(s):  
Marco Ceccarelli ◽  
Mykhailo Riabtsev ◽  
Axel Fort ◽  
Matteo Russo ◽  
Med Amine Laribi ◽  
...  
Keyword(s):  
Elderly People ◽  
Operating Performance ◽  
Assistive Device ◽  
Test Results ◽  
Experimental Characterization ◽  
Elbow Motion ◽  
Laboratory Prototype

An experimental characterization is presented for an improved version of a wearable assistive device for elbow motion. The design is revised with respect to requirements for elbow motion assistance, looking at applications both in rehabilitation therapies and exercising of elderly people. A laboratory prototype is built with lightweight, portable, easy-to-use features that are verified with test results, whose discussion is also provided as a characterization of operating performance.

scholarly journals Fabrication and Evaluation of Nano-TiO2 Superhydrophobic Coating on Asphalt Pavement

Materials ◽  
2021 ◽  
Vol 14 (1) ◽  
pp. 211
Author(s):  
Hongfeng Li ◽  
Xiangwen Lin ◽  
Hongguang Wang
Keyword(s):  
Contact Angle ◽  
Stearic Acid ◽  
Asphalt Pavement ◽  
Asphalt Mixture ◽  
Waterborne Polyurethane ◽  
Superhydrophobic Coating ◽  
Nano Tio2 ◽  
Sem Image ◽  
Low Surface Energy ◽  
Water Damage

In order to address water damage of asphalt pavement, reduce the occurrence of water-related potholes, deformation, and other diseases, and improve the performance and service life of the pavement, a nano-TiO2 superhydrophobic coating (PSC) on asphalt pavement was prepared from waterborne polyurethane and nano-TiO2 modified by stearic acid. FT-IR measured stearic acid successfully modified low surface energy substance on the surface of nano-TiO2. The SEM image shows that the PSC has a rough surface structure. The contact angle and rolling angle of the PSC in the contact angle test are 153.5° and 4.7°, respectively. PSC has a super-hydrophobic ability, which can improve the water stability of the asphalt mixture. Although the texture depth and pendulum value have been reduced by 2.5% and 4.4%, respectively, they all comply with the standard requirements. After the abrasion resistance test, the PSC coating still has a certain hydrophobic ability. These results surface PSC coating can effectively reduce water damage on asphalt pavement, and has considerable application value.

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