Analysis of chemical properties of Extracted Aged Asphalt Binder based on Fourier transform infrared (FTIR) spectrometry

2021 ◽  
Vol 23 (1) ◽  
pp. 115-124
Author(s):  
Sang-Min Yu ◽  
Chi-Su Lim ◽  
Oh-Sun Kwon ◽  
Jaejun Lee
2014 ◽  
Vol 548-549 ◽  
pp. 133-136
Author(s):  
Yusoff Way ◽  
Hadi Puwanto ◽  
Farizahani ◽  
P.T. Pham

Selective Laser Sintering (SLS) or Laser Sintering (LS) allows functional parts to be produced in a wide range of powdered materials using a dedicated machine, and is thus gaining popularity within the field of Rapid Prototyping (RP). One of the advantages of employing LS is that the loose powder of the building chamber can be recycled. The properties of polymer powder significantly influence the melt viscosity and sintering mechanism during Laser Sintering (LS) processes which results in a good surface finish. The objective of this research is to investigate the chemical composition of fresh polymer materials used in Laser Sintering. There are seven virgin SLS materials which are PA2200, GF3200, Alumide, PrimeCast, PrimePart, Duraflex and CastForm. Fourier Transform Infrared Spectroscopy (FTIR) was used to analyze the chemical composition of the materials by using infrared radiation and absorbed frequency. The spectra show that similar functional groups were found in the materials apart from PrimePart and Duraflex. Obtained data from this analysis could be used to investigate on how the fresh and recycled powder materials with different chemical properties would affect the part surface finish.


Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1466
Author(s):  
Carmen Steluta Ciobanu ◽  
Daniela Predoi ◽  
Patrick Chapon ◽  
Mihai Valentin Predoi ◽  
Simona Liliana Iconaru

Samarium doped hydroxyapatite (Ca10−xSmx(PO4)6(OH)2, xSm = 0.5, 50SmHAp) is a very promising candidate to be used for different coatings in various dental and orthopedic implants. We report, for the first time, the obtaining of 50SmHAp thin films by a cost-effective method, namely spin coating. Thin films of 50SmHAp on silicon substrate have been analyzed by various techniques such as Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), atomic force microscopy (AFM), Metallographic microscopy and Glow Discharge Optical Emission Spectroscopy (GDOES). The stability of 50SmHAp suspension was evaluated by ultrasound measurements. Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were also used to evaluate the 50SmHAp suspension. The antifungal activity of 50SmHAp suspension and coatings was assessed using Candida albicans ATCC 10231 fungal strain (C. albicans). The results of the antifungal assays depicted that both 50SmHAp suspensions and coatings were effective in inhibiting the development of C. albicans fungal cells, thus making them ideal candidates for the development of novel antifungal agents. The obtained results give new perspective for possible applications of 50SmHAp thin films in various medical applications due to their antifungal properties.


2017 ◽  
Vol 737 ◽  
pp. 547-553
Author(s):  
Iva Krcmova ◽  
Petr Hyzl ◽  
Pavla Nekulova ◽  
Pavel Coufalik ◽  
Ondrej Dasek

With increased demand and limited aggregate and binder supply, hot mix asphalt (HMA) producers discovered that reclaimed asphalt pavement (RAP) is a valuable component in HMA. This paper is concerned with the current issue of higher using RAP (Reclaimed Asphalt Pavement) in asphalt mixtures for pavement wearing courses. It describes the effects of application of three types of rejuvenation additives on properties of aged asphalt binders made from a regular RAP. These rejuvenation additives restore the physical and chemical properties of aged binders. In addition, the aged asphalt binder with rejuvenators applied was subjected to a short-term laboratory aging using the RTFOT (Rolling Thin Film Oven Test). This method simulate aging asphalt binder during the manufacturing process and laying. To assess the binder properties, both the standard empirical tests and more advanced functional tests (dynamic shear rheometer and bending beam rheometer) have been performed. Last part of the paper provides an evaluation of the individual rejuvenation additives. Based on the results it can be concluded that a positive change in properties of aged asphalt binder after applying all the three rejuvenators has been proven.


2015 ◽  
Vol 7 (13) ◽  
pp. 5695-5701
Author(s):  
Rafaela M. R. Bezerra ◽  
Ana C. O. Neves ◽  
Alexandre S. Pimenta ◽  
Kássio M. G. Lima

The aim of the present work was to estimate fixed-carbon, volatile matter and ash contents in Brazilian commercial charcoal.


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