scholarly journals Microstructural Changes During Short-Term Heat Treatment of Martensitic Stainless Steel—Simulation and Experimental Verification

2021 ◽  
Author(s):  
N. Schmidtseifer ◽  
S. Weber
Keyword(s):  
Heat Treatment ◽  
Martensitic Stainless Steel ◽  
Computer Assisted ◽  
Austenitizing Temperature ◽  
Short Term ◽  
Microstructural Changes ◽  
Martensitic Stainless Steels ◽  
Treatment Processes ◽  
Start Temperature ◽  
Steel Heat

AbstractShort-term heat treatments of steels are used for tools and cutlery but also for the surface treatment of a variety of other workpieces. If corrosion resistance is required, martensitic stainless steels like AISI 420L or AISI 420MoV are typically used. The influence of short-term heat treatment on the different metastable states of the AISI 420L steel was examined and reported in this article. Starting from a defined microstructural state, the influence of a short-term heat treatment is investigated experimentally with the help of a quenching dilatometer and computer assisted simulations are carried out. With the results obtained, a simulation model is built up which allows to compute the microstructural changes during a short-term heat treatment to be evaluated without the need for an experiment. As an indicator, the value of the martensite start temperature is calculated as a function of different holding times at austenitizing temperature. The martensite start temperature is measured by dilatometry and compared to calculated values. Validation of simulated results reveals the potential of optimizing steel heat treatment processes and provides a reliable approach to save time, resources and energy.

Microstructure and Properties of Heat-Treated 440C Martensitic Stainless Steel

2013 ◽  
Vol 334-335 ◽  
pp. 105-110 ◽  
Author(s):  
Siti Hawa Mohamed Salleh ◽  
Mohd Nazree Derman ◽  
Mohd Zaidi Omar ◽  
Junaidi Syarif ◽  
S. Abdullah
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Stainless Steel ◽  
Martensitic Stainless Steel ◽  
Ferrite Matrix ◽  
Rapid Quenching ◽  
Heat Treated Sample ◽  
Treatment Processes ◽  
Heat Treated ◽  
Treated Sample

440C martensitic stainless steels are widely used because of their good mechanical properties. The mechanical properties of 440C martensitic stainless steel were evaluated after heat treatment of these materials at various types of heat treatment processes. The initial part of this investigation focused on the microstructures of these 440C steels. Microstructure evaluations from the as-received to the as-tempered condition were described. In the as-received condition, the formations of ferrite matrix and carbide particles were observed in this steel. In contrast, the precipitation of M7C3carbides and martensitic structures were present in this steel due to the rapid quenching process from the high temperature condition. After precipitation heat treatment, the Cr-rich M23C6carbides were identified within the structures. Moreover, a 30 minutes heat-treated sample shows the highest value of hardness compared to the others holding time. Finally, the tempering process had been carried out to complete the whole heat treatment process in addition to construct the secondary hardening phenomenon. It is believed that this phenomenon influenced the value of hardness of the 440C steel.

Isothermal treatment of nitrided layers formed on steels

2019 ◽  
Vol 25 (4) ◽  
pp. 34-41
Author(s):  
Piotr Nawrocki ◽  
Jerzy Szawłowski
Keyword(s):  
Heat Treatment ◽  
Cross Sections ◽  
Nitrogen Saturation ◽  
Nitrided Layer ◽  
Isothermal Transformation ◽  
Isothermal Treatment ◽  
Surface Zone ◽  
Austenitizing Temperature ◽  
Treatment Processes ◽  
Different Content

This work was aimed at investigating the formation of nitrided layers during the isothermal transformation (austempering) and at describing the formed nitrided layer properties. The tested steels were characterized by a different content of carbon and alloying elements. In the case of the isothermal transformation, 4 variants of heat treatment parameters of nitrided layers were applied. The heat treatment differed in the austenitizing temperature (750°C–860°C) and the isothermal transformation temperature (390°C- 420°C). The microstructure and the mechanical properties (hardness) of the nitrided layers formed after the heat treatment processes were determined. After the nitriding process, during 30 hours in the nitriding atmosphere consisting only of ammonia, the high nitrogen saturation in the surface zone of the layers was obtained. The nitrided layers, after the heat treatment processes, were char-acterized by the diversified thickness, as evidenced by the hardness distributions at their cross-sections.

scholarly journals Effect of Quenching Media Variations on the Mechanical Behavior of Martensitic Stainless Steel

2019 ◽  
Vol 15 (2) ◽  
pp. 1-12 ◽  
Author(s):  
Abbas Kh. Hussein ◽  
Laith K. Abbas ◽  
Wisam N. Hasan
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Wear Rate ◽  
Process Parameters ◽  
Impact Energy ◽  
Salt Solution ◽  
Martensitic Stainless Steel ◽  
Austenitizing Temperature ◽  
Soaking Time ◽  
Α Al2o3

The purpose of this study is designate quenching and tempering heat treatment by using Taguchi technique to determine optimal factors of heat treatment (austenitizing temperature, percentage of nanoparticles, type of base media, nanoparticles type and soaking time) for increasing hardness, wear rate and impact energy properties of 420 martensitic stainless steel. An (L18) orthogonal array was chosen for the design of experiment. The optimum process parameters were determined by using signal-to-noise ratio (larger is better) criterion for hardness and impact energy while (Smaller is better) criterion was for the wear rate. The importance levels of process parameters that effect on hardness, wear rate and impact energy properties were obtained by using analysis of variance which applied with the help of (Minitab18) software. The variables of quenching heat treatment were austenitizing temperature (985 C˚,1060 C˚),a soaking times (50,70 and 90 minutes) respectively, Percentage of volumetric fractions of nanoparticles with three different levels(0.01, 0.03 and 0.08 %) were prepared by dispersing nanoparticles that are  (α-Al2O3,TiO2 and CuO) with base fluids (De-ionized water, salt solution and engine oil).The specimens were tempered at 700°C after quenching of nanofluids for  (2 hours).The results for ( S/N) ratios showed the order of the factors in terms of the proportion of their effect on hardness, and wear rate  properties as follow: Austenitizing temperature ( 1060 C˚),Type of base media (salt solution), Nanoparticles type (CuO), Percentage of nanoparticles (0.08%) and Soaking time(90min) was the least influence while for the impact energy were as follows: Type of base media (oil), Austenitizing temperature (985C˚), Percentage of nanoparticles (0.01%), Nanoparticles type (α-Al2O3) and last soaking time (50min).

Effect of Heat Treatment on the Microstructure of Cast Martensitic Stainless Steel

2021 ◽  
Vol 58 (4) ◽  
pp. 180-192
Author(s):  
F. van gen Hassend ◽  
S. Weber
Keyword(s):  
Heat Treatment ◽  
Stainless Steels ◽  
Martensitic Stainless Steel ◽  
Corrosion Resistant Steel ◽  
Resistant Steel ◽  
Eutectic Carbide ◽  
Corrosion Resistant ◽  
Martensitic Stainless Steels ◽  
Wear And Corrosion ◽  
Steel Castings

Abstract The resistance of martensitic stainless steels to wear and corrosion is greatly influenced by the martensitic matrix and the presence of carbides. The precipitation of carbides along the grain boundaries will lead to a significant decrease in fracture toughness and furthermore, will increase the risk of intergranular corrosion. With tools made of corrosion-resistant steel castings, this fact is of particular relevance as coarse eutectic carbide precipitates are normally not sufficiently dissolved during conventional austenitization. In this context, the dissolution of carbides will be studied on the basis of systematic heat treatment experiments and observed using light optical microscopy and the resulting microstructure and its impact on the mechanical properties (hardness) will be discussed in the following sections.

Effect of Heat Treatment on Microstructural Evolution of 13Cr Martensitic Stainless Steel

2017 ◽  
Vol 727 ◽  
pp. 29-35 ◽  
Author(s):  
Hou Yu Ma ◽  
Yin Sheng He ◽  
Kwon Yeong Lee ◽  
Kee Sam Shin
Keyword(s):  
Heat Treatment ◽  
Precipitation Hardening ◽  
Martensitic Stainless Steel ◽  
Tempering Temperature ◽  
Gas Industry ◽  
Martensitic Stainless Steels ◽  
Optimum Parameters ◽  
Tempering Treatment ◽  
Optimum Heat ◽  
Optimum Heat Treatment

13Cr martensitic stainless steels are widely used in gas industry, which are usually manufactured by quenching-tempering treatment. Microstructural study of 13Cr steel through various heat treatments was carried out for determining the optimum parameters for industry manufacture. After quenching treatment at 975 °C for 20 min, precipitation-free martensitic structures were formed. During tempering, recovery of martensite through grain boundaries migration and dislocations annihilation was found to soften the steel. In addition, transformation of needle-like Cr7C3 carbides to the irregular shaped Cr23C6 carbides was observed when tempering temperature is above 710 °C. The phase transformation induced precipitation strengthening is discussed. The optimum heat treatment parameters of 13Cr steel for avoiding over tempering and the precipitation hardening are found.

scholarly journals Jominy End Quench Test of Martensitic Stainless Steel X30Cr13

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1071
Author(s):  
Pierre Landgraf ◽  
Peter Birnbaum ◽  
Enrique Meza-García ◽  
Thomas Grund ◽  
Verena Kräusel ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Cooling Rate ◽  
Pitting Corrosion ◽  
Martensitic Stainless Steel ◽  
High Hardness ◽  
Optimum Process ◽  
Austenitizing Temperature ◽  
Fe Method ◽  
Corrosion Properties

In this study, the influence of thermal treatments on the properties of the martensitic stainless steel X30Cr13 (EN 10088-3: 1.4028) were investigated. These steels are characterized by a high hardness as well as corrosion resistance and can be specifically adjusted by heat treatment. In particular, the austenitizing temperature ϑA and cooling rate T˙ affect the hardness and corrosion properties of martensitic stainless steels. In order to investigate these influences, the Jominy end quench tests were performed at varying austenitizing temperatures. The aim is to determine the hardness and corrosion properties as a function of the austenitizing temperature and the cooling rate. The austenitizing temperature strongly influences the solubility of alloying elements within the austenitic lattice as well as the grain size, and thus affects both precipitation and phase transformation kinetics. In consequence, different austenitizing temperatures lead to different macroscopic material properties, like hardness and pitting corrosion potential. The heat treatment was simulated using finite element (FE) method and compared with time-temperature sequences measured at different locations of the Jominy end quench sample using thermocouples. That allows determining the cooling rate T˙ between 800∘C and 500∘C and to assign it to each location of the Jominy end quench sample. The numerical estimations were in close conformity with the experimental values. By assigning the hardness and pitting corrosion potentials to the respective cooling rates as a function of the austenitizing temperature, it is possible to determine optimum process windows for the required properties.

INFLUENCE THE QUENCHING AND TEMPERING ON THE MICROSTRUCTURE, MECHANICAL PROPERTIES AND SURFACE ROUGHNESS, OF MEDIUM CARBON STEEL

2018 ◽  
Vol 18 (1) ◽  
pp. 125-135
Author(s):  
Sattar H A Alfatlawi
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Surface Roughness ◽  
Carbon Steel ◽  
Cold Water ◽  
Medium Carbon Steel ◽  
Medium Carbon ◽  
Heating And Cooling ◽  
Treatment Processes ◽  
Quenching And Tempering

One of ways to improve properties of materials without changing the product shape toobtain the desired engineering applications is heating and cooling under effect of controlledsequence of heat treatment. The main aim of this study was to investigate the effect ofheating and cooling on the surface roughness, microstructure and some selected propertiessuch as the hardness and impact strength of Medium Carbon Steel which treated at differenttypes of heat treatment processes. Heat treatment achieved in this work was respectively,heating, quenching and tempering. The specimens were heated to 850°C and left for 45minutes inside the furnace as a holding time at that temperature, then quenching process wasperformed in four types of quenching media (still air, cold water (2°C), oil and polymersolution), respectively. Thereafter, the samples were tempered at 200°C, 400°C, and 600°Cwith one hour as a soaking time for each temperature, then were all cooled by still air. Whenthe heat treatment process was completed, the surface roughness, hardness, impact strengthand microstructure tests were performed. The results showed a change and clearimprovement of surface roughness, mechanical properties and microstructure afterquenching was achieved, as well as the change that took place due to the increasingtoughness and ductility by reducing of brittleness of samples.

Wear volume prediction of AISI H13 die steel using response surface methodology and artificial neural network

2020 ◽  
Vol 14 (2) ◽  
pp. 6789-6800
Author(s):  
Vishal Jagota ◽  
Rajesh Kumar Sharma
Keyword(s):  
Neural Network ◽  
Heat Treatment ◽  
Artificial Neural Network ◽  
Response Surface ◽  
Sliding Wear ◽  
Austenitizing Temperature ◽  
Tempering Temperature ◽  
Die Steel ◽  
Artificial Neural ◽  
Tempering Time

Resistance to wear of hot die steel is dependent on its mechanical properties governed by the microstructure. The required properties for given application of hot die steel can be obtained with control the microstructure by heat treatment parameters. In the present paper impact of different heat treatment parameters like austenitizing temperature, tempering time, tempering temperature is studied using response surface methodology (RSM) and artificial neural network (ANN) to predict sliding wear of H13 hot die steel. After heat treating samples at austenitizing temperature of 1020°C, 1040°C and 1060°C; tempering temperature 540°C, 560°C and 580°C; tempering time 1hour, 2hours and 3hours, experimentation on pin-on-disc tribo-tester is done to measure the sliding wear of H13 die steel. Box-Behnken design is used to develop a regression model and analysis of variance technique is used to verify the adequacy of developed model in case of RSM. Whereas, multi-layer feed-forward backpropagation architecture with input layer, single hidden layer and an output layer is used in ANN. It was found that ANN proves to be a better tool to predict sliding wear with more accuracy. Correlation coefficient R2 of the artificial neural network model is 0.986 compared to R2 of 0.957 for RSM. However, impact of input parameter interactions can only be analysed using response surface method. In addition, sensitivity analysis is done to determine the heat treatment parameter exerting most influence on the wear resistance of H13 hot die steel and it showed that tempering time has maximum influence on wear volume, followed by tempering temperature and austenitizing temperature. The prediction models will help to estimate the variation in die lifetime by finding the amount of wear that will occur during use of hot die steel, if the heat treatment parameters are varied to achieve different properties.

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