This study sought to create a biocomposite of Magnesium and Titanium via a powder metallurgy technique. Powder metallurgy technique was used to produce three different volume percentages of Magnesium (30% , 35% , 40%). Titanium powder was mixed with Magnesium, then the samples were compressed by 1800 Bar using a cold, isostatic press process. The samples were then sintered to 850 for 100 min. At this temperature, the compressive yield strength was increased to 210 Mpa and significantly depended on the volume percent of Magnesium present, the core size and temperature of sintering. The bioactivity of the samples in a simulated body fluid (SBF) was also investigated. When the samples were immersed in the simulated body fluid for a 14 and 28 days, calcium and other elements were found to be deposited on the surface. Additionally, it was found that TiO2 has the ability to induce the formation of bone-like apatite in the SBF. In addition, the degradation product of Magnesium in a biological system caused a rise in the pH and environment for the deposition of calcium and other element on the surface were enhanced. Finally, the samples were analyzed using XRD, EDS, and optical and scanning electron microscopy (SEM).