Microstructural Characterization of Hydrogen Induced Cracking in TRIP Steels by EBSD

2014 ◽  
Vol 922 ◽  
pp. 412-417 ◽  
Author(s):  
A. Laureys ◽  
Tom Depover ◽  
Roumen H. Petrov ◽  
Kim Verbeken
Keyword(s):  
Retained Austenite ◽  
Electron Backscatter Diffraction ◽  
Mechanical Load ◽  
High Strength ◽  
Microstructural Characterization ◽  
Trip Steels ◽  
Multiphase Microstructure ◽  
Hydrogen Induced Cracking ◽  
Backscatter Diffraction

The present work evaluates hydrogen induced cracking in a high strength TRIP steel with a complex multiphase microstructure, containing ferrite, bainite, retained austenite, and some martensite. Each structural constituent demonstrates a different behavior in the presence of hydrogen and when deformed, the retained austenite transforms to martensite. The goal of this work is to understand the response of the hydrogen saturated multiphase structure to a mechanical load. A tensile test on notched samples combined with in-situ electrochemical hydrogen charging was carried out. The test was interrupted at certain specific points, before the macroscopic failure of the material. Hydrogen induced crack initiation and propagation were examined by studying several intermediate elongations. The microstructure of the samples was characterized by scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). The EBSD measurements allowed both microstructural and crystallographic characterization of the hydrogen induced crack surroundings. A correlation was found between the occurrence of martensite, which is known to be very susceptible to hydrogen embrittlement, and the initiation of hydrogen induced cracks. These cracks were located at the surface in specific high stressed regions. Finite element simulations indicated that these regions were induced due to the presence of the notch.

The Effect of Texture on the Stability of Retained Austenite in Al-Alloyed TRIP Steels

2011 ◽  
Vol 1296 ◽  
Author(s):  
Kemal Davut ◽  
Stefan Zaefferer
Keyword(s):  
Retained Austenite ◽  
Electron Backscatter Diffraction ◽  
High Strength ◽  
Trip Steels ◽  
Tension And Compression ◽  
Stable Austenite ◽  
Ebsd Technique ◽  
Face Centered ◽  
The Stability ◽  
Backscatter Diffraction

ABSTRACTSteels with transformation induced plasticity (TRIP) offer an excellent combination of high strength and ductility. The transformation of meta-stable austenite into martensite during straining leads to strong local hardening and prevents early localization of strain. Therefore, the mechanical properties of TRIP steels, including the damage resistance depend to a significant extent on the stability of retained austenite. The aim of this study was to evaluate the effect of texture on the stability of retained austenite. In order to compare the changes in both tension and compression the steel was deformed by a micro 3-point-bending device. The texture development upon bending was followed by electron backscatter diffraction (EBSD) technique. Based on a simple analysis using the relation between face centered cube (FCC) and body centered cube (BCC) shear geometries theoretically expected changes of texture components due to deformation are proposed. Using the results of this analysis the observed changes of the austenite texture due to deformation could be distinguished from those due to transformation, by comparing the experimental results with the theoretically expected behavior. From this comparison, austenite grains with “Brass (B) {011} <211>” and “Goss (G) {110} <100>” texture components were found to transform into martensite much easier than differently oriented grains.

The Influence of Deformation on Microstructure Evolution of Low Alloy TRIP Steel

2010 ◽  
Vol 638-642 ◽  
pp. 3531-3536
Author(s):  
Lucia Suarez ◽  
Josep Antonio Benito ◽  
Pablo Rodriguez-Calvillo ◽  
Daniel Casellas ◽  
Yvan Houbaert ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Electron Backscatter Diffraction ◽  
Physical And Mechanical Properties ◽  
Microstructural Characterization ◽  
Ferrite Matrix ◽  
Characterization Methods ◽  
Steel Microstructure ◽  
Trip Steels ◽  
Multiphase Microstructure

Low alloy transformation-induced plasticity aided (TRIP) steels have attracted much interest over the last years. TRIP steels were initially developed for automotive applications as they offer an excellent combination of strength and ductility at reasonable costs. These excellent mechanical properties mainly arise from a complex multiphase microstructure of a ferrite matrix and a dispersion of multiphase grains of bainite, martensite and metastable retained austenite. The relevant influence of microstructure on physical and mechanical properties makes metallographic study essential for an appropriate understanding and improvement of the mechanical behavior. An accurate microstructural characterization and quantification of the amount of the different constituents is indispensable to know how the stresses and strains are distributed within the different microstructural constituents. Among the different characterization methods commonly used electron backscatter diffraction (EBSD) appears to be the unique technique able to observe retained austenite grains often no larger than 1 μm. The present work shows the evolution of retained austenite while straining. Microstructural and textural evolution after different strains was examined by optical microscopy OM, EBSD and XRD techniques on TRIP800 steel. EBSD technique appears as a powerful tool for characterizing the complex multiphase steel microstructure and provides an accurate evaluation of the local crystallographic texture. It allows to measure orientation gradients within individual grains of each different phase. The distinction between some phases is observed.

scholarly journals Effect of Retained Austenite and Non-Metallic Inclusions on the Mechanical Properties of Resistance Spot Welding Nuggets of Low-Alloy TRIP Steels

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1064 ◽  
Author(s):  
Víctor H. Vargas Cortés ◽  
Gerardo Altamirano Guerrero ◽  
Ignacio Mejía Granados ◽  
Víctor H. Baltazar Hernández ◽  
Cuauhtémoc Maldonado Zepeda
Keyword(s):  
Mechanical Properties ◽  
Tensile Test ◽  
Retained Austenite ◽  
High Strength ◽  
Microstructural Characterization ◽  
Spot Welds ◽  
Trip Steels ◽  
Resistance Spot ◽  
Lap Shear ◽  
Metallic Inclusions

The combination of high strength and formability of transformation induced plasticity (TRIP) steels is interesting for the automotive industry. However, the poor weldability limits its industrial application. This paper shows the results of six low-alloy TRIP steels with different chemical composition which were studied in order to correlate retained austenite (RA) and non-metallic inclusions (NMI) with their resistance spot welded zones to their joints’ final mechanical properties. RA volume fractions were quantified by X-ray microdiffraction (µSXRD) while the magnetic saturation technique was used to quantify NMI contents. Microstructural characterization and NMI of the base metals and spot welds were assessed using scanning electron microscopy (SEM). Weld nuggets macrostructures were identified using optical microscopy (OM). The lap-shear tensile test was used to determine the final mechanical properties of the welded joints. It was found that NMI content in the fusion zone (FZ) was higher than those in the base metal and heat affected zone (HAZ). Whereas, traces of RA were found in the HAZ of highly alloyed TRIP steels. Lap-shear tensile test results showed that mechanical properties of spot welds were affected by NMI contents, but in a major way by the decomposition of RA in the FZ and HAZ.

Hydrogen effects on fracture of high-strength steels with different micro-alloying

2015 ◽  
Vol 33 (6) ◽  
pp. 515-527 ◽  
Author(s):  
Olga Todoshchenko ◽  
Yuriy Yagodzinskyy ◽  
Valentina Yagodzinska ◽  
Tapio Saukkonen ◽  
Hannu Hänninen
Keyword(s):  
Chemical Composition ◽  
Electron Backscatter Diffraction ◽  
High Strength Steels ◽  
Thermal Desorption Spectroscopy ◽  
High Strength ◽  
Constant Load ◽  
Carbon Steels ◽  
Hydrogen Induced Cracking ◽  
Load Tests ◽  
Backscatter Diffraction

AbstractConstant load tests of high-strength carbon steels with different micro-alloying using strengths in the range of 1000–1400 MPa were performed at ambient temperature under continuous electrochemical hydrogen charging. Hydrogen markedly affects delayed fracture of all the studied steels. Fractography of the studied steels shows that fracture mechanism depends on the chemical composition of the studied steels and hydrogen-induced cracking exhibits intergranular or transgranular character occurring often in the form of hydrogen flakes. The size and chemical composition of non-metallic inclusions are analyzed by scanning electron microscopy and energy-dispersive X-ray spectroscopy. Hydrogen-induced cracking initiates at TiN/TiC particles in steels with Ti alloying. Crack paths are studied with electron backscatter diffraction mapping to analyze crack initiation and growth. The thermal desorption spectroscopy method is used to analyze the distribution of hydrogen in the trapping sites. The mechanisms of hydrogen effects on fracture of high-strength steels are discussed.

Microstructure and Mechanical Properties of Cold-Rolled TRIP Steel Sheets

2011 ◽  
Vol 266 ◽  
pp. 280-283 ◽  
Author(s):  
Cai Nian Jing ◽  
Xiao Hui Chen ◽  
Ming Gang Wang ◽  
Qi Zhong Tian ◽  
Zuo Cheng Wang
Keyword(s):  
Retained Austenite ◽  
High Strength ◽  
Transformation Induced Plasticity ◽  
Trip Steels ◽  
Multiphase Microstructure ◽  
Steel Sheets ◽  
High Strength Level ◽  
Cold Rolled ◽  
Level 2 ◽  
Strength And Ductility

Transformation induced plasticity (TRIP) steels have complex multiphase microstructure composed of ferrite, bainite and retained austenite [1]. These metastable retained austenite can transforms into martensite during plastic deformation, which generates a TRIP effect resulting in excellent combination of high strength and ductility even at high strength level [2-5]. For this reason, the TRIP-aided steel sheets are suitable to fabricate automobile parts, as they can offer excellent formability without sacrifice the strength and safety requirement of the steel sheets. As a result, the development of TRIP-aided steels has been a very important issue in the automobile field.

scholarly journals On the interplay of microstructure and residual stress in LPBF IN718

2020 ◽  
Vol 56 (9) ◽  
pp. 5845-5867
Author(s):  
Itziar Serrano-Munoz ◽  
Tobias Fritsch ◽  
Tatiana Mishurova ◽  
Anton Trofimov ◽  
Daniel Apel ◽  
...  
Keyword(s):  
Residual Stress ◽  
Electron Backscatter Diffraction ◽  
Microstructural Characterization ◽  
Theoretical Models ◽  
Near Surface ◽  
Powder Bed ◽  
Rs Analysis ◽  
Scanning Strategies ◽  
Backscatter Diffraction

AbstractThe relationship between residual stresses and microstructure associated with a laser powder bed fusion (LPBF) IN718 alloy has been investigated on specimens produced with three different scanning strategies (unidirectional Y-scan, 90° XY-scan, and 67° Rot-scan). Synchrotron X-ray energy-dispersive diffraction (EDXRD) combined with optical profilometry was used to study residual stress (RS) distribution and distortion upon removal of the specimens from the baseplate. The microstructural characterization of both the bulk and the near-surface regions was conducted using scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). On the top surfaces of the specimens, the highest RS values are observed in the Y-scan specimen and the lowest in the Rot-scan specimen, while the tendency is inversed on the side lateral surfaces. A considerable amount of RS remains in the specimens after their removal from the baseplate, especially in the Y- and Z-direction (short specimen dimension and building direction (BD), respectively). The distortion measured on the top surface following baseplate thinning and subsequent removal is mainly attributed to the amount of RS released in the build direction. Importantly, it is observed that the additive manufacturing microstructures challenge the use of classic theoretical models for the calculation of diffraction elastic constants (DEC) required for diffraction-based RS analysis. It is found that when the Reuß model is used for the calculation of RS for different crystal planes, as opposed to the conventionally used Kröner model, the results exhibit lower scatter. This is discussed in context of experimental measurements of DEC available in the literature for conventional and additively manufactured Ni-base alloys.

scholarly journals Recent Advances in EBSD Characterization of Metals

Metals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 1097
Author(s):  
Íris Carneiro ◽  
Sónia Simões
Keyword(s):  
Grain Boundary ◽  
Electron Backscatter Diffraction ◽  
Microstructural Characterization ◽  
Grain Boundary Character Distribution ◽  
Grain Boundary Character ◽  
Recent Advances ◽  
Wide Range ◽  
Plane Distribution ◽  
Backscatter Diffraction

Electron backscatter diffraction (EBSD) has been attracting enormous interest in the microstructural characterization of metals in recent years. This characterization technique has several advantages over conventional ones, since it allows obtaining a wide range of characterization possibilities in a single method, which is not possible in others. The grain size, crystallographic orientation, texture, and grain boundary character distribution can be obtained by EBSD analysis. Despite the limited resolution of this technique (20–50 nm), EBSD is powerful, even for nanostructured materials. Through this technique, the microstructure can be characterized at different scales and levels with a high number of microstructural characteristics. It is known that the mechanical properties are strongly related to several microstructural aspects such as the size, shape, and distribution of grains, the presence of texture, grain boundaries character, and also the grain boundary plane distribution. In this context, this work aims to describe and discuss the possibilities of microstructural characterization, recent advances, the challenges in sample preparation, and the application of the EBSD in the characterization of metals.

scholarly journals Characterization of Ni–CNTs Nanocomposites Produced by Ball-Milling

Metals ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 2 ◽  
Author(s):  
Íris Carneiro ◽  
Filomena Viana ◽  
Manuel F. Vieira ◽  
José Valdemar Fernandes ◽  
Sónia Simões
Keyword(s):  
Ball Milling ◽  
Milling Time ◽  
Electron Backscatter Diffraction ◽  
Microstructural Characterization ◽  
Ni Powder ◽  
Metal Matrix Nanocomposite ◽  
Cold Pressed ◽  
Backscatter Diffraction ◽  
Matrix Nanocomposite

This research focuses on the characterization of a metal matrix nanocomposite (MMNC) comprised of a nickel matrix reinforced by carbon nanotubes (CNTs). The aim of this study was to characterize Ni–CNTs nanocomposites produced by powder metallurgy using ball-milling. CNTs were initially untangled using ultrasonication followed by mixture/dispersion with Ni powder by ball-milling for 60, 180, or 300 min. The mixtures were cold-pressed and then pressureless sintered at 950 °C for 120 min under vacuum. Their microstructural characterization was mainly performed by optical microscopy (OM), scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). The mechanical properties were evaluated by Vickers microhardness. The results indicate that combining ultrasonication and ball-milling can successfully produce Ni–CNTs nanocomposites. The ball-milling time has a significant effect on both the CNT dispersion and the final nanocomposite microstructure.

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