Study on the Thermal Insulation Performance of PAN Pre-Oxidised Fibre Felts

2020 ◽  
Vol 28 (3(141)) ◽  
pp. 27-37
Author(s):  
Xiaoming Zhao ◽  
Yuanjun Liu ◽  
Tenglong Liang

In this paper, an orthogonal experiment of 3 factors and 3 levels was firstly designed to prepare PAN pre-oxidised fibre felts with good thermal insulation properties; the range method was used to analyse the result of the orthogonal experiment, and finally the tensile properties and thermal stability were tested. Finally, pre-oxidised fibre felt composites for the coating of silica aerogel were prepared using the coating process to compound silica aerogel on re-oxidised fibre felts. Firstly, the influence of the content of silica aerogel on the heat insulation performance of the coated composite materials was analysed, and then a test of the coefficient of thermal conductivity, an experiment on the back temperature, and characterisations of the tensile properties and thermal stability of the composite coating of pre-oxidised fibre felt composites of the coating of silica aerogel were carried out. Results showed that through analysis of the orthogonal experiment, we can state that the best preparation process of pre-oxidised fibre needled felts was as follows: needle number – 2, needle depth – 8 mm, and needle frequency – 140 times/min. The transverse tensile strength of PAN pre-oxidised fibre needled felts prepared by crossly webbing of PAN pre-oxidised fibres was superior to the longitudinal tensile strength; thermogravimetric analysis showed that the pre-oxidised fibre needled felts had excellent thermal stability. The coefficient of thermal conductivity of the aerogel coating of the composites firstly decreased and then increased with an increase in the content of aerogel. Coated composites had the lowest coefficient of thermal conductivity when the aerogel content was 4% wt. At temperatures of 100 °C, 150 °C and 200 °C, the heating rate of the transient-state back temperature and the steady-state average temperature were both the lowest when the aerogel content was 6% wt.

2011 ◽  
Vol 250-253 ◽  
pp. 502-506
Author(s):  
Jin Xiu Gao ◽  
Xiao Shan Wang ◽  
Lu Bao Li ◽  
Hua Ruan ◽  
Hao Chi Tu ◽  
...  

In recent years, many buildings went up in flames one after another. It is thought-provoking. So the fire-proof property should be considered into one of the most important performance of the building thermal insulation materials. As a result, the study on the expanded perlite lightweight porous inorganic material heated up fast although its application still has some problems to be solved. In this paper, we take the expanded perlite as raw material to make thermal insulation board, and then study on the effect of volume weight on the coefficient of thermal conductivity and tensile strength. What is more important, we find that a new binding agent of Na2O-B2O3-SiO2 syetem sol contributes to improving its water resistance.


2021 ◽  
pp. 0021955X2110626
Author(s):  
Tae Seok Kim ◽  
Yeongbeom Lee ◽  
Chul Hyun Hwang ◽  
Kwang Ho Song ◽  
Woo Nyon Kim

The effect of perfluoroalkane (PFA) on the morphology, thermal conductivity, mechanical properties and thermal stability of rigid polyurethane (PU) foams was investigated under ambient and cryogenic conditions. The PU foams were blown with hydrofluorolefin. Morphological results showed that the minimum cell size (153 μm) was observed when the PFA content was 1.0 part per hundred polyols by weight (php). This was due to the lower surface tension of the mixed polyol solution when the PFA content was 1.0 php. The thermal conductivity of PU foams measured under ambient (0.0215 W/mK) and cryogenic (0.0179 W/mK at −100°C) conditions reached a minimum when the PFA content was 1.0 php. The low value of thermal conductivity was a result of the small cell size of the foams. The above results suggest that PFA acted as a nucleating agent to enhanced the thermal insulation properties of PU foams. The compressive and shear strengths of the PU foams did not appreciably change with PFA content at either −170°C or 20°C. However, it shows that the mechanical strengths at −170°C and 20°C for the PU foams meet the specification. Coefficient of thermal expansion, and thermal shock tests of the PU foams showed enough thermal stability for the LNG carrier’s operation temperature. Therefore, it is suggested that the PU foams blown by HFO with the PFA addition can be used as a thermal insulation material for a conventional LNG carrier.


Molecules ◽  
2018 ◽  
Vol 23 (12) ◽  
pp. 3192 ◽  
Author(s):  
Dong Chen ◽  
Xiaodong Wang ◽  
Wenhui Ding ◽  
Wenbing Zou ◽  
Qiong Zhu ◽  
...  

Owing to their ultra-low thermal conductivity, silica aerogels are promising thermal insulators; however, their extensive application is limited by their high production cost. Thus, scientists have started to explore low-cost and easy preparation processes of silica aerogels. In this work, a low-cost method was proposed to prepare silica aerogels with industrial silica hydrosol and a subsequent ambient pressure drying (APD) process. Various surfactants (cationic, amphoteric, or anionic) were added to avoid solvent exchange and surface modification during the APD process. The effects of various surfactants on the microstructure, thermal conductivity, and thermal stability of the silica aerogels were studied. The results showed that the silica aerogels prepared with a cationic or anionic surfactant have better thermal stability than that prepared with an amphoteric surfactant. After being heated at 600 °C, the silica aerogel prepared with a cationic surfactant showed the highest specific surface area of 131 m2∙g−1 and the lowest thermal conductivity of 0.038 W∙m−1∙K−1. The obtained low-cost silica aerogel with low thermal conductivity could be widely applied as a thermal insulator for building and industrial energy-saving applications.


Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5616
Author(s):  
Katarzyna Uram ◽  
Maria Kurańska ◽  
Jacek Andrzejewski ◽  
Aleksander Prociak

This paper presents results of research on the preparation of biochar-modified rigid polyurethane foams that could be successfully used as thermal insulation materials. The biochar was introduced into polyurethane systems in an amount of up to 20 wt.%. As a result, foam cells became elongated in the direction of foam growth and their cross-sectional areas decreased. The filler-containing systems exhibited a reduction in their apparent densities of up to 20% compared to the unfilled system while maintaining a thermal conductivity of 25 mW/m·K. Biochar in rigid polyurethane foams improved their dimensional and thermal stability.


2021 ◽  
Vol 887 ◽  
pp. 480-486
Author(s):  
T.N. Vachnina ◽  
I.V. Susoeva ◽  
A.A. Titunin ◽  
S.V. Tsybakin

Many plant wastes are not currently used in production, they are disposed of in landfills or incinerated. The aim of this study is to develop a composite thermal insulation material from unused spinning waste of flax and cotton fibers and soft wood waste. Samples of thermal insulation materials from plant waste were made by drying using the technology of production of soft wood fiber boards. For composite board defined physico-mechanical characteristics and thermal conductivity. The experiment was carried out according to a second-order plan, regression models of the dependences of the material indicators on the proportion of the binder additive, drying temperature and the proportion of wood waste additives were developed. The study showed that composites from unused spinning waste of plant fibers and soft wood waste have the necessary strength under static bending, the swelling in thickness after staying in water is much lower in comparison with the performance of boards from other plant fillers. The coefficient of thermal conductivity of the boards is comparable with the indicator for mineral wool boards.


2020 ◽  
Vol 15 (2) ◽  
Author(s):  
K. Keerthi Sanghamitra ◽  
A. Yamini ◽  
A. Venu Vinod ◽  
Neha Hebalkar

AbstractAerogels are regarded as the superior thermal insulating materials for wide range of temperatures, from cryogenic insulation, cold water diving garments to high temperature applications and even to defense and aerospace applications. For most of such applications, the aerogels are used in composite form rather than monolithic form as aerogels are fragile in nature due to its high porosity of up to 98%. These composites constitute aerogel infiltrated fiber mats to give flexibility, on the other hand, compromises on the insulation performance due to reinforcing aerogel with fibers that have comparatively higher thermal conductivity than silica aerogel. To increase the efficiency, density of the fiber mat needs to be reduced to incorporate higher loading of silica aerogel. Many techniques are being used to study the insulation performance of these composites. This paper presents about the study of insulation performance of fibre mats with different aerogel content and composition using a well-known thermography technique. The morphological, compositional, thermal and physical studies of the fiber mats and its composites using FESEM, EDAX, BET, thermal conductivity etc., are discussed.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3075
Author(s):  
Štěpán Hýsek ◽  
Pavel Neuberger ◽  
Adam Sikora ◽  
Ondřej Schönfelder ◽  
Gianluca Ditommaso

This study provides a solution for the utilization of two waste materials, namely the residues of soft polyurethane foam from the production of mattresses and winter wheat husks. Thermal insulation panels with a nominal density of 50–150 kg/m3, bonded one-component moisture curing polyurethane adhesive, were developed, and the effect of the ratio between recycled polyurethane foam and winter wheat husk on internal bond strength, compressive stress at 10% strain, water uptake, coefficient of thermal conductivity, and volumetric heat capacity was observed. The developed composite materials make use of the very good thermal insulation properties of the two input waste materials, and the coefficient of thermal conductivity of the resulting boards achieves excellent values, namely 0.0418–0.0574 W/(m.K). The developed boards can be used as thermal insulation in the structures of environmentally friendly buildings.


2012 ◽  
Vol 535-537 ◽  
pp. 239-242
Author(s):  
Alena Kalužová ◽  
Jan Pěnčík ◽  
Libor Matějka ◽  
Libor Matějka ◽  
Tomáš Pospíšil ◽  
...  

Recycling of materials is an important point of sustainable construction. The aim is to find a compromise between energy saving, economy and ecology. The contribution discusses the production of thermal insulation composite material made of polymers. Uniform dispersion of grains of foamy glass waste (filler) in polymer filling from recycled thermoplastics induces formation of particle composite. The production supports usage of secondary raw materials. Decisive properties in choosing the materials to be applied include mainly the coefficient of thermal conductivity, density, compressive strength and water absorption.


2016 ◽  
Vol 39 (S2) ◽  
pp. E664-E670 ◽  
Author(s):  
Djamila Kada ◽  
Ahmed Koubaa ◽  
Ghezalla Tabak ◽  
Sebastien Migneault ◽  
Bertrand Garnier ◽  
...  

2020 ◽  
Vol 3 (3) ◽  
pp. 21-27 ◽  
Author(s):  
T. Drozdyuk ◽  
Arkadiy Ayzenshtadt ◽  
M. Frolova ◽  
Rama Shanker Rama Shanker Verma

the paper shows the possibility of producing a thermal insulating composite based on basalt fibers and sapo-nite-containing mining waste. A method for manufacturing thermal insulating composites from hydro-mass with different contents of the mixture components is proposed. Basalt fibers were used as a filler, and pre-mechanoactivated saponite-containing material (SCM) was used as a binder. It was found experimentally that depending on the composition of composites, the coefficient of thermal conductivity varies from 0.1109 to 0.1342 W/(m•K), and the compressive strength – from 0.45 to 0.93 MPa. In addition, it was found that thermal modification of composites at temperatures up to 1200°C significantly (up to 3 times) increases the compressive strength of composites, while not affecting the coefficient of thermal conductivity. The ex-periments to determine the conductivity of the composite “basalt fiber – SСM” depending on its moisture content showed that the obtained composite is characterized by intense and linear increase in the values of conductivity when the humidity of the sample to 12% and further increase in humidity practically does not change the values of the coefficient of thermal conductivity. Comparison of the studied thermal insulation composite with known structural thermal insulation materials in terms of its thermal insulation and strength characteristics showed that it is comparable to gas and foam blocks. It should also be noted that this material is environmentally safe and can withstand high temperatures without collapsing.


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