Microstructure and Mechanical Properties of Spray-Deposited Zn-30Al-1Cu Alloy

2012 ◽  
Vol 706-709 ◽  
pp. 264-267
Author(s):  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yon Gan Zhang ◽  
Hong Wei Liu ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tensile Tests ◽  
Chinese Script ◽  
Spray Atomization ◽  
Test Results ◽  
X Ray Diffraction ◽  
X Ray ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron

In this study, Zn-30Al-1Cu alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using optical microscopy, scanning electron microscopy, transmission electron microscopy, X-ray diffraction and tensile tests. It can be seen that the microstructure of spray-deposited Zn-30Al-1Cu alloy is composed of the Zn/Al eutectoids and few compounds. The Zn/Al eutectoids were shown lamellar, particle and Chinese script morphologies. The compound phases in the microstructure of the spray-deposited alloy were examined. The property test results indicate that the spray-deposited Zn-30Al-1Cu alloy displays superior tensile strength.

Research on the Microstructure and Mechanical Properties of Spray-Deposited 8009 Heat Resistant Aluminum Alloy

2014 ◽  
Vol 543-547 ◽  
pp. 3733-3736
Author(s):  
Rong Hua Zhang ◽  
Biao Wu ◽  
Xiao Ping Zheng
Keyword(s):  
Mechanical Properties ◽  
Aluminum Alloy ◽  
Tensile Tests ◽  
Test Results ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
X Ray ◽  
Heat Resistant ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron

In this study, 8009 heat resistant aluminum alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using transmission electron microscopy, X-ray diffraction, and tensile tests. The secondary phases in the microstructure of the spray-deposited alloy were examined. The tensile test results indicate that the spray-deposited 8009 alloy both at room and elevated temperature displays superior tensile strength due to the presence of the thermally stable Al12(Fe,V)3Si particles.

Microstructure and Mechanical Properties of an Al-Cu-Mg-Fe-Ni Alloy

2014 ◽  
Vol 988 ◽  
pp. 156-160
Author(s):  
Hong Wei Liu ◽  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cast Alloy ◽  
Tensile Tests ◽  
Eutectic Structure ◽  
Test Results ◽  
X Ray Diffraction ◽  
X Ray ◽  
Microstructure And Mechanical Properties ◽  
Ni Alloy ◽  
Scanning Electron

The microstructure and mechanical properties of the Al-2.24Cu-1.42Mg-0.9Fe-0.9Ni alloy were studied using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and tensile tests. The results indicate that the microstructures of the as cast alloy involve α-Al matrix, Al/Al2CuMg eutectic structure, Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds. The tensile test results indicate that the alloy at elevated temperature (200°C) displays superior tensile strength due to the presence of the thermally stable Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds.

Influence of Temperature of Accumulative Roll Bonding on the Microstructure and Mechanical Properties of AA5251 Aluminum Alloy

2014 ◽  
Vol 59 (1) ◽  
pp. 127-131 ◽  
Author(s):  
J. Bogucka
Keyword(s):  
Mechanical Properties ◽  
Ambient Temperature ◽  
Accumulative Roll Bonding ◽  
Bonding Temperature ◽  
Tensile Tests ◽  
Structure Evolution ◽  
X Ray Diffraction ◽  
Roll Bonding ◽  
X Ray ◽  
Microstructure And Mechanical Properties

Abstract The influence of bonding temperature on microstructure and mechanical properties of AA5251 alloy sheets have been analyzed in the paper. The alloy was deformed with the method of accumulative roll bonding (ARB) in various temperature conditions i.e. at ambient temperature up to 5th cycle (ε = 4.0) and using pre-heating of sheet packs at 200°C and 300°C up to 10 cycles (ε = 8.0). The deformed material was subjected to structural observations using TEM, measurements of crystallographic texture with the technique of X-ray diffraction and tensile tests. It was established that the temperature of roll-bonding had a significant effect on the structure evolution and the observed changes of mechanical properties. High refinement of microstructure and optimum mechanical properties were obtained for the material processed at lower temperatures, i.e. at ambient temperature and pre-heating at 200°C. Recovery structure processes occurring during deformation were observed in the alloy bonded with pre-heating at 300°C and therefore mechanical properties were lower than for the alloy bonded at lower temperatures.

Fullerene-Metal Composites: Phase Transformations During Milling and Sintering

2011 ◽  
Vol 172-174 ◽  
pp. 727-732 ◽  
Author(s):  
Ileana Irais Santana ◽  
Francisco Carlos Robles Hernandez ◽  
Vicente Garibay-Febles ◽  
Hector A. Calderon
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Phase Transformations ◽  
Mechanical Milling ◽  
X Ray Diffraction ◽  
Metal Composites ◽  
X Ray ◽  
Plasma Sintering ◽  
Transmission Electron ◽  
Spark Plasma

Composites of Fe-C60and Al C60produced by mechanical milling and sinterized by Spark Plasma Sintering are investigated with special attention to the mechanical properties of the products. The processing involves phase transformations of the fullerenes that are interesting to follow and characterize. This involves formation of tetragonal/rhombohedral diamond and carbides during sintering and milling. Transmission Electron Microscopy (TEM) and Raman Spectroscopy techniques are also used to confirm preliminary results of X Ray Diffraction (XRD) related to the formation of nanostructures i.e., grain size of the crystals during mechanical milling and after sintering, spatial distribution of phases and the different phases that are developed during processing.

Transmission electron microscopy of SI-AL-O-N alloys

1978 ◽  
Vol 36 (1) ◽  
pp. 302-303 ◽  
Author(s):  
M. Kirn ◽  
M. Rühle ◽  
H. Schmid ◽  
L.J. Gauckler
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Imaging Technique ◽  
Construction Materials ◽  
Physical And Mechanical Properties ◽  
Operating Voltage ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron

It is expected that Si-Al-O-N alloys are important high temperature construction materials. The phase diagrams for Si-Al-O-N alloys were studied systematically mainly by X-ray diffraction work (for a summary see). Different stable phases were found. For the understanding of the physical and mechanical properties it is of great interest to know for the different stable phases the microstructure and the morphology, which can be obtained by TEM observations. Results of some TEM studies are reported here utilizing not only the conventional TEM but also the lattice fringe imaging technique.Specimens of the different phases were produced as described in They were prepared for TEM observations. For high resolution work a Siemens ELMISKOP 102 (operating voltage 125 kV) was used fitted with a double tilting stage (± 45°), for conventional TEM studies the specimens were examined in an AEI EM7 high voltage EM operated at 1 MeV.

Mechanical Properties and Microstructure of Graphene-Cement Composites

2017 ◽  
Vol 748 ◽  
pp. 295-300 ◽  
Author(s):  
Rui Shuang Jiang ◽  
Bao Min Wang
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Compressive Strength ◽  
Cement Paste ◽  
Control Sample ◽  
Cement Composites ◽  
X Ray Diffraction ◽  
Visible Spectroscopy ◽  
X Ray ◽  
Transmission Electron

In this work, two type graphene were dispersed in aqueous solution via sonication, and graphene nanoplatelets (GP) and graphene oxide (GO) were characterized by means of ultraviolet visible spectroscopy (UV-vis), X-ray diffraction (XRD) and transmission electron microscopy (TEM). In addition, the effects of different graphene (GP and GO) on mechanical properties and microstructure of cement-based materials were investigated via filed emission scanning electron microscopy (FESEM). The results suggested that the incorporation of GP and GO both improved the flexural and compressive strength of cement, and the GP had a more prominent impact on the strengths of cement, compared with GO. The flexural and compressive strength of cement increased up to 23.5% and 7.5% with 0.05 wt% GP, respectively. FESEM analysis indicated that the microstructure of GP-cement paste was similar to that of control sample without graphene, whereas, a few flower-like crystals were generated in GO-cement paste. This work could provide a new understanding for further researches of graphene-cement composites.

Influence of Al-Content on the Microstructure and Mechanical Properties in ZrAlN Coatings

2014 ◽  
Vol 1004-1005 ◽  
pp. 778-783 ◽  
Author(s):  
Xiao Ying Zhu ◽  
Jun Du ◽  
Gui Min Liu ◽  
Xiao Hui Zheng
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Phase Structure ◽  
Cubic Phase ◽  
X Ray Diffraction ◽  
Two Phase ◽  
Al Content ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron ◽  
Indentation Methods

Zirconium aluminum nitride coatings have been deposited onto Ti-6Al-4V substrates by reactive magnetron sputtering in order to investigate the influence of Al-content on the microstructure and mechanical properties. The morphology and microstructure of the coatings were investigated by field emission scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Nanoindentation and Vicker’s indentation methods were employed to measure the hardness and toughness of the coatings, respectively. The results show that a structure of single cubic phase with twinning is formed at Al content of x ≤ 0.23, and a two-phase structure of hexagonal and cubic phase is formed at Al content of x ≥ 0.47. Hardness and toughness of the Zr1-xAlxN coatings show similar tendency with the increasing of Al-content. Both of them reach the maximum values at x=0.23 and drop to the minimum values at x=0.47, after that, they slightly increase with the increasing Al-content. The enhanced hardness and toughness achieved at x=0.23 is ascribed not only to single cubic phase structure but also to twinning structure.

Effect of Ca on Microstructure and Properties of Mg-Al-Si Alloys

2011 ◽  
Vol 194-196 ◽  
pp. 1369-1373 ◽  
Author(s):  
Chun Xiang Xu ◽  
Hui Ju ◽  
Yang Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Chinese Script ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ca Addition ◽  
The Matrix ◽  
Morphology Modification ◽  
Scanning Electron

Effect of Ca addition on the morphology modification in Mg-7Al-0.8Zn-0.2Mn-1Si (AS71) alloys has been investigated using X-ray diffraction (XRD), optical microscopy (OM), and scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and various testing machines. The results show that when adding 0.1 wt% Ca, a small fraction of Mg2Si change from Chinese script type to polygonal type; with the Ca addition up to 0.3 wt%, edges and angles of polygonal type Mg2Si phase are changed; further increase in Ca addition, the morphology of Mg2Si is changed to strip-like or spot-like one. Meanwhile, the addition of Ca results in the morphology of β- Mg17Al12 phase changing from discontinuous net-like to dispersive island-like. Ca exists as solid-soluting atomic in the matrix with small Ca addition while in the form of CaSi2 with large Ca addition. Optimal mechanical properties can be achieved when Ca addition is 0.3 wt%.

Microstructural and Mechanical Properties of Polyester/Nanoclay Nanocomposites: Microstructure-Mixing Strategy Correlation

2011 ◽  
Vol 1312 ◽  
Author(s):  
Hamid Dalir ◽  
Rouhollah D. Farahani ◽  
Vireya Nhim ◽  
Benjamin Samson ◽  
Martin Lévesque ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Strain ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Roll Mill ◽  
The Matrix ◽  
Polyester Matrix ◽  
Excellent Improvement

ABSTRACTDifferent nanoclay mixing strategies using a three-roll mill and ultrasonication is proposed to obtain the desired polyester/nanoclay dispersion, intercalation, and exfoliation. The dispersion states of the modified nanoclay in polymer with 2, 4 and 6 wt% loading were characterized with X-ray diffraction, scanning electron microscopy (SEM), and low and high magnification transmission electron microscopy (TEM). The mechanical properties of the clay-reinforced polyester nanocomposites were a function of the nature and the content of the clay in the matrix. The nanocomposite containing 4 wt% modified Cloisite® 15A exhibits excellent improvement in modulus (by ~51%) and tensile strength (by ~12%) with a decrease in fracture strain (by ~26%) and fracture energy (by ~17%). These mechanical characteristic changes can be attributed to the dispersion, intercalation, and exfoliation of the nanoclays inside the polyester matrix.

scholarly journals FEATURES OF STRUCTURE FORMATION AND CHANGES IN THE MECHANICAL PROPERTIES OF CAST Al-Mg-Si-Mn ALLOY WITH THE ADDITION OF (Ti+Zr)

2015 ◽  
Vol 55 (4) ◽  
pp. 282 ◽  
Author(s):  
Oleksandr Trudonoshyn ◽  
Maxim Puchnin ◽  
Kostiantyn Mykhalenkov
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Ageing Time ◽  
Tensile Tests ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Transmission Electron ◽  
Heat Treated ◽  
Scanning Electron

<p>The as-cast and heat-treated structure of permanent mould castings of AlMg<sub>5</sub>Si<sub>2</sub>Mn alloys with different contents of Ti has been investigated by differential scanning calorimetry, hardness and microhardness measurements, tensile tests and fractography analyses, scanning electron microscopy, transmission electron microscopy, and energy dispersive X-ray analysis. We have established that α-Al dendrites can be nucleated on an Al-Ti substrate, and also that primary Mg<sub>2</sub>Si crystals can be nucleated on oxides, including oxides of Al and Ti compounds. The dependence of the change in mechanical properties on ageing time, and on the amount of Ti in the alloys, is shown.</p>

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