Predicting the Delamination Mechanisms of Multidirectional Laminates Using the Energy Release Rate Obtained from AE Monitoring

This study investigates delamination damage mechanisms during the double cantilever beam standard test using the strain energy release rate. The acoustic emission parameter is used to replace the original calculation method of measuring crack length to predict delamination. For this purpose, 24-layer glass/epoxy multidirectional specimens with different layups, and interface orientations of 0°, 30°, 45°, and 60°, were fabricated based on ASTM D5528 (2013). Acoustic emission testing (AE) is used to detect the damage mechanism of composite multidirectional laminates (combined with microscopic real-time observation), and it is verified that the strain energy release rate can be used as a criterion for predicting delamination damage in composite materials. By comparing the AE results with the delamination expansion images observed by microvisualization in real time, it is found that the acoustic emission parameters can predict the damage of laminates earlier. Based on the data inversion of the acoustic emission parameters of the strain energy release rate, it is found that the strain energy release rate of the specimens with different fiber interface orientations is consistent with the original calculated results.

Experimental Investigation on the Propagation of Hydraulic Fractures through Coal-Rock Interfaces

Although hydraulic fracturing has been one of the primary stimulation methods for coal-bed methane (CBM) exploration, it is difficult to be applied in soft and low-permeability coal seams due to the instability of wells in such geological structures. In order to solve the problem, an idea of indirect fracturing is proposed, that is, fractures are initiated in stable and hard rocks and then propagated to coal seams in which crack networks can be formed. To verify the feasibility of such an approach, the true triaxial hydraulic fracturing experiments were conducted using two-dimensional and three-dimensional coal-rock combination samples, respectively. This study investigates the fracture patterns, pressure variation, and fracture morphology. The results show that in the process of fracture propagation from sandy mudstones to coals, the strain energy release rate in the sandy mudstones is 10.69∼25.53 times greater than that in the coal. When the fracture has a tendency to deflect toward the lower strength coal strata, under the condition of large K2/K1, the deflection criterion will be met first and the fracture will deflect and grow into the coal strata. In addition, the complex crack network can be generated when the hydrofracture intersects the coal-rock interface and the fracture pattern is analyzed.

Brittleness of Concrete under Different Curing Conditions

In order to shorten construction periods, concrete is often cured using steam and is loaded at an early age. This changes the performance and even the durability of the concrete compared to concrete that has been cured under normal conditions. Thus, the pattern and the mechanism of concrete performance change under different curing conditions, and loading ages are of great significance. The development of brittleness under different curing conditions and loading ages was studied. The evaluation methods that were used to determine concrete brittleness were expounded. Steam, standard, and natural curing conditions were carried out on single-side notched concrete beams as well as on a concrete prism and cubic blocks. The compressive strength and splitting tensile strength of the concrete blocks along with the fracture performance of the concrete beams were tested after 3, 7, 28, and 90 days. The steam curing condition significantly improved the strength of concrete before 28 days had passed, and the standard curing condition improved the strength of concrete after 28 days. Based on the experimental fracture parameters, a two-parameter fracture model was applied to study the development of fracture toughness KICS, critical crack tip opening displacement CTODc, and critical strain energy release rate GICS with hydration age under different curing conditions. With respect to long-term performance, the standard curing condition was better at resisting concrete crack propagations than the steam curing condition was. The characteristic length lch and the material length Q under the three curing conditions and the long-term development of brittleness in the concrete indicated that steam curing increased the concrete brittleness. Considering the effects of the curing condition and the loading age, a time-dependent concrete fracture toughness model was established, and the predicted value of the model was verified against the measured value. The results indicated that the model was able to accurately predict the fracture toughness with an error rate of less than 16%.

Resistance of Polymeric Laminates Reinforced with Fabrics against the Growth of Delaminations

Dependence of the initiation values of the Strain Energy Release Rate, GCi, on the orientation of the reinforcement direction α relative to the delamination front was investigated for two laminates of different interfacial ply arrangements. In the case of the first laminate, the delamination was located at the interface of the layers reinforced with symmetric fabric and unidirectional fabric. In the case of the second laminate, the delamination was located at the interface of layers reinforced with symmetric fabric. In both laminates, the orientation of fibers in the layers separated by the delamination differed by 45° regarding the warp directions. The investigations were carried out for Mode I, Mode II, and Mixed-Mode I/II (GII/GI = 1 and GII/GI = 1.7) loadings using hybrid beam specimens. The major problem appearing in the intended tests was the inevitable lack of symmetry in the xz and xy planes of the specimens and the resulting deformation and stress–strain couplings, causing undesired loading modes. To decrease these couplings, especially designed hybrid beam specimens were used. An auxiliary finite element analysis was performed to assess the remaining effects of the reduced couplings. To ascertain whether statistically significant differences between Gci values for different α occurred, the one-way analysis of variance supplemented by Levene’s test was carried out. The dependence of Gci on α was found out for both laminates. However, it was not equally strong, and it turned out that the loading mode and the interfacial ply were arrangement sensitive.

Experimental characterization of Mode II fatigue delamination growth onset in composite Joints

In this article, the structural behavior of co-cured composite joint (CC), co-bonded composite joint (CB), and secondary-bonded composite joint (SB) under Mode II fatigue loading was evaluated. Fatigue performance was evaluated in sub-critical strain energy release rate (SERR) associated with Mode II fatigue induced delamination growth onset. Fatigue tests were carried out using the three-point bending End Notched Flexure test setup for different energy ratios. The experimental results are presented in terms of SERR versus number of cycles, and the SERR threshold for no growth is determined (Gth). Fractographic analyses were performed in order to identify the main failure mechanisms related to each joining technology under Mode II. The results indicated an initial cohesive failure followed by an adhesive failure promoted by crack propagation at the interface between the adhesive and the composite adherend on SB and CB samples, through the coalescence of microcracks that promote the adhesive failure process, leading to fiber pull-out from the matrix and cusps formation in the fracture surface. These results explain the low performance behavior observed on SB and CB bonded techniques. It is worth mentioning that the results and behavior observed in this work are valid only for the laminates, adhesives, surface treatment, and environmental conditions tested herein.

Evolution of Potting-PCB Interfacial Reliability After Long Term High Temperature Operation

Fine Pitch Electronic Components are reinforced using epoxy potting compounds and underfills to improve reliability and survivability, in extreme environments. Potting of electronic components offers structural support, shock damping and protection for the components from environmental conditions like moisture. Potting is one of the cost-effective and viable way to improve the survivability of the electronic components. On dynamic shock loading, interfacial delamination occurs between the potting material and the PCB, which further propagates to solder interconnect failures. The interfacial properties change with long-term exposure to temperature during operating and storage conditions. Mechanics of interface delamination of the epoxy potted PCB samples with thermal aging is a primary focus on this paper. Determination of fracture parameters such as fracture toughness and strain energy release rate at steady state stress is important in selection of the potting material and the reliability study of the supplemental restraint systems. PCB/Epoxy specimens are prepared, and their fracture behavior is observed under quasi-static three-point and four-point bend loading. In three-point bending, the peak stress acts at the midpoint of the specimen. In four-point bend loading, the peak stress is along whole area of the specimen under load (load span). The curing temperature providing the best fracture resistance is selected and followed throughout the study. The samples are exposed to 100°C for 30days and 60 days. Under dynamic loading, damage at the interface is studied. The experimental results provide the peak critical load, from which the fracture toughness parameters are calculated. A comparison has been made on fracture toughness and crack initiation of the PCB/Epoxy systems, based on flexure method and thermal aging.