Application of Radial Forging and Remelting Treatment to Prepare Semi-Solid Billet of AlMg0.7Si Alloy

2016 ◽  
Vol 256 ◽  
pp. 257-262 ◽  
Author(s):  
Yong Fei Wang ◽  
Sheng Dun Zhao ◽  
Chen Yang Zhang

Semi-solid AlMg0.7Si alloy was prepared by recrystallization and partial melting (RAP) method which including radial forging (RF) and remelting process. RF was carried out with different area reduction ratios (ARRs) to accumulate strains, effect of ARR and remelting time on microstructure was studied, mechanism of RAP preparing semi-solid AlMg0.7Si alloy was summarized. Results show that, compared with the large and irregular solid grains form remelting of starting material, solid grains of semi-solid alloy prepared by RAP are fine and globular, and the optimum microstructure can be obtained when alloy with 80% ARR is remelted at 630 °C for 10 min. With the increase of ARR, the solid grains are smaller and rounder. With the increase of remelting time, the average grain size is increased, and the spheroidization degree of solid grain is gradually improved. The main mechanism consists of pre-deformation, recovery and recrystallization, grains fragmentation, grains spheroidization and coarsening.

2011 ◽  
Vol 211-212 ◽  
pp. 142-146 ◽  
Author(s):  
Wen Liu ◽  
Jian Bo Tan ◽  
Ji Qiang Li ◽  
Xu Ding

An experimental vibrational cooling-shearing slope was developed to prepare the ZAlSi9Mg semi-solid alloy. The results show that the molten alloy is nucleated heterogeneously under shearing of the gravitation and vibration on the inclined cooling plate surface. Primary α-Al phase converts gradually from the cellular dendrite into tiny spherical or granular crystal. Under 600°C of pouring temperature, 600mm of casting length and 50Hz of vibration frequency, the semisolid alloy melt with good microstructure can obtained. In the alloy melt the average grain size of the original α-Al phase is 50μm, and its shape factor is 0.71. Mechanical vibration can refine obviously the microstructure of ZAlSi9Mg alloy. Along with increasing of vibration frequency, the original α-Al phases are refined obviously, their roundness is improved.


2020 ◽  
Author(s):  
Cindy Urueña ◽  
Charlotte Möller ◽  
Jenny Andersson ◽  
Mattias Göransson ◽  
Jan Erik Lindqvist ◽  
...  

<p>The Precambrian shield in southern Sweden exposes a granitic bedrock segment that represents a part of an ancient eroded mountain belt and expose a gradual change in metamorphic grade from cold (<300°C), little affected by recrystallization, to hot (>800°C) and partially molten sections at the west coast (Möller and Andersson, 2018). This area – the Eastern Segment – offers a large scale study of the interdependence of metamorphism, deformation, partial melting, and functional properties of crushed rock aggregates.</p><p>In the petrological community, it is well-known that the evolution of a metamorphic unit (e.g. a high-pressure unit) with respect to pressure, temperature, time, and deformation holds key information on its tectonic history. It has rarely been emphasized, however, that the same factors determine the physical properties of the rock and thus, its technical properties. Basic research in metamorphic petrology thus contributes with a fundament to applied and technical science, e.g. by providing data that lead to quarrying of proper materials.</p><p>This study assesses the variations of technical properties with the metamorphic state, primarily metamorphic temperature and partial melting during metamorphism. Our first results show the correlation between the petrological characteristics and technical properties of felsic orthogneiss within a migmatized eclogite-bearing terrane and its high-pressure granulite-bearing footwall.</p><p>Measurements include the Los Angeles and Micro-Deval value tests. The Los Angeles value is a measure of the resistance to fragmentation (EN 1097-2, 2010). The Micro-Deval test measures the resistance to wear.</p><p>High values of the Los Angeles and Micro-Deval analyses for felsic orthogneiss in the eclogite-bearing domain reflect poor technical properties and are largely linked to that the rocks underwent partial melting. Orthogneisses in the footwall, which recrystallized under high-temperature, dry conditions, and without partial melting, tend to have lower values. This group includes high-quality rocks for the production of aggregates suitable for asphalt base courses and unbound road layers.</p><p>Micro-textures in the orthogneisses are linked with these metamorphic conditions. The clinopyroxene-bearing orthogneisses have complex grain boundaries and micro-perthitic feldspars, finer average grain size, lower biotite content, and absence of migmatitic segregation or penetrative veining. These textures in the footwall orthogneisses contrast with those in the migmatitic orthogneisses from the eclogite-bearing domain, which have a coarser average grain size, even-grained and granoblastic texture, and lack of perthitic texture in feldspars. Thus, these petrographic parameters govern the technical differences.</p><p>Our ongoing research addresses the relations between macro-fabric, micro-texture and technical properties of felsic orthogneiss and metagabbro, respectively, along 120 km profile across the metamorphic field gradient from greenschist- to high-pressure granulite-facies in the Eastern Segment.</p>


2021 ◽  
Author(s):  
Jiayao Yuan ◽  
Xing Chen ◽  
Zhilong Zhao ◽  
Baoshou Sun ◽  
Xuedao Shu

Abstract To seek a fundamental understanding for further improving the Ti-6Al-4V alloy utilization of Cross-Wedge Rolling (CWR) and the comprehensive mechanical properties of shaft parts, the effect of the CWR processing parameters on the microstructure evolution of Ti-6Al-4V alloy shaft preform is studied in this paper. An Arrhenius-type microstructure structure evolution model was employed and implemented into the finite element software DEFORM-3D. The average grain size and dynamic re-crystallization volume fraction distribution in the α+β two-phase region and the β single phase region under different rolling temperature, roller rotating speed and area reduction were analyzed, respectively. It is finding that the area reduction, rolling temperature and roller rotating speed significantly affect the microstructure evolution of Ti-6Al-4V alloy. Meanwhile, the corresponding CWR and Metallographic experiments were conducted to verify the reliability of the FE simulation results. Results showed that the agreement of the process parameters effect on dynamic recrystallization in the α+β two-phase region between simulation and experimental is reasonably good. The difference in average grain size in the β phase region between simulation and experimental is ranged from 5.77% to 18.56%. In addition, the evenly distributed microstructure can be found as the area reduction of 50%, rolling temperature of 950℃ and the speed of 5 r⋅min−1 were employed. After rolling under optimized processing conditions, the tensile strength of Ti-6Al-4V alloy shaft preform increased by 18.57% and the plasticity enhanced significantly due to smaller grain size and bi-model microstructure obtained.


2006 ◽  
Vol 116-117 ◽  
pp. 132-135 ◽  
Author(s):  
Ju Fu Jiang ◽  
Shou Jing Luo

By using equal channel angular extrusion (ECAE) as strain induced step in strain induced melt activated (SIMA) and completing melt activated step by using semi-solid isothermal treatment, a new SIMA method is introduced firstly. The results show that semi-solid billet with highly spheroidal and homogeneous grains with the average grain size of 20μm can be prepared by new SIMA method. High mechanical properties, such as ultimate tensile strength of 321.8MPa and elongation of 15.2% are obtained in magazine plate components thixoforged using semi-solid billet prepared by new SIMA.


2011 ◽  
Vol 66-68 ◽  
pp. 1854-1857
Author(s):  
Rong Xi Yi ◽  
Xiao Qiu Zheng ◽  
Shi Kun Xie ◽  
Xiu Yan Guo

The influences of heating temperature and holding time on the microstructures were investigated during the semi-solid remelting process of rare earth Al-4.5Cu alloy. The evolution mechanism of crystal organization was discussed. Experiments show that the heating temperature and holding time are very important to the grain size and uniformity. It is the most suitable parameters, as heating temperature is 630°C and holding time is 20 minutes, to remelting process. During the remelting process, grain mergering and Ostwald growing up is the main mechanism of change on microstructures.


Author(s):  
Abeyram M Nithin ◽  
M Joseph Davidson ◽  
Chilakalapalli Surya Prakash Rao

The microstructure evolution of sintered and extruded samples of Al–4Si–0.6Mg powder alloys at various semi-solid temperature ranges of 560 °C, 580 °C, and 600 °C, holding times of 600, 1200, and 1800 s, and strain rates of 0.1, 0.2, and 0.3 s−1 was studied. From the stress–strain curves and metallographic studies, Arrhenius grain growth model and Avrami dynamic recrystallization model have been formulated by means of linear regression. Parameters such as peak strain, critical strain, recrystallization fraction, and material constants have been found using the above equations. The experimental and calculated values of various material parameters agree with each other, indicating the accuracy of the developed model. Finite element method-based simulations were performed using DEFORM 2D software, and the average grain size obtained from experiments and simulations was validated by means of average grain size. The relative density of the compacted specimens as well as the extruded specimens was also simulated. The simulation results showed that large grains appeared at high temperatures and at the bottom of the specimen.


2012 ◽  
Vol 192-193 ◽  
pp. 130-135
Author(s):  
Shu Sen Wu ◽  
Chong Lin ◽  
Shu Lin Lü ◽  
Ping An

The microstructure and mechanical properties of Al-17Si-2Fe-2Cu-1Ni (mass fraction, %) alloys with 0.4% or 0.8% Mn produced by semi-solid casting process were studied. The semi-solid slurry of the alloys was prepared by ultrasonic vibration (USV) process. With USV process, the average grain size of primary Si in the alloys could be refined to 21~24μm, whether with or without P modification. The P addition has no further refinement effect on the primary Si in the case of the combined use of USV with P addition. Without USV, the alloys contain a large amount of long needle-like β-Al5(Fe,Mn)Si phase and plate-like δ-Al4(Fe,Mn)Si2 phase. Besides, the alloy with 0.8% Mn contains a small amount of coarse dendritic α-Al15(Fe,Mn)3Si2 phase. With USV treatment and semi-solid casting process, the Fe-containing compounds in the alloys are refined and exist mainly as δ-Al4(Fe,Mn)Si2 particles with average grain size of about 18μm, and only a small amount of β-Al5(Fe,Mn)Si phase is remained. With USV treatment and without P modification, the ultimate tensile strengths (UTS) of the alloys containing 0.4% and 0.8%Mn produced by semi-solid process are 260MPa and 270MPa respectively at room temperature, and the UTS are 127MPa and 132MPa at 350°C.


2010 ◽  
Vol 154-155 ◽  
pp. 1280-1283 ◽  
Author(s):  
Afzalur Alfan ◽  
Mohd Zaidi Omar ◽  
Junaidi Syarif

In order to be considered as a material for semi-solid processing, an alloy has to possess solid spheroids within liquid matrix. Therefore, it is important to investigate the structure of the candidate alloy prior to forming process by conducting partial melting experiment. In this research, the partial melting was conducted for XW-42 steel directly from as annealed condition without any pre-treatment (Direct Partial Remelting). Liquid Fraction Profile obtained from Differential Thermal Analysis (DTA) showed that temperature of 1340°C was located in a low temperature sensitivity region, hence making it as a candidate for processing temperature. Direct Partial Remelting at this temperature for 0, 2 and 5 minutes revealed near spheroidal structure with average grain size between between 45-51 µm which can be considered suitable for semi-solid processing.


2013 ◽  
Vol 58 (1) ◽  
pp. 95-98 ◽  
Author(s):  
M. Zielinska ◽  
J. Sieniawski

Superalloy René 77 is very wide used for turbine blades, turbine disks of aircraft engines which work up to 1050°C. These elements are generally produced by the investment casting method. Turbine blades produced by conventional precision casting methods have coarse and inhomogeneous grain structure. Such a material often does not fulfil basic requirements, which concern mechanical properties for the stuff used in aeronautical engineering. The incorporation of controlled grain size improved mechanical properties. This control of grain size in the casting operation was accomplished by the control of processing parameters such as casting temperature, mould preheating temperature, and the use of grain nucleates in the face of the mould. For nickel and cobalt based superalloys, it was found that cobalt aluminate (CoAl2O4) has the best nucleating effect. The objective of this work was to determine the influence of the inoculant’s content (cobalt aluminate) in the surface layer of the ceramic mould on the microstructure and mechanical properties at high temperature of nickel based superalloy René 77. For this purpose, the ceramic moulds were made with different concentration of cobalt aluminate in the primary slurry was from 0 to 10% mass. in zirconium flour. Stepped and cylindrical samples were casted for microstructure and mechanical examinations. The average grain size of the matrix ( phase), was determined on the stepped samples. The influence of surface modification on the grain size of up to section thickness was considered. The microstructure investigations with the use of light microscopy and scanning electron microscopy (SEM) enable to examine the influence of the surface modification on the morphology of ’ phase and carbides precipitations. Verification of the influence of CoAl2O4 on the mechanical properties of castings were investigated on the basis of results obtained form creep tests.


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