Determination of Free Carbon in Rubber. The Cresol Method

1941 ◽  
Vol 14 (1) ◽  
pp. 241-248 ◽  
Author(s):  
J. B. Roberts

Abstract A simple, accurate method for the determination of free carbon in either raw or vulcanized rubber is presented. It has replaced the nitric acid method entirely in the laboratory of the United States Rubber Company, Detroit, Michigan. A study of the effects of interfering substances, and numerous comparisons of results by the cresol and the nitric acid methods, are given. Results by the cresol method, in the absence of interfering substances, are within 1 per cent of the calculated free carbon content. The method requires only simple apparatus readily available.

1951 ◽  
Vol 24 (1) ◽  
pp. 224-227
Author(s):  
I. M. Kolthoff ◽  
R. G. Gutmacher

Abstract A method for the determination of free carbon in vulcanized rubber stocks is described. The sample is softened in boiling p-dichlorobenzene before treatment with tert-butyl hydroperoxide in the presence of osmium tetroxide. No difficulties are encountered in the filtration of the carbon black. The carbon black is washed on the filter with dilute nitric acid to remove acid-soluble inorganic fillers. The method has been successfully applied to natural rubber, GR-S, Butyl rubber, and Neoprene. No correction is necessary.


Author(s):  
Darya Sergeevna Kareva ◽  
◽  
Sevinj Mahmud kyzy Ismailova ◽  
Elena Evgenievna Dozhdva ◽  
◽  
...  

The article substantiates the need to reform cameral tax control in Russia based on the experience of the United States. The necessity of introducing into the procedure of cameral control the mechanism of requesting all documents confirming the correct determination of tax obligations is determined. The aim of improving the process of desk audits of control is that the new procedure for conducting audits will reduce the likelihood of tax violations.


1915 ◽  
Vol 7 (2) ◽  
pp. 219-239 ◽  
Author(s):  
W. F. Cooper ◽  
W. H. Nuttall

The dipping of sheep and cattle, as a means of eradicating ‘scab,’ lice, ticks, etc., and the diseases which it is now known the latter may transmit, has met with such success, that compulsory dipping is now in vogue in most pastoral countries. Where compulsory dipping obtains, there must of necessity be some system of the standardisation of dips. In Queensland and South Africa, the respective Governments issue official formulae from which the stockbreeder can prepare his own dipping fluid. Only such proprietary dips, as are duly recognised by the Government, may be employed. In the United States, the regulations for the sale of proprietary dips are still more stringent. The quantity of active substance, usually sodium arsenite, nicotine or cresylic acid, is defined within very narrow limits. Further, no proprietary dip is now recognised, unless the manufacturer can furnish a ‘Field Tester,’ by means of which the stockbreeder can himself determine, in a simple and fairly trustworthy manner, the percentage of active constituent in his bath.


Jurnal ICMES ◽  
2018 ◽  
Vol 2 (2) ◽  
pp. 179-196
Author(s):  
Firmanda Taufiq

Throughout 2018, relations between Turkey and the United States seemed to deteriorate. The leaders of the two countries issued sharp diplomatic statements and the US even imposed economic sanctions on Turkey. This article aims to analyze how the future of relations between Turkey and the United States. Cooperation between the two has a long historical side after the Cold War. Relations between the two countries are based on various interests, both economic, political, military and security interests. The theory used in this study is the theory of national interest. The US has great interests in the Middle East and Turkey is the front-line ally in achieving those interests. However, there are many US foreign policies that ignore the Turkish concern and create tensions between the two countries. On the contrary, Turkey also has considerable economic interests, but the role of the government elite (in this case, President Erdogan) has a significant influence in the determination of Turkish foreign policy. The findings of this study, although it will go through complex challenges and processes, the US and Turkey will continue to maintain their relations.


Author(s):  
N.N. Ravochkin ◽  
◽  

The author examines the ideological foundations of political and legal institutional architectonics in Western Europe and the United States and presents its structure. Close attention is paid to the role of social ideas and the development of these issues in modern scientific directions. The author clarifies the principles of synthesis of ideal and institutional and shows three ways of ideological determination of political and legal institutional settings. The mutually conditioned nature of functioning of the system of ideological frameworks and management institutions is substantiated.


Author(s):  
Craig L. Symonds

‘An ad hoc navy: the Revolutionary War (1775–1783)’ describes the Patriots’ response to the British Royal Navy strongholds in Boston and New York and the role of armed vessels during the Revolutionary War. It begins with George Washington’s attempts to threaten the British supply line using boats. The Continental Navy was founded on October 13, 1775, but the new program could hardly challenge the Royal Navy. With the exception of John Paul Jones, the Continental Navy proved mostly disappointing. The United States won its independence largely because the determination of the Patriot forces outlasted the British willingness to fight—and to pay for—a war three thousand miles away.


2019 ◽  
Vol 12 (8) ◽  
pp. 3439-3447 ◽  
Author(s):  
Gan Luo ◽  
Fangqun Yu ◽  
James Schwab

Abstract. The widely used community model GEOS-Chem 12.0.0 and previous versions have been recognized to significantly overestimate the concentrations of gaseous nitric acid, aerosol nitrate, and aerosol ammonium over the United States. The concentrations of nitric acid are also significantly overpredicted in most global models participating in a recent model intercomparison study. In this study, we show that most or all of this overestimation issue appears to be associated with wet scavenging processes. The replacement of constant in-cloud condensation water (ICCW) assumed in GEOS-Chem standard versions with one varying with location and time from the assimilated meteorology significantly reduces mass loadings of nitrate and ammonium during the wintertime, while the employment of an empirical washout rate for nitric acid significantly decreases mass concentrations of nitric acid and ammonium during the summertime. Compared to the standard version, GEOS-Chem with updated ICCW and washout rate significantly reduces the simulated annual mean mass concentrations of nitric acid, nitrate, and ammonium at surface monitoring network sites in the US from 2.04 to 1.03, 1.89 to 0.88, and 1.09 to 0.68 µg m−3, respectively, in much better agreement with corresponding observed values of 0.83, 0.70, and 0.60 µg m−3, respectively. In addition, the agreement of model-simulated seasonal variations of corresponding species with measurements is also improved. The updated wet scavenging scheme improves the skill of the model in predicting nitric acid, nitrate, and ammonium concentrations, which are important species for air quality and climate.


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