Effect of Initial Structure on the Characteristics of Austenite Formed Under Heat Treatment of Spring Steels

Author(s):  
M. N. Cheerova ◽  
T. V. Komarova ◽  
V. N. Dubinskii
2014 ◽  
Vol 716-717 ◽  
pp. 74-78
Author(s):  
Fei Zhao ◽  
Huan Zhang ◽  
Yi Long Liang

An investigation of low Si spring steels (50CrVA) subjected to quenching-isothermal-quenching-tempering (Q-I-Q-T) process is presented. The results indicated that Q-I-Q-T process lead to the excellent mechanical properties compare to those treated by traditional heat-treatment, quenching and tempering, owing to the multiphase structure. The Q-I-Q-T treated microstructure consists of martensite, retained austensite, bainite and fine distributed carbides.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4159
Author(s):  
Marina Gushchina ◽  
Gleb Turichin ◽  
Olga Klimova-Korsmik ◽  
Konstantin Babkin ◽  
Lyubov Maggeramova

Additive manufacturing of titanium alloys is one of the fastest growing areas of 3D metal printing. The use of AM methods for parts production in the aviation industry is especially promising. During the deposition of products with differently sized cross-sections, the thermal history changes, which leads to non-uniformity of the structure and properties. Such heterogeneity can lead to failure of the product during operation. The structure of deposited parts, depending on the thermal cycle, may consist of α’, α + α’ + β’, and α + β in different ratios. This problem can be solved by using heat treatment (HT). This paper presents research aimed towards the determination of optimal heat treatment parameters that allows the reception of the uniform formation of properties in the after-treatment state, regardless of the initial structure and properties, using the example of a deposited Ti-6Al-4V gas turbine blade.


2021 ◽  
Vol 87 (7) ◽  
pp. 30-37
Author(s):  
V. V. Kozlov ◽  
A. A. Vasilev ◽  
I. G. Gorichev ◽  
A. Т. Kalashnik ◽  
V. G. Kostishin ◽  
...  

Developing of nanotechnology-based electronics entails developing of new carbon nanocrystalline materials with predetermined physicochemical properties, e.g., obtained by synthesis of polyacrylonitrile (PAN) in conditions of heat treatment. We have studied the properties of PAN heat-treated in air in the temperature range 150 – 250°C and the effect of stabilization on the kinetic parameters of synthesis and thermochemical properties of carbon material upon heat treatment in N2 atmosphere. It is shown that an increase in the temperature of a preliminary treatment up to 200°C leads to a decrease in the activation energy and pre-exponential factor compared to the corresponding values characteristic for the initial polymer (from 90.9 and 3.1 × 106 to 53.3 kJ/mol and 1.1 × 103 min–1, respectively), which indicates to the occurrence of diffusion limitations. When the temperature of a preliminary treatment in air increases from 180 to 250°C, the difference between temperature peaks for DSC and TGA curves decreases due to appearance of a «core-shell» structure. XRD data indicate that the initial PAN structure does not change up to 150°C. Further increase in the temperature leads to significant changes in the initial structure of the polymer which are manifested in a decrease in the peak area in the X-ray diffraction pattern of the polymer. The results obtained can be used in the development of a method for the synthesis of carbon materials with controlled properties predetermined at the stage of stabilization.


1984 ◽  
Vol 34 ◽  
Author(s):  
J. M. Schissler ◽  
J. Saverna ◽  
R. Bellocci ◽  
C. Bak

ABSTRACTAs heat treatments of metallic alloys generally require high temperatures, energy saving cycles are increasingly looked for. Castings offer the advantage over wrought products of possible hot shake out as they are just made.The object of this study was to observe the structure of a SG cast iron resulting from hot shakeout right after the end of solidification, followed or not by a 1 000°C holding and subsequent heat treatment.The austenite then presents the peculiarity of not having been re-generated by heating up from an initial structure as it is the case in conventional cycles.This study has clearly showed the influence of composition heterogeneity within the solidification cell on the response to heat treatment. Along the solidification cell boundary, an increase in carbon and manganese contents was found while silicon decreased. Along the SG nodules, the opposite is true. Between these two zones, gradients vary. The presence of these three areas results in having three different CCT curves and, therefore, a varying response to heat treatment. This is even magnified by the section size of the sample because the cell size increases, but this is minimized by the decrease in quenching rate.Structural differences observed in hot shake out samples and re-heated samples, both held or not at 1 000°C, and then cooled down, are directly related to these composition heterogeneities:- hot shakeout cast iron shows a high hardenability which varies with the holding time at 1 000°C;- after a ferritizing treatment, an homogeneous matrix is difficult to obtain from a hot shakeout cast iron;- after austempering the structural heterogeneity of the cell boundary is greater for the hot shakeout cast iron;- after the pearlitic transformation, the structure of the hot shakeout cast iron is similar to that resulting from conventional treatment.


Author(s):  
R. M. Anderson

Aluminum-copper-silicon thin films have been considered as an interconnection metallurgy for integrated circuit applications. Various schemes have been proposed to incorporate small percent-ages of silicon into films that typically contain two to five percent copper. We undertook a study of the total effect of silicon on the aluminum copper film as revealed by transmission electron microscopy, scanning electron microscopy, x-ray diffraction and ion microprobe techniques as a function of the various deposition methods.X-ray investigations noted a change in solid solution concentration as a function of Si content before and after heat-treatment. The amount of solid solution in the Al increased with heat-treatment for films with ≥2% silicon and decreased for films <2% silicon.


Author(s):  
E. Bischoff ◽  
O. Sbaizero

Fiber or whisker reinforced ceramics show improved toughness and strength. Bridging by intact fibers in the crack wake and fiber pull-out after failure contribute to the additional toughness. These processes are strongly influenced by the sliding and debonding resistance of the interfacial region. The present study examines the interface in a laminated 0/90 composite consisting of SiC (Nicalon) fibers in a lithium-aluminum-silicate (LAS) glass-ceramic matrix. The material shows systematic changes in sliding resistance upon heat treatment.As-processed samples were annealed in air at 800 °C for 2, 4, 8, 16 and 100 h, and for comparison, in helium at 800 °C for 4 h. TEM specimen preparation of as processed and annealed material was performed with special care by cutting along directions having the fibers normal and parallel to the section plane, ultrasonic drilling, dimpling to 100 pm and final ionthinning. The specimen were lightly coated with Carbon and examined in an analytical TEM operated at 200 kV.


Author(s):  
A.H. Advani ◽  
L.E. Murr ◽  
D. Matlock

Thermomechanically induced strain is a key variable producing accelerated carbide precipitation, sensitization and stress corrosion cracking in austenitic stainless steels (SS). Recent work has indicated that higher levels of strain (above 20%) also produce transgranular (TG) carbide precipitation and corrosion simultaneous with the grain boundary phenomenon in 316 SS. Transgranular precipitates were noted to form primarily on deformation twin-fault planes and their intersections in 316 SS.Briant has indicated that TG precipitation in 316 SS is significantly different from 304 SS due to the formation of strain-induced martensite on 304 SS, though an understanding of the role of martensite on the process has not been developed. This study is concerned with evaluating the effects of strain and strain-induced martensite on TG carbide precipitation in 304 SS. The study was performed on samples of a 0.051%C-304 SS deformed to 33% followed by heat treatment at 670°C for 1 h.


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