Study on Influence of Surface Plasma Activation of Quartz Fiber/Cyanate Ester Composite at Meter Range Working Distance

The surface of quartz fiber/cyanate ester composite at meter working distance was activated by plasma treatment technology. Influence of plasma treatment parameters on surface contact angle of the composite was investigated, as well as changes of surface morphology, intrinsic performance and membrane-based bonding strength. Results showed that surface contact angle of the composite decreased significantly after plasma treatment with nitrogen and argon. Moreover, activation effect of argon plasma was better than that of nitrogen plasma. With the increase of voltage, surface contact angle of composite became smaller and activation effect was better. After plasma treatment, glass transition temperature (Tg) and bending strength of the composite did not change, and intrinsic property of the composite was not damaged. After plasma treatment, surface roughness and specific surface area of the composite increased, and membrane-based bonding strength of the composite with Al coating increased significantly.

The High-Temperature Tensile Test of Quartz Fiber Fabric- Reinforced Resin Composites

The tensile properties of quartz fiber fabric-reinforced resin composites at high temperature were studied. The effects of specimen type and dimension, temperature loading procedure, holding time and loading rate on the tensile properties of the composites at high temperatures were analyzed through series of comparative experiments, the tensile test parameters were determined. Chinese national standard for high-temperature tensile property testing of the composites was compiled based on the data collected. According to the established standard, the tensile testing at 500°C was carried out. Compared with the tensile properties at room temperature, the tensile strength and tensile modulus of the composite at high temperature decreases significantly, with the tensile strength decreasing by about 42.32% and the tensile modulus decreasing by about 24.18%. This is mainly due to the high temperature which causes part of the resin matrix to pyrolyze and detach from around the fiber, thus losing the integrity of the material. In addition, this national standard for high-temperature tensile properties has some general applicability to different types of fiber-reinforced resin composites.

A novel insertion design of fiber materials for the adhesive reattachment in vertically fractured teeth

Objective This ex vivo study aimed to evaluate the strengthening effect of different ferrule and reattachment designs with fiber and adhesive materials on vertically fractured teeth. Methods Ninety extracted single-root premolars were instrumented and divided into nine groups (two control groups and seven experimental groups; n = 10). The negative control (NC) group comprised of intact teeth, while the positive control (PC) group comprised of root canal-treated teeth. The roots of the teeth in the experimental groups were vertically fractured into two equal fragments. The fragments were reattached with one of the followings: 4-methacryloxyethyl trimellitate anhydride/methacrylate-tri-n-butyl borane (4-META/MMA-TBB) resin, 4-META/MMA-TBB + quartz fiber post, 4-META/MMA-TBB + glass fiber bundles, 4-META/MMA-TBB + quartz fiber post + 1 mm ferrule, 4-META/MMA-TBB + glass fiber bundles + 1 mm ferrule, 4-META/MMA-TBB + quartz fiber post + 2 mm ferrule, and 4-META/MMA-TBB + glass fiber bundles + 2 mm ferrule. The core build-ups were made with composite resin. The specimens were subjected to compressive loading until failure occurred. Mean load necessary to fracture each sample and the fracture types of these samples were recorded. Results The highest mean fracture load was recorded in the NC group (1,036.7 N), which was not significantly higher than the PC group (989.66 N) (p > 0.05). The roots reattached with quartz fiber post demonstrated significantly less fracture strength (871.9 N) as compared to the other test and control groups (p < 0.05). There was no significant difference between the PC group and reattached fragments with different ferrule designs in terms of fracture resistance (p > 0.05). Conclusions The customized fiber bundles may be more suitable for reattachment of vertically fractured teeth than the rigid fiber posts. For reattachment procedures, the ferrule design may be preferred to increase the fracture strength of vertically fractured teeth.

Characterization of black crusts developed on historic stones with diverse mineralogy under different air quality environments

Black crusts (BCs) are one of the most critical alteration forms found on stones belonging to architectural heritage. Since they could be considered as passive samplers of atmospheric pollution, it would be plausible to establish relations between the air contamination and the BCs. With this aim, we have characterized BCs collected on historic buildings from two Spanish cities (Granada and Vigo) with different polluted atmospheres, as well as formed on stone substrates of varied mineralogy and texture. Likewise, in order to assess the impact of the atmospheric pollutants on the growth of BCs, quartz fiber filters were used as surrogate substrates and placed nearby the studied buildings to collect and analyze the aerosol particulate matter (PM). To this end, an array of complementary analytical techniques was used to evaluate the mineralogy, chemical composition, and texture of the BCs and to establish the correlation with the ions, OC (organic carbon), and EC (elemental carbon) detected in the PM on the quartz fiber filters. As result, BCs developed on carbonate substrates from Granada show more complex structure than those from Vigo, which are thinner because of frequent rain episodes. In both cities, NaCl, Pb-Cl, and Ca-Cl-rich particles, Ca-phosphate particles and clusters of Ba-sulfate-rich particles were detected. However, metal-rich rounded particles were more abundant in Granada’s BCs, including soot particles. BCs from Granada were richer in carbonaceous components (OC and EC) than the Vigo’s BCs. Although in the filters PM did not show EC—mainly due to traffic—, in the BCs from both locations OC and EC were detected. Therefore, this different composition was related to the mineralogy of the stones and the higher pollution of Granada in contrast to the industrial and sea-exposed city of Vigo.

Performance Comparison of Aerospace High-Temperature Resistant Ceramic Fiber Felt

Be aimed at the development and application of aerospace high-temperature resistant ceramic fiber felt, in this paper, as the common ceramic fiber felt in the field of high temperature resistance, quartz fiber felt, high silica fiber felt and mullite fiber felt were compared. The microstructure, thermal insulation, temperature resistance and mechanical properties were analyzed respectively, the performance advantages and disadvantages of three kinds of ceramic fiber felt were given, and its internal causes were studied. The results show that, the temperature resistance of mullite fiber felt is better than that of quartz fiber felt and high silica fiber felt, mainly due to its polycrystalline mullite structure, the thermal insulation performance of mullite fiber felt and high silica fiber felt is better than quartz fiber felt at high temperature, mainly due to the thermal reflection of polycrystalline mullite and the small pore structure of high silica fiber felt, the compressibility of quartz fiber felt is better than high silica fiber felt and mullite fiber felt.

Modeling of 980 nm and 1470 nm Laser Radiation Absorbance Efficiency in the Blood Vessel Depending on the Structure of Titanium–Containing Optothermal Fiber Converter

Using quartz fiber with titanium-containing optothermal fiber converter (TOTFC) is promising in endovenous laser coagulation (EVLA) for the treatment of varicose veins. This study aims to research the variation in the optical properties of TOTFC as its microstructure changes under the condition that TiO2 spheres inside converter are arranged in such a way that the Mie theory approximation can be applied. The absorbance efficiency of laser energy with 980 nm and 1470 nm wavelengths for TOTFC has been calculated. Optical multidimensional simulation for the EVLA process was developed and calculated. The optimal ranges of microstructure’s parameters for TOTFC in the EVLA process were discussed.