Using Granulate Composites with Calcined Phosphogypsum and Pet Additive in Asphalting

2022 ◽  
Vol 1049 ◽  
pp. 257-265
Author(s):  
Pavel Borisovich Razgovorov ◽  
Аleksey A. Ignatiev ◽  
Valeriy Michailovich Gotovtsev ◽  
Elena Aleksandrovna Vlasova
Keyword(s):  
Polyethylene Terephthalate ◽  
Raw Materials ◽  
Chemical Properties ◽  
Crushed Rock ◽  
Great Promise ◽  
X Ray Diffraction ◽  
Average Size ◽  
Tropical Climates ◽  
Physical And Chemical ◽  
And Chemical Properties

The paper discusses the change of phosphogypsum surface state produced by Apatit (Cherepovetsky branch, Vologda region) during calcination at 298-1173 K. The authors have determined the average size of its crystallites and studied the atomic composition of raw materials and finished composites that include crushed rock fraction (5-10 mm), oil bitumen, and polyethylene terephthalate additive (1.0-1.2 wt. %). The compounds present in calcined phosphogypsum have been analyzed by X-ray diffraction. The granulate was obtained by pelletizing phosphogypsum with a mixture of the above components. The paper presents the assessment of its physical and chemical properties. The granulated composites based on the specified samples of calcined phosphogypsum, bitumen, and melted polyethylene terephthalate waste show great promise for construction road works in European countries in summer and winter, as well as countries with tropical climates.

Glass-Ceramics Obtained from Sewage Sludge and its Characteristics Affected by Alkalinity

2014 ◽  
Vol 937 ◽  
pp. 70-73
Author(s):  
Di Wu ◽  
Jun Zhang ◽  
Xing Wang Wen ◽  
Hui Ling Liu
Keyword(s):  
Sewage Sludge ◽  
Raw Materials ◽  
Glass Ceramics ◽  
Chemical Properties ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Sludge Disposal ◽  
Physical And Chemical ◽  
And Chemical Properties

Sewage sludge was tested as component for producing glass-ceramics with the addition of analytic reagent CaO to solve the sewage sludge disposal problems. The effect of alkalinity (Ak=mCaO/mSiO2) on the characteristics of the glass-ceramics was investigated. Differential scanning calorimetry (DSC) and X-ray diffraction (XRD) were used to investigate thermal behavior and crystalline phase of the samples. It was found that the degree and characteristics of crystals in vitrified sludge significantly correlate to the alkalinity of the raw materials. The glass-ceramics with Ak = 0.36 possessed the best physical and chemical properties.

Diesel Biofuels - Preparation, Characterization and Testing

2008 ◽  
Vol 59 (11) ◽  
Author(s):  
Cristina Dusescu ◽  
Anca Borcea ◽  
Vasile Matei ◽  
Ion Popa ◽  
Irina Gabriela Radulescu
Keyword(s):  
Vegetable Oils ◽  
Sunflower Oil ◽  
Raw Materials ◽  
Chemical Properties ◽  
Soya Bean ◽  
Production Unit ◽  
Physical And Chemical Properties ◽  
Physical And Chemical ◽  
And Chemical Properties

The present paper studies biodiesel samples preparation by transesterification and compares their physical and chemical properties (biofuels prepared from different raw materials - vegetable oils: sunflower oil, crocus oil and soya bean oil) and the biodegradability degree, as well as the possibilities of the integration of such production unit in industrial diagram of auto fuels production.

Monitoring of Fluctuations in the Physical and Chemical Properties of a High-Calcium Fly Ash

1987 ◽  
Vol 113 ◽  
Author(s):  
Scott Schlorholtz ◽  
Ken Bergeson ◽  
Turgut Demirel
Keyword(s):  
Fly Ash ◽  
Chemical Properties ◽  
Operating Conditions ◽  
Physical And Chemical Properties ◽  
X Ray Diffraction ◽  
X Ray ◽  
Morphological Studies ◽  
High Calcium ◽  
Physical And Chemical ◽  
And Chemical Properties

ABSTRACTThe physical and chemical properties of fly ash produced at Ottumwa Generating Station have been monitored since April, 1985. The fly ash is produced from burning a low sulfur, sub-bituminous coal obtained from the Powder River Basin near Gillette, Wyoming. One-hundred and sixty samples of fly ash were obtained during the two year period. All of the samples were subjected to physical testing as specified by ASTM C 311. About one-hundred of the samples were also subjected to a series of tests designed to monitor the self-cementing properties of the fly ash. Many of the fly ash samples were subjected to x-ray diffraction and fluorescence analysis to define the mineralogical and chemical composition of the bulk fly ash as a function of sampling date. Hydration products in selected hardened fly ash pastes, were studied by x-ray diffraction and scanning electron microscopy. The studies indicated that power plant operating conditions influenced the compressive strength of the fly ash paste specimens. Mineralogical and morphological studies of the fly ash pastes indicated that stratlingite formation occurred in the highstrength specimens, while ettringite was the major hydration product evident in the low-strength specimens.

scholarly journals Study of the Incorporation of Biomass Bottom Ash as a Filler for Discontinuous Grading Bituminous Mixtures with Bitumen Emulsion

2021 ◽  
Vol 11 (8) ◽  
pp. 3334
Author(s):  
Jorge Suárez-Macías ◽  
Juan María Terrones-Saeta ◽  
Francisco Javier Iglesias-Godino ◽  
Francisco Antonio Corpas-Iglesias
Keyword(s):  
Raw Materials ◽  
Bottom Ash ◽  
Chemical Properties ◽  
Physical And Mechanical Properties ◽  
Waste Biomass ◽  
Bituminous Mixtures ◽  
Bitumen Emulsion ◽  
Main Disadvantage ◽  
Physical And Chemical ◽  
And Chemical Properties

Energy consumption, because of population development, is progressively increasing. For this reason, new sources of energy are being developed, such as that produced from the combustion of biomass. However, this type of renewable energy has one main disadvantage, the production of waste. Biomass bottom ash is a residue of this industry that currently has not much use. For this reason, this research evaluates its use as a filler in bituminous mixtures, since this sector also has a significant impact on the environment, as it requires large quantities of raw materials. With this objective, first, the physical and chemical properties of biomass bottom ashes were evaluated, verifying their characteristics for their use as filler. Subsequently, bituminous mixtures were conformed with biomass bottom ash as filler, and their physical and mechanical properties were analyzed through particle loss and Marshall tests. The results of these tests were compared with those obtained with the same type of mixture but with conventional and ophite aggregates. This study confirmed that biomass bottom ash was viable for use as a filler, creating mixtures with a higher percentage of bitumen, better mechanical behavior, and similar physical properties. In short, more sustainable material for roads was obtained with waste currently condemned to landfill.

scholarly journals Investigation of Microbial Contamination and Physicochemical Properties of Compounded Medications in Pharmacies

2020 ◽  
Vol 26 (1) ◽  
pp. 82-93
Author(s):  
Reihaneh Radmanesh ◽  
◽  
Mohsen Nabi Meybodi ◽  
Vahid Ramezani ◽  
Maryam Akrami ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Microbial Contamination ◽  
Raw Materials ◽  
Chemical Properties ◽  
Pharmaceutical Product ◽  
Physical And Chemical ◽  
Made In ◽  
And Chemical Properties

Aims: Any pharmaceutical product made in pharmacy, hospital or factory may be contaminated with microbes. This contamination can originate from raw materials or during production. Hence, it is important to study the physical and chemical properties and stability of compounded drugs. Methods & Materials: In this study, first a specific sample of prescribed medication was ordered from 63 pharmacies in Yazd, Iran. After collecting the samples, the amount of microbial contamination, viscosity and particle size distribution and their stability were investigated and their results were compared to the standard levels. Findings: Based on the results, 31.7% of the samples had discoloration and 23.8% showed creaming phenomenon. In terms of particle size distribution, 57.1% of the samples had a 20-40 μm particle size and 49.2% had a viscosity equal to 2500-3000 centipoise. Regarding stability, 12.6% of the samples underwnet phase change at 30-40°C. About of the amount of hydroquinone in samples, 35% had acceptable amount. In 23.8% of the samples, fungal infection was observed. Conclusion: Contrary to a popular belief that the compounded medicines produced in pharmacies have microbial contamination, the results of this study showed that the microbial contamination of these compounded medications is low.

scholarly journals Influence of temperature regimes of ripening and fermentation stages on the physical and chemical properties of cream and sour-cream butter quality indicators

2018 ◽  
Vol 12 (3) ◽  
Author(s):  
O. O. Bondarchuk
Keyword(s):  
Milk Fat ◽  
Raw Materials ◽  
Chemical Properties ◽  
Physical And Chemical Properties ◽  
Second Stage ◽  
Temperature Regimes ◽  
Third Stage ◽  
Sour Cream ◽  
Physical And Chemical ◽  
And Chemical Properties

Physical and chemical properties of cream multistep modes of ripening and fermentations are investigation and their role in the production of sour-cream butter is studied. The process of ripening of cream was carried out multistep, regimes were selected depending on seasonal changes in the composition of milk fat. For raw materials of the autumn-winter period, for the values of iodine number 29.1–34.5, the first stage of ripening was carried out at a temperature of 8°C for 2 hours, the second stage – at 21°C for 7 hours, the third stage – at 13°C for 10 hours. For raw of spring-summer period, for the values of iodine number 34.5–40.1, the first stage of ripening was carried out at 21°C for 6 hours, the second stage – at 13°C for 4 hours, the third stage – at 8°C for 8 hours. It has been established that individual modes of low-temperature cream preparation, taking into account seasonal changes in the composition of milk fat, make it possible to obtain cream before churning almost with the same indexes of effective viscosity. The content of the crystalline phase of milk fat under both temperature regimes was 38.7–40.1%, which is sufficient to obtain of proper consistency sour-cream butter. The content of diacetyl and volatile organic acids more depend on the level of fermentation of cream than on the technological regimes of ripening and seasonality of raw materials. It has been proved that an increase in the fermentation degree of cream promotes an increase in the acidity of plasma and the content of aroma-producing components in the butter, and, accordingly, affects the degree of the sour taste. It is recommended for the production of cultured butter to begin the cream when the acidity of the plasma reaches 60ºT, which ensures the formation of high sensorial characteristic of the finished product.

Preparation and Melting of Zr-1.0Nb Alloy

2016 ◽  
Vol 869 ◽  
pp. 578-584 ◽  
Author(s):  
Armando Cirilo Souza ◽  
J.L. Rossi ◽  
P. Tsakiropoulos ◽  
L.G. Martinez ◽  
Carlos Roberto Grandini ◽  
...  
Keyword(s):  
Nuclear Reactor ◽  
Chemical Properties ◽  
Zirconium Alloys ◽  
Processing Parameters ◽  
X Ray Diffraction ◽  
High Permeability ◽  
Physical And Chemical ◽  
Good Homogeneity ◽  
Consumable Electrodes ◽  
And Chemical Properties

Zirconium alloys have many applications in industry in services too harsh for stainless steels, nickel alloys or where a noteworthy improvement in service life may be achieved, by choosing zirconium alloys instead of other metals, such as high permeability to thermal neutrons and excellent corrosion resistance in nuclear reactor environments. Mixing alloying elements, such as niobium, molybdenum, tin, titanium and tantalum, with zirconium changes its physical and chemical properties, especially its resistance to corrosion. In this study, specimens of Zr-1.0Nb alloy were obtained by melting in a furnace with non-consumable electrodes in argon atmosphere. Different samples were prepared to ensure good homogeneity of the specimens. The melting procedure was tested several times to determine the parameters that ensure proper alloy handling. These parameters include the melting point of the alloys under pressure and the current in the furnace. Using the derived melting parameters and processing parameters, it has been obtained Zr-1.0Nb alloy specimens with appropriate homogeneity, as confirmed by auxiliary characterization techniques, such as optical microscopy, scanning electron microscopy, energy dispersive spectroscopy and X-ray diffraction. For these methods, the requirements for physicochemical properties in the nuclear sector were incorporated into the analyses.

Vegetable oils – raw materials for producing biodiesel

2021 ◽  
Vol 80 (2) ◽  
pp. 286-292
Author(s):  
T. Mamilov ◽  
◽  
G.S. Aitkaliyeva ◽  
A.B. Ismailova ◽  
M.A. Yelubay ◽  
...  
Keyword(s):  
Functional Groups ◽  
Vegetable Oils ◽  
Raw Materials ◽  
Chemical Properties ◽  
Biodiesel Fuel ◽  
Physical And Chemical Properties ◽  
Sunflower Oils ◽  
Transesterification Method ◽  
Physical And Chemical ◽  
And Chemical Properties

This paper presents the results of a study of the physical and chemical properties of samples of vegetable oils (sunflower, rapeseed, olive). It has been shown that the viscosity of oils varies from 41.4 to 61.7 cSt at a temperature of 40 ° C for olive and sunflower oils, respectively. The acid numbers of the oil samples were also determined, it was found that the lowest indicator is characteristic of sunflower oil. Pour points of oils also range from -3 to -16 ° C for olive and sunflower oils, respectively. Using the method of IR spectroscopy, functional groups in the composition of samples of vegetable oils were studied and it was shown that the composition of oils contains carbonyl and hydroxyl functional groups, indicating the presence of carboxylic acids. Based on studies of the physical and chemical properties of vegetable oils, it was found that sunflower, olive and rapeseed oils can serve as raw materials for the synthesis of biofuels based on them, since they contain free fatty acids. To obtain biodiesel fuel based on vegetable oils, it is planned to use the transesterification method in the presence of various catalysts (alkaline, acidic, and complex).

Characterization of Shivirtui Zeolite Modified with Aluminum Oxyhydroxide Nanofibers

2019 ◽  
Vol 942 ◽  
pp. 40-49
Author(s):  
Yulia Murashkina ◽  
Olga B. Nazarenko
Keyword(s):  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
X Ray Diffraction ◽  
Scanning Electronic Microscopy ◽  
Electronic Microscopy ◽  
X Ray ◽  
Physical And Chemical ◽  
And Chemical Properties ◽  
Aluminum Oxyhydroxide

Natural zeolite of Shivirtui deposit (Russia) was modified with nanofibers of aluminum oxyhydroxide AlOOH. Aluminum oxyhydroxide nanofibers were produced at the heating and oxidation of aluminum powder with water. The properties of modified zeolite were investigated by means of X-ray diffraction, transmission electronic microscopy, scanning electronic microscopy, low-temperature nitrogen adsorption, thermal analysis, and Fourier transform infrared spectroscopy. It was found that water content in the modified sample of zeolite was about 15 %. Based on the study of the physical and chemical properties, shivirtui zeolite modified with nanofibers of aluminum oxyhydroxide can be proposed for use as a flame-retardant additive to polymers.

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