Valuation of Mechanical Properties and Microstructural Characterization of ASTM F75 Co-Cr Alloy Obtained by Selective Laser Melting (SLM) and Casting Techniques

2017 ◽  
Vol 899 ◽  
pp. 323-328 ◽  
Author(s):  
Marcello Vertamatti Mergulhão ◽  
Carlos Eduardo Podestá ◽  
Maurício David Martins das Neves

Advances in processes using the powder metallurgy techniques are making this technology competitive compared to the other traditional manufacturing processes, especially in medicine area. The additive rapid prototyping technique – selective laser melting (SLM) was applied in a biomaterial of CoCrMoFe alloy (ASTM F75), to study the mechanical properties and microstructural characterization in comparison between the conventional technique – casting. The gas atomized powder was investigated by their physical (as apparent density, bulk density and flow rate) and the chemical properties. The powder was analyzed using scanning electron microscope with energy-dispersed X-ray spectroscopy (SEM-EDS) and X-ray fluorescence. Specimens of standard samples were manufactured using these techniques to evaluate the mechanical properties as uniaxial tensile (yield strength, rupture tensile and elongation), transverse rupture strength and the micro hardness. The mechanical properties showed higher values in the SLM specimens than the casting specimens. Before the mechanical tests the specimens were examined using optical microscope (OM) and SEM-EDS. The micrographs revealed a microstructure with finer morphology in the SLM technique and the dendrites in the casting technique.

2017 ◽  
Vol 899 ◽  
pp. 534-539 ◽  
Author(s):  
Marcello Vertamatti Mergulhão ◽  
Carlos Eduardo Podestá ◽  
Maurício David Martins das Neves

The aim of this study is the consolidation of Cobalt-Chromium (CoCr) alloy powder using the additive manufacturing - selective laser melting (SLM) and the investment casting techniques. The research of this study has been applied to their biomaterial applied to development of prosthesis and dental implants. The gas atomized powder are spherical (mean diameter equal to 42,74 μm) and was analyzed by their physical and chemical properties. The microstructure of the powder and specimens was evaluated using optical microscope (OM) and scanning electron microscope with energy-dispersed X-ray spectroscopy (SEM-EDS). The mechanical properties were evaluated of standard samples using a tensile (yield strength, maximum tensile, rupture tensile and elongation), three point bending (transverse rupture strength) and micro hardness tests. The mechanical results indicate higher values for the SLM than casting specimens. The micrographs revealed a characteristic morphology of laser been used in the SLM technique and the dendrites in the casting technique. The microstructure of samples made by SLM is thinner than the samples obtained in the cast.


MRS Advances ◽  
2019 ◽  
Vol 4 (44-45) ◽  
pp. 2431-2439
Author(s):  
N. Iqbal ◽  
E. Jimenez-Melero ◽  
U. Ankalkhope ◽  
J. Lawrence

ABSTRACTThe microstructure homogeneity and variability in mechanical properties of 316L stainless steel components fabricated using selective laser melting (SLM) have been investigated. The crack free, 99.9% dense samples were made starting from SS316L alloy powder, and the melt pool morphology was analysed using optical and scanning electron microscopy. Extremely fast cooling rates after laser melting/solidification process, accompanied by slow diffusion of alloying elements, produced characteristic microstructures with colonies of cellular substructure inside grains, grown along the direction of the principal thermal gradient during laser scanning. In some areas of the microstructure, a significant number of precipitates were observed inside grains and at grain boundaries. Micro hardness measurements along the build direction revealed slight but gradual increase in hardness along the sample height. Uniaxial tensile tests of as manufactured samples showed the effect of un-melted areas causing scatter in room-temperature mechanical properties of samples extracted from the same SLM build. The ultimate tensile strength (UTS) varied from 458MPa to 509MPa along with a variation in uniform elongation from 3.3% to 14.4%. The UTS of a sample exposed to the Cl- rich corrosion environment at 46oC temperature revealed a similar strength as of the original sample, indicating good corrosion resistance of SLM samples under those corrosion conditions.


2014 ◽  
Vol 783-786 ◽  
pp. 898-903 ◽  
Author(s):  
Anne Mertens ◽  
Sylvie Reginster ◽  
Quentin Contrepois ◽  
Thierry Dormal ◽  
Olivier Lemaire ◽  
...  

In this study, samples of stainless steel AISI 316L have been processed by selective laser melting, a layer-by-layer near-net-shape process allowing for an economic production of complex parts. The resulting microstructures have been characterised in details in order to reach a better understanding of the solidification and consolidation processes. The influence of the processing parameters on the mechanical properties was investigated by means of uniaxial tensile testing performed on samples produced with different main orientations with respect to the building direction. A strong anisotropy of the mechanical behaviour was thus interpreted in relation with the microstructures and the processing conditions.


Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 825 ◽  
Author(s):  
Mustafa Awd ◽  
Felix Stern ◽  
Alexander Kampmann ◽  
Daniel Kotzem ◽  
Jochen Tenkamp ◽  
...  

The laser-based fusion of metallic powder allows construction of components with arbitrary complexity. In selective laser melting, the rapid cooling of melt pools in the direction of the component building causes significant anisotropy of the microstructure and properties. The objective of this work is to investigate the influence of build anisotropy on the microstructure and mechanical properties in selective laser melted AlSi10Mg. The alloy is comprehensively used in the automotive industry and has been one of the most frequently investigated Al alloys in additive manufacturing. Using specimens produced in three different building orientations with respect to the build platform, the anisotropy of the microstructure and defects will be investigated using scanning electron microscopy and microcomputed tomography. The analysis showed a seven-times higher pore density for the 90°-specimen compared to the 0°-specimen. The scanning electron microscopy revealed the influence of the direction of the cooling gradient on the constitution of the eutectic phase. Mechanical properties are produced in quasi-static and fatigue tests of variable and constant loading amplitudes. Specimens of 0° showed 8% higher tensile strength compared to 90°-specimens, while fracture strain was reduced almost 30% for the 45°-specimen. The correlation between structural anisotropy and mechanical properties illustrates the influence of the building orientation during selective laser melting on foreseen fields of application.


2018 ◽  
Vol 24 (7) ◽  
pp. 1235-1244 ◽  
Author(s):  
Mingkang Zhang ◽  
Yongqiang Yang ◽  
Changhui Song ◽  
Yuchao Bai ◽  
Zefeng Xiao

PurposeThis study aims to focus on the heat treatment influence on the corrosion resistance, adhesion of Streptococcus mutans and mechanical properties of CoCrMo alloys manufactured by the selective laser melting (SLM). Design/methodology/approachCoCrMo alloys were manufactured using the Dimetal-100 machine. X-ray diffraction (XRD), metallographic analysis, scanning electron microscopy (SEM), electrochemical corrosion, Vickers microhardness and tensile tests were used to characterize SLM-produced CoCrMo alloys and compare them with the ones manufactured by casting and with the ASTM F75 standard. FindingsThe electrochemical results showed that SLM900 samples had the best corrosion resistance in artificial saliva. The adhesion results showed least propagation and overall quantity of Streptococcus mutans on the SLM900 sample. The microhardness, tensile and yield strength of As-SLM, SLM900 and SLM1200D samples were measured according to the ASTM F75 standard. The elongation of SLM900 was less than 8 per cent, which does not meet the standard specifications. Analysis of the fracture morphology showed that the fracture mechanisms of As-SLM and SLM1200D belong to the quasi-cleavage fracture type, and the mechanical fracture mechanism of SLM900 can be characterized as brittle fracture. Originality/valueThis paper presents the adhesion properties of Streptococcus mutans on the surface of CoCrMo alloys manufactured by SLM and proposes how to regulate the effect of the heat treatment on the corrosion resistance and mechanical properties of CoCrMo alloys manufactured by SLM.


2015 ◽  
Vol 58 (3) ◽  
pp. 161-165 ◽  
Author(s):  
J. Haan ◽  
M. Asseln ◽  
M. Zivcec ◽  
J. Eschweiler ◽  
R. Radermacher ◽  
...  

Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4174 ◽  
Author(s):  
Angelina Strakosova ◽  
Jiří Kubásek ◽  
Alena Michalcová ◽  
Filip Průša ◽  
Dalibor Vojtěch ◽  
...  

Maraging steels are generally characterized by excellent mechanical properties, which make them ideal for various industrial applications. The application field can be further extended by using selective laser melting (SLM) for additive manufacturing of shape complicated products. However, the final mechanical properties are strongly related to the microstructure conditions. The present work studies the effect of heat treatment on the microstructure and mechanical properties of 3D printed samples prepared from powder of high-strength X3NiCoMoTi 18-9-5 maraging steel. It was found that the as-printed material had quite low mechanical properties. After sufficient heat treatment, the hardness of the material increased from 350 to 620 HV0.1 and the tensile yield strength increased from 1000 MPa up to 2000 MPa. In addition, 3% ductility was maintained. This behavior was primarily affected by strong precipitation during processing.


2016 ◽  
Vol 48 (1) ◽  
pp. 178-187 ◽  
Author(s):  
Anthony P. Ventura ◽  
C. Austin Wade ◽  
Gregory Pawlikowski ◽  
Martin Bayes ◽  
Masashi Watanabe ◽  
...  

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