Effect of Rolling-Remelting SIMA Process on Semi-Solid Microstructure of ZCuSn10 Alloy

2014 ◽  
Vol 217-218 ◽  
pp. 418-425 ◽  
Author(s):  
Jia Wang ◽  
De Hong Lu ◽  
Han Xiao ◽  
Rong Feng Zhou ◽  
Rong Zhou ◽  
...  
Keyword(s):  
Liquid Phase ◽  
Deformation Process ◽  
Volume Fraction ◽  
Solid Phase ◽  
Solid Particles ◽  
Deformation Degree ◽  
Fine Grain ◽  
Sima Process ◽  
Semi Solid ◽  
Sharp Corners

Semi-solid billet of ZCuSn10 (Wt%: 88.25Cu, 10.48Sn) alloy is prepared by strain induced melt activated (SIMA) method which including rolling and remelting process. Firstly, ZCuSn10 alloy is casted, and rolling samples are cut from ingot casting. Secondly, the rolling samples are two pass or four pass rolled after holding 15 minutes at 450°C, then samples with 10% and 20% pre-deformation degree are obtained. The remelting samples are cut from pre-deformed samples. Lastly, the remelting samples are reheated up to 850°C or 875°C, water quenching after holding for 15 minutes. Then semi-solid microstructure of ZCuSn10 alloy is prepared. The semi-solid microstructure of ZCuSn10 alloy is observed and compared with annealed microstructure and microstructure of ZCuSn10 alloy directly remelted after casting. The results indicate that semi-solid microstructure of ZCuSn10 alloy by rolling-remelting SIMA process is uniform and fine grain, and spheroidization level of solid particle is well. The optimum semi-solid microstructure is obtained when alloy with pre-deformation 20% is remelted at 875°C for 15 minutes, the average grain diameter is about 75.80μm, shape factor is 1.62, and volume fraction of liquid phase reaches about 17.28%. Pre-deformation process plays a crucial role in grain refinement and spheroidization during SIMA process for preparing the semi-solid ZCuSn10 alloy, as pre-deformation degree and remelting temperature increases, volume fraction of liquid phase increases, the solid particles in semi-solid microstructure are smaller and rounder. The main mechanism of SIMA process preparing semi-solid billet of ZCuSn10 alloy is that pre-deformation breaks dendrites and stores energy of deformation into alloy, and promotes dendrites fusing through remelting process. Meanwhile, liquid phase occupies sharp corners of solid particles by Sn element diffusing from liquid phase into α solid phase, so that fine and uniform and globular α solid particles are gained.

The Microstructure Evolvement and Simulation Analysis during Semi-Solid Processing of Aluminum Alloy

2008 ◽  
Vol 141-143 ◽  
pp. 139-144 ◽  
Author(s):  
Yi Tao Yang ◽  
Jian Fu Wang ◽  
Heng Hua Zhang ◽  
Guang Jie Shao
Keyword(s):  
Liquid Phase ◽  
Solid Phase ◽  
General Structure ◽  
Die Casting ◽  
Fluid Velocity ◽  
Solid Particles ◽  
Forming Process ◽  
Unequal Distribution ◽  
Semi Solid ◽  
Die Castings

To enhance the comprehension on the internal rule of microstructure evolvement and quality-controlled relativity, the microstructure during the induction reheating of billets and die casting of parts was systematically investigated. According to general structure observation and aided analysis of some computer simulations, the quantitative relationships between microscopic morphology (including solid fraction and grain shape) and formation state was minutely discussed. The experimental results showed that liquid and solid phase in semi-solid slurry had different filling tendency, fluid velocity of liquid phase in the area of high filling speed was relative quick and easy to flow into far area and corner. Solid particles far from gate possessed fine and round grain. Moreover, the structure configuration of original billets markedly affected forming process; billets with fine and round grain were required for the die-castings of complex shape and thin thickness. In the case of the big change in shape and thickness of die-castings, the design of gating system and the control of plunger speed should be so properly carried out as to avoid unequal distribution of solid and liquid phase in die-casting part as soon as possible.

Comparative Assessment of Turbulence Models for Prediction of Flow-Induced Corrosion Damages

2011 ◽  
Author(s):  
Kaushik Das ◽  
Debashis Basu ◽  
Todd Mintz
Keyword(s):  
Corrosion Rate ◽  
Cross Sections ◽  
Volume Fraction ◽  
Solid Phase ◽  
Turbulence Models ◽  
Reynolds Stress Model ◽  
Continuous Phase ◽  
Comparative Assessment ◽  
Solid Particles ◽  
Protective Film

The present study makes a comparative assessment of different turbulence models in simulating the flow-assisted corrosion (FAC) process for pipes with noncircular cross sections and bends, features regularly encountered in heat exchangers and other pipeline networks. The case study investigates material damage due to corrosion caused by dissolved oxygen (O2) in a stainless steel pipe carrying an aqueous solution. A discrete solid phase is also present in the solution, but the transport of the solid particles is not explicitly modeled. It is assumed that the volume fraction of the solid phase is low, so it does not affect the continuous phase. Traditional two-equation models are compared, such as isotropic eddy viscosity, standard k-ε and k-ω models, shear stress transport (SST) k-ω models, and the anisotropic Reynolds Stress Model (RSM). Computed axial and radial velocities, and turbulent kinetic energy profiles predicted by the turbulence models are compared with available experimental data. Results show that all the turbulence models provide comparable results, though the RSM model provided better predictions in certain locations. The convective and diffusive motion of dissolved O2 is calculated by solving the species transport equations. The study assumes that solid particle impingement on the pipe wall will completely remove the protective film formed by corrosion products. It is also assumed that the rate of corrosion is controlled by diffusion of O2 through the mass transfer boundary layer. Based on these assumptions, corrosion rate is calculated at the internal pipe walls. Results indicate that the predicted O2 corrosion rate along the walls varies for different turbulence models but show the same general trend and pattern.

Development of New Type Semi-Solid Injection Process for Magnesium Alloy

2014 ◽  
Vol 217-218 ◽  
pp. 361-365
Author(s):  
Yuichiro Murakami ◽  
Kenji Miwa ◽  
Naoki Omura ◽  
Shuji Tada
Keyword(s):  
Magnesium Alloy ◽  
Volume Fraction ◽  
Solid Particles ◽  
Casting Defects ◽  
Microstructure Observation ◽  
Injection Process ◽  
Fraction Solid ◽  
The Matrix ◽  
New Type ◽  
Semi Solid

We have developed new type semi-solid injection process for magnesium alloy. This process does not require to use any cover gases and the special magnesium billet such as thixo-billet. In this study, plate specimens were produced by injecting the semi-solid billet with different fraction solid. The microstructure observation, detection of casting defects by an X-ray computed tomography scanner, and tensile test were carried out. With increasing fraction solid, the size and shape of α-Mg solid particles became smaller and more spherical. In the condition of low fraction solid or forming in liquid state, the casting defects were located in the center of the specimen at the thickness direction. Additionally, the volume fraction of the casting defect decreased with increasing fraction solid. Moreover, the casting defects can be reduced by preventing solidifying and clogging of the top of the nozzle. Then, the specimen which has few casting defects could be obtained by injecting the slurry of fraction solid 0.5. However, the tensile strength and yield strength were highest in fraction solid 0.4. It is contemplated that the composition of the solid solution component element in the matrix was increased in fraction solid of 50%, therefore the matrix became brittle.

Three-Dimensional Numerical Simulation of Convective Melting of Solid Particles in a Fluid

1999 ◽  
Author(s):  
Y. L. Hao ◽  
Y.-X. Tao
Keyword(s):  
Volume Fraction ◽  
Solid Phase ◽  
Rectangular Cross Section ◽  
Three Dimensional ◽  
Phase Changes ◽  
Solid Particles ◽  
Preliminary Calculation ◽  
Two Phase ◽  
Closed Set ◽  
Gravity Effects

Abstract A physical model of two-phase flow and heat-mass transfer with the phase changes based on the theory of interacting continua is proposed. All terms in the conservation equations are analyzed and the constitutive equations are presented. A closed set of governing equations describing the convective melting of solid particles in a fluid is obtained. The numerical method is developed for the solution of velocity, temperature, and volume fraction of solid phase for the three-dimensional melting in a rectangular cross-section channel. Preliminary calculation, including gravity effects, shows that the result is reasonable. This study provides a basis for the theoretical and experimental investigation of convective melting of solid particles in a fluid.

Investigation on Sub-Rapid Solidification Behavior of Semi-Solid Magnesium Alloy Metal

2011 ◽  
Vol 320 ◽  
pp. 156-162
Author(s):  
Hai Tao Teng ◽  
Bai Qing Xiong ◽  
Yon Gan Zhang ◽  
Ting Ju Li
Keyword(s):  
Magnesium Alloy ◽  
Rapid Solidification ◽  
Volume Fraction ◽  
Solidification Rate ◽  
Solid Particles ◽  
Solidification Behavior ◽  
Vacuum Suction ◽  
Semi Solid ◽  
Rapidly Solidified ◽  
Alloy Metal

In order to investigate sub-rapid solidification behavior of semi-solid magnesium alloy metal, a novel semi-solid processing technique, called new vacuum suction casting (NVSC), is used to manufacture thin castings of AZ91D Mg-alloy directly from a liquid metal. The resulting microstructures of castings are characterized in detail and linked to the solidification behavior. In the microstructure of the sub-rapidly solidified SSM sheet, the “preexisting” primary solid particles, with the morphology of near-globules or rosettes, disperse in the homogeneous matrix consisting of fine near-equiaxed secondary α-Mg grains and fine precipitates of β-Mg17Al12 intermetallics. Owing to rapid solidification rate, the volume fraction of the β phase in the sub-rapidly solidified SSM sheets is much lower than that in the as-cast ingot. In addition, the content of alloying elements of Al and Zn was higher in the grain boundaries and the eutectic structure than that in the primary solid particles and in the second α-grains.

The nonlinear dynamics of solidification of a binary melt with a quasi-equilibrium mushy region

1990 ◽  
Vol 68 (9) ◽  
pp. 790-793 ◽  
Author(s):  
Yu. A. Buyevich ◽  
L. Y. Iskakova ◽  
V. V. Mansurov
Keyword(s):  
Mass Transfer ◽  
Heat And Mass Transfer ◽  
Volume Fraction ◽  
Solid Phase ◽  
Internal Heat ◽  
Solid Particles ◽  
Mushy Region ◽  
Parameter Method ◽  
Quasi Equilibrium ◽  
Phase Volume Fraction

A mushy region (a two-phase zone) between the solid and liquid phases occurs often in the process of solidification of a binary melt. An analysis of the structure of the mushy region, which includes the liquid, solid particles, and dendrites extending from the bulk solid surface, is suggested. The processes of heat and mass transfer in the mushy region are considered on the basis of the small parameter method. The analysis leads to equations governing unsteady heat and mass transfer with internal heat, and mass sources within the mushy region, and it includes the condition for the absence of supercooling (the condition for the zone quasi-equilibrium), convection being neglected. The temperature, concentration of solute, and solid phase volume fraction are found. On the basis of this solution a new model of the process is formulated. Within the scope of this model the mushy region is replaced by a liquid–solid interface with discontinuous boundary conditions.

Grain Refinement of 6061 Al Alloy by the Modified Strain-Induced Melt- Activated(SIMA) Process for Semi-Solid Processing

2007 ◽  
Vol 119 ◽  
pp. 311-314 ◽  
Author(s):  
Young Buem Song ◽  
Chun Pyo Hong
Keyword(s):  
Grain Refinement ◽  
Grain Structure ◽  
Al Alloy ◽  
Fine Grained ◽  
Fine Grain ◽  
Fine Grained Structure ◽  
Size Uniformity ◽  
Sima Process ◽  
Semi Solid ◽  
6061 Al Alloy

The dynamic process of fine grain evolution of 6061 aluminum alloy during modified strain-induced, melt-activated (SIMA) process was studied. The modified SIMA process employed casting, two stage homogenization, warm multi-forging, and recrystallization and partial melting (RAP). Multi-forging was carried out at a strain rate of 9x10-3 s-1 to accumulate high strains, with decreasing temperature from 250 to 200 °C. The alloy multi-forged with the accumulated strain of about 12 and RAP at 640 °C for 10 min exhibited the uniform equiaxed recrystallized grain structure. Accordingly, it was evident that multi-forging was very effective on grain refinement and grain size uniformity. The present modified SIMA process was discussed as an alternative thermo-mechanical processing for preparing the alloys with fine grained structure for semi solid processing.

Herbicidal and Seed Dormancy Induction Activity of Fermentation Residual Vinasse

Weed Science ◽  
2018 ◽  
Vol 66 (3) ◽  
pp. 317-323
Author(s):  
Ramon G. Leon ◽  
Rocio van der Laat
Keyword(s):  
Liquid Phase ◽  
Seed Dormancy ◽  
Soil Amendment ◽  
Solid Phase ◽  
Organic Liquid ◽  
Herbicidal Activity ◽  
Solid Particles ◽  
Amaranthus Palmeri ◽  
Seedling Mortality ◽  
Radicle Growth

AbstractVinasse, a liquid fermentation residual of bio-ethanol production that also contains solid particles in suspension, is commonly used as a soil amendment. Previous studies reported vinasse reduced seed germination and seedling establishment, suggesting herbicidal activity. Laboratory experiments were conducted to determine whether vinasse herbicidal activity is present in the liquid or solid phase, and whether it affects plants during seed early germination (i.e., imbibition), late germination (i.e., embryo growth and radicle protrusion), or seedling growth. Most of the herbicidal activity was associated with the liquid phase, and for most species, seed viability was predominantly affected after the imbibition phase. Susceptibility to vinasse was species dependent. Lettuce (Lactuca sativaL.) germination was <8% when seeds were imbibed and germinated in vinasse solutions or imbibed in water and germinated in vinasse. Conversely, imbibing lettuce seeds in vinasse solutions and germinating them in water did not change their germination in comparison with seeds imbibed and germinated in water (>80% germination). Wheat (Triticum aestivumL.) and sicklepod [Senna obtusifolia(L.) H. S. Irwin & Barneby] germination decreased 10% and 35% when seeds were imbibed and germinated in vinasse, respectively, while Palmer amaranth (Amaranthus palmeriS. Watson) and southern crabgrass [Digitaria ciliaris(Retz.) Koeler] germination decreased >90%. All evaluated species reduced radicle growth as vinasse concentration increased. Filtered liquid vinasse with reduced concentration of salt and ionic compounds inhibited radicle growth similarly to unfiltered vinasse, indicating that the herbicidal activity was not due to osmotic effects and was likely present in the organic liquid phase.Amaranthus palmeri,S. obtusifolia, andD. ciliarisincreased the proportion of dormant seed more than 2-fold when they were imbibed or imbibed and germinated in vinasse solutions. Vinasse might be useful for weed management to reduce germinable weed seedbanks by increasing seedling mortality and seed dormancy either by properly timing of its application as a soil amendment or by purifying herbicidal compounds and using them directly for weed control.

MODELING AND INJURY REPAIR ANALYSIS OF ARTICULAR CARTILAGE BASED ON FIBER CONTENT

2019 ◽  
Vol 19 (08) ◽  
pp. 1940050
Author(s):  
MONAN WANG ◽  
YUANXIN JI ◽  
YUZHENG MA ◽  
JUNTONG JING
Keyword(s):  
Mechanical Properties ◽  
Liquid Phase ◽  
Volume Fraction ◽  
Solid Phase ◽  
Von Mises Stress ◽  
Elastic Model ◽  
Fiber Reinforced ◽  
Element Analysis ◽  
Simulation Results ◽  
Von Mises

It has great guiding significance for the prevention of osteoarthritis and the mechanical state of cartilage after tissue engineering repair to study the relationship between the mechanical properties of cartilage and its structure. This paper considered both the consideration of the solid phase, liquid phase, fiber-reinforced phase in the cartilage and the influence of the contents of major fibers and minor fibers near the cartilage surface. Based on these, a tangential zone of cartilage was established, and a certain improvement and optimization of the fiber-reinforced porous elastic model was performed. The Abaqus software and the Fortran language were used to complete simulation. Simulation results were compared with experiment’s results to verify the validity of the model. Finally, the model was used to perform finite element analysis of different degrees of repairable depth under sliding conditions. Several results were obtained. When the indenter is farther from the interface at the repair site, the mechanical changes in the cartilage are relatively stable. The contact stress of the tangential layer repair and the full-layer repair is small. The volume fraction of the liquid phase in the tangential layer and the full layer repair is lower than that in the other layer regions. The liquid flow rate and the Von Mises stress at the junction of the tangential layer repair are very high. Simulation results were used to explore differences in cartilage mechanical properties of different repairable depths, so as to select the best repairable depth for cartilage.

Numerical Investigation of the Effect of Solid Particles on Liquid Holdup in Stratified Wavy Gas-Liquid Flow in Natural Gas Pipelines

2014 ◽  
Author(s):  
Mahdi Jafari ◽  
Zohreh Mansoori ◽  
Majid Saffar Avval ◽  
Goodarz Ahmadi
Keyword(s):  
Liquid Phase ◽  
Natural Gas ◽  
Solid Phase ◽  
Gas Pipeline ◽  
Solid Particles ◽  
Liquid Holdup ◽  
Horizontal Pipe ◽  
Natural Gas Pipelines ◽  
Gas Liquid Flow ◽  
Liquid Flows

The effect of presence of solid particles on stratified wavy gas-liquid flows has been studied. The height of liquid phase in the natural gas pipeline is a key parameter in designing and can affect the corrosion/erosion rate. In present paper, the numerical four-way simulation of solid particles in gas-liquid wavy stratified flow has been used. The computational model is shown to be able to evaluate the effect of the particles on liquid holdup which is critical for gas pipeline design. The particles cause the liquid phase height in horizontal pipe decreases by increasing the solid phase concentration.

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