Defect and Dislocation Density Parameters of 5251 Al Alloy Using Positron Annihilation Lifetime Technique

2012 ◽  
Vol 332 ◽  
pp. 17-25 ◽  
Author(s):  
M.A. Abdel-Rahman ◽  
M. Elsayed ◽  
Ahmed G. Attallah ◽  
A.A. Ibrahim ◽  
Emad A. Badawi

The result of positron lifetime measurements of a defected 5251 Al alloy is reported. Positron lifetime is measured as a function of the thickness reduction of the sample which shows a nearly linear increase and then becomes constant; which can be considered to be a reason for the defect movement saturation. The trapping rate, trapping efficiency, trapping cross-section, defect concentration and defect density of positrons are also measured for the sample concerned. The behaviors of these parameters are matched with theoretical calculations. Data are analyzed using the PATFIT88 computer program.

1990 ◽  
Vol 209 ◽  
Author(s):  
J.C. O'Brien ◽  
R.H. Howell ◽  
H.B. Radousky ◽  
P.A. Sterne ◽  
D.G. Hinks ◽  
...  

ABSTRACTTemperature-dependent positron lifetime experiments have been performed from room temperature to cryogenic temperatures on Ba1−xKxBiO3. for x=0.4 and 0.5. From the temperature dependence of the positron lifetime in the normal state, we observe a clear signature of competition between separate defect populations to trap the positron. Theoretical calculations of lifetimes of free or trapped positrons have been performed on Ba1−xKxBiO3, to help identify these defects. Lifetime measurements separated by long times have been performed and evidence of aging effects in the sample defect populations is seen in these materials.


2013 ◽  
Vol 22 ◽  
pp. 112-117 ◽  
Author(s):  
A. MANDAL ◽  
S. MUKHERJEE ◽  
S. PAN ◽  
A. SENGUPTA

Positron annihilation lifetime spectra (PLAS) have been measured for natural rubber polymer with different fillers (Titenium dioxide, Nanosilica and Nanoclay) as a function of filler concentration to investigate how these fillers affect the microstructure of free volume of natural rubber. The lifetime spectra is analyzed by using LT9.0 and the longest lived component(τo-Ps) is attributed to the pick- off annihilation of o-Ps in free volume sites, available mostly in the amorphous region of polymer. On the basis of the τo-Ps values the radii of the free volume holes (Rh) are calculated. The PALS results show that o-Ps lifetime as well as the size of free volume decreases with the increase of filler concentration.


1995 ◽  
Vol 413 ◽  
Author(s):  
C. M. Huang ◽  
J. Liu ◽  
T. C. Sandreczki ◽  
Y. C. Jean

ABSTRACTPositron annihilation lifetime measurements are made in a series of polyaniline polymers with different chemical compositions and protonation ratios at room temperature. Two positron lifetimes are observed in these materials: one is assigned to annihilation in the bulk and the other to voids created due to protonation. A relationship between conductivities and positron annihilation probabilities is found.


2010 ◽  
Vol 666 ◽  
pp. 50-53 ◽  
Author(s):  
Jerzy Kansy ◽  
Aneta Hanc ◽  
Magdalena Jabłońska ◽  
E. Bernstock-Kopaczyńska ◽  
Dawid Giebel

The defect structure of Fe28Al samples is examined with the Positron Annihilation Lifetime Spectroscopy. The studies are carried out for samples in as-cast state and after heat treatments: annealing for 24 hours at 900°C (or 1050°C) and either slow cooling with furnace or quenching to oil. The PALS spectra are analyzed using two-state trapping model. Only one type of defects is detected. The positron lifetime in these defects (V) suggests that they are quenched-in Fe-monovacancies (VFe). The vacancy concentration strongly depends on the rate of cooling. Besides, V also depends slightly on the rate of cooling of the material. This fact suggests, according to the predictions of latest theoretical calculations, that V is sensitive to the atomic configuration in the nearest neighborhood of VFe, which give hope to estimate the degree of atomic ordering in alloys by the PALS technique.


2004 ◽  
Vol 11 (04n05) ◽  
pp. 427-432 ◽  
Author(s):  
M. A. ABDEL-RAHMAN ◽  
M. S. ABDALLAH ◽  
EMAD A. BADAWI

The measurements of Positron Annihilation Lifetime Technique (PALT) have been performed on AlSi 11.35 Mg 0.23 Alloys. It has been shown that positrons can become trapped at imperfect locations in solids and their mean lifetime can be influenced by changes in the concentration of such defects. No change has been observed in the mean lifetime values at the saturation of defect concentration. The trapping rates of positrons can be determined for thickness reduction up to 11% for dislocation. The concentration of defect (ρ') range varies from 8.65×1015 to 2.35×1018 cm -3 up to the maximum value of strain (ε) 0.23.


1988 ◽  
Vol 102 ◽  
pp. 71-73
Author(s):  
E. Jannitti ◽  
P. Nicolosi ◽  
G. Tondello

AbstractThe photoabsorption spectra of the carbon ions have been obtained by using two laser-produced plasmas. The photoionization cross-section of the CV has been absolutely measured and the value at threshold, σ=(4.7±0.5) × 10−19cm2, as well as its behaviour at higher energies agrees quite well with the theoretical calculations.


2008 ◽  
Vol 607 ◽  
pp. 64-66
Author(s):  
Nicolas Laforest ◽  
Jérémie De Baerdemaeker ◽  
Corine Bas ◽  
Charles Dauwe

Positron annihilation lifetime measurements on polymethylmethacrylate (PMMA) at low temperature were performed. Different discrete fitting procedures have been used to analyze the experimental data. It shows that the extracted parameters depend strongly on the fitting procedure. The physical meaning of the results is discussed. The blob model seems to give the best annihilation parameters.


1993 ◽  
Vol 321 ◽  
Author(s):  
A. J. Kruk ◽  
H. Schut ◽  
J. Sietsma ◽  
A. Van Veen

ABSTRACTThe first stages of the nano-crystallization process of amorphous Fe75.5Cu1Nb3Si12.5B8 into a nano-crystalline structure are investigated by the positron annihilation lifetime technique. Samples have been isothermally annealed at 643 K for times varying between 600 and 105 seconds. The positron lifetime spectra have been analyzed allowing for three lifetimes. The shortest and the longest lifetime, τ1 = 150 ± 2 ps and τ3 = 1500–2000 ps respectively, are attributed to annihilation of positrons in the amorphous phase and to the formation and annihilation of ortho-positronium at the surface of the stacked foils and did not change significantly upon the annealing. The intermediate positron lifetime τ2 increased from 324 ps to 387 ps. The intensity of this component increased from 5 to 15%. Comparison with resistivity measurements indicates that the change of this lifetime component occurs at an early stage in the crystallisation process, i.e. when the fraction of crystalline material is on the order of 10−3. The increase of τ2 is attributed to positrons annihilating in a region with lower average density surrounding the small crystallite.


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