scholarly journals The Effect of Energy Density and Nb Content on the Microstructure and Mechanical Properties of Selective Laser Melted Ti-(10-30 wt.%) Nb

2021 ◽  
Author(s):  
James M. Borgman ◽  
Jing Wang ◽  
Lorenzo Zani ◽  
Paul P. Conway ◽  
Carmen Torres-Sanchez
Keyword(s):  
Mechanical Properties ◽  
Energy Density ◽  
Mechanical Performance ◽  
Post Processing ◽  
Laser Melting ◽  
Solid Solution Strengthening ◽  
Nb Content ◽  
Compositional Homogeneity ◽  
Solution Strengthening

AbstractIn this study, Ti-(0-30 wt.%)Nb alloys developed from elemental powders were fabricated by the Selective Laser Melting (SLM) process. Compositional homogeneity, microstructure and mechanical performance were investigated as a function of energy density. The proportion of un-melted Nb particles and isolated pore count reduced with increasing energy density, while Ti allotropic content (i.e. α’, α” and β) varied with energy density due to in-situ alloying. Increasing the Nb content led to the stabilisation of the α” and β phases. The mechanical properties were similar to those compositions manufactured using casting methods, without further post processing. The addition of 20Nb (wt.%) and using an energy density of 230 J/mm3 resulted in a Young’s Modulus of 65.2 ± 1.8 GPa, a yield strength of 769 ± 36 MPa and a microstructure of predominantly α” martensite. This strength to stiffness ratio (33% higher than Ti-10Nb and 22% higher than Ti-30Nb), is attributed to in-situ alloying that promotes solid solution strengthening and homogenisation. These alloys are strong contenders as materials suitable for implantable load-bearing orthopaedic applications.

In Situ Decomposition of Silicon Nitride Particles in Titanium Composite and its Mechanical Properties

2017 ◽  
Vol 737 ◽  
pp. 38-43
Author(s):  
Hisashi Imai ◽  
Hiroyasu Yamabe ◽  
Katsuyoshi Kondoh ◽  
Junko Umeda ◽  
Anak Khantachawana
Keyword(s):  
Mechanical Properties ◽  
Silicon Nitride ◽  
Solid Phase ◽  
High Strength ◽  
Solid Solution Strengthening ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Solution Strengthening ◽  
Ti Powder

Dependence of the mechanical properties of PM extruded titanium with the silicon nitride (Si3N4) on solid phase decomposition of Si3N4 was investigated. Si3N4 particles within Ti composite powder were decomposed during spark plasma sintering at 1223 K with 30 MPa pressure for 3.6 ks; and then, decomposition by-products of nitrogen and silicon atoms were defused into titanium matrix. The extruded Ti-1.0 mass% Si3N4 composite showed ultimate tensile strength (UTS) of 1139 MPa, and yield stress (0.2%YS) of 1065 MPa. UTS and 0.2%YS of P/M extruded Ti-1.0 mass% Si3N4 composite were 2 and 2.5 times compared to extruded pure Ti powder material, respectively. It was considered that the solid solution strengthening of both nitrogen and silicon originated from Si3N4 caused the high strength of PM extruded Ti-1.0 mass% Si3N4 composite.

Selective Laser Melting Additive Manufacturing of Novel Aluminum Based Composites With Multiple Reinforcing Phases

2015 ◽  
Vol 137 (2) ◽  
Author(s):  
Dongdong Gu ◽  
Fei Chang ◽  
Donghua Dai
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Energy Density ◽  
Selective Laser Melting ◽  
Laser Energy ◽  
Laser Energy Density ◽  
Wear Property ◽  
Laser Melting ◽  
Sic Particles

The selective laser melting (SLM), due to its unique additive manufacturing (AM) processing manner and laser-induced nonequilibrium rapid melting/solidification mechanism, has a promising potential in developing new metallic materials with tailored performance. In this work, SLM of the SiC/AlSi10Mg composites was performed to prepare the Al-based composites with the multiple reinforcing phases. The influence of the SLM processing parameters on the constitutional phases, microstructural features, and mechanical performance (e.g., densification, microhardness, and wear property) of the SLM-processed Al-based composites was studied. The reinforcing phases in the SLM-processed Al-based composites included the unmelted micron-sized SiC particles, the in situ formed micron-sized Al4SiC4 strips, and the in situ produced submicron Al4SiC4 particles. As the input laser energy density increased, the extent of the in situ reaction between the SiC particles and the Al matrix increased, resulting in the larger degree of the formation of Al4SiC4 reinforcement. The densification rate of the SLM-processed Al-based composite parts increased as the applied laser energy density increased. The sufficiently high density (∼96% theoretical density (TD)) was achieved for the laser linear energy density larger than 1000 J/m. Due to the generation of the multiple reinforcing phases, the elevated mechanical properties were obtained for the SLM-processed Al-based composites, showing a high microhardness of 214 HV0.1, a considerably low coefficient of friction (COF) of 0.39, and a reduced wear rate of 1.56 × 10−5 mm3 N−1 m−1. At an excessive laser energy input, the grain size of the in situ formed Al4SiC4 reinforcing phase, both the strip- and particle-structured Al4SiC4, increased markedly. The significant grain coarsening and the formation of the interfacial microscopic shrinkage porosity lowered the mechanical properties of the SLM-processed Al-based composites. These findings in the present work are applicable and/or transferrable to other laser-based powder processing processes, e.g., laser cladding, laser metal deposition, or laser engineered net shaping.

scholarly journals Novel Co-Cu-Based Immiscible Medium-Entropy Alloys with Promising Mechanical Properties

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 238
Author(s):  
Sujung Son ◽  
Jongun Moon ◽  
Hyeonseok Kwon ◽  
Peyman Asghari Rad ◽  
Hidemi Kato ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Binary System ◽  
Design Methodology ◽  
Miscibility Gap ◽  
Face Centered Cubic ◽  
Solid Solution Strengthening ◽  
Solution Strengthening ◽  
Face Centered ◽  
Strength And Ductility ◽  
Cobalt Copper

New AlxCo50−xCu50−xMnx (x = 2.5, 10, and 15 atomic %, at%) immiscible medium-entropy alloys (IMMEAs) were designed based on the cobalt-copper binary system. Aluminum, a strong B2 phase former, was added to enhance yield strength and ultimate tensile strength, while manganese was added for additional solid solution strengthening. In this work, the microstructural evolution and mechanical properties of the designed Al-Co-Cu-Mn system are examined. The alloys exhibit phase separation into dual face-centered cubic (FCC) phases due to the miscibility gap of the cobalt-copper binary system with the formation of CoAl-rich B2 phases. The hard B2 phases significantly contribute to the strength of the alloys, whereas the dual FCC phases contribute to elongation mitigating brittle fracture. Consequently, analysis of the Al-Co-Cu-Mn B2-strengthened IMMEAs suggest that the new alloy design methodology results in a good combination of strength and ductility.

scholarly journals A Short Review on the Phase Structures, Oxidation Kinetics, and Mechanical Properties of Complex Ti-Al Alloys

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1677
Author(s):  
Hooi Peng Lim ◽  
Willey Yun Hsien Liew ◽  
Gan Jet Hong Melvin ◽  
Zhong-Tao Jiang
Keyword(s):  
Mechanical Properties ◽  
Oxidation Kinetics ◽  
Mass Gain ◽  
Short Review ◽  
Al Alloys ◽  
Alloying Elements ◽  
Isothermal Exposure ◽  
Solid Solution Strengthening ◽  
Phase Structures ◽  
Solution Strengthening

This paper reviews the phase structures and oxidation kinetics of complex Ti-Al alloys at oxidation temperatures in the range of 600–1000 °C. The mass gain and parabolic rate constants of the alloys under isothermal exposure at 100 h (or equivalent to cyclic exposure for 300 cycles) is compared. Of the alloying elements investigated, Si appeared to be the most effective in improving the oxidation resistance of Ti-Al alloys at high temperatures. The effect of alloying elements on the mechanical properties of Ti-Al alloys is also discussed. Significant improvement of the mechanical properties of Ti-Al alloys by element additions has been observed through the formation of new phases, grain refinement, and solid solution strengthening.

scholarly journals In-situ reactions and mechanical properties of 6061 aluminum alloy weld joint with SiCp by laser melting injection

2021 ◽  
Vol 203 ◽  
pp. 109538
Author(s):  
Boan Xu ◽  
Ping Jiang ◽  
Shaoning Geng ◽  
Yilin Wang ◽  
Jintian Zhao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Aluminum Alloy ◽  
Weld Joint ◽  
Laser Melting ◽  
6061 Aluminum Alloy ◽  
In Situ Reactions ◽  
Alloy Weld

Effect of Ti Element on Microstructure and Properties of Cu-Cr Alloy

2015 ◽  
Vol 817 ◽  
pp. 307-311 ◽  
Author(s):  
Peng Chao Zhang ◽  
Jin Chuan Jie ◽  
Yuan Gao ◽  
Tong Min Wang ◽  
Ting Ju Li
Keyword(s):  
Mechanical Properties ◽  
Solid Solution ◽  
Spherical Shape ◽  
Precipitation Strengthening ◽  
Peak Hardness ◽  
Ti Alloy ◽  
Strengthening Mechanisms ◽  
Vacuum Melting ◽  
Solid Solution Strengthening ◽  
Solution Strengthening

The Cu-Cr and Cu-Cr-Ti alloy plates were prepared by vacuum melting and plastic deformation. The effect of slight Ti element on microstructure and mechanical properties of Cu-Cr alloy was discussed. The result shows that Cr particles with spherical shape precipitated from Cu matrix after aging. Plenty Ti atoms dissolved in the vicinity of Cr particles and there were still parts of solid solution Ti atoms in other regions. Improvements in peak hardness and softening resistance were achieved with the addition of Ti element in Cu-Cr alloy. The addition of 0.1 wt.% Ti element makes Cu-Cr alloy possess tensile strength of 565 MPa and hardness of 185.9 HV after aging at 450 °C for 120 min, which can be attributed to multiple strengthening mechanisms, i.e. work hardening, solid solution strengthening and precipitation strengthening.

scholarly journals Mechanical Properties of In-Situ Synthesis of Ti-Ti3Al Metal Composite Prepared by Selective Laser Melting

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1121 ◽  
Author(s):  
Li ◽  
Liang ◽  
Tian ◽  
Yang ◽  
Xie ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Selective Laser Melting ◽  
Melting Process ◽  
In Situ Synthesis ◽  
Metal Composite ◽  
Dispersion Strengthening ◽  
Laser Melting ◽  
Compression Properties

Titanium composite strengthened by Ti3Al precipitations is considered to be one of the excellent materials that is widely used in engineering. In this work, we prepared a kind of Ti-Ti3Al metallic composite by in-situ synthesis technology during the SLM (selective laser melting) process, and analyzed its microstructure, wear resistance, microhardness, and compression properties. The results showed that the Ti-Ti3Al composite, prepared by in-situ synthesis technology based on SLM, had more homogeneous Ti3Al-enhanced phase dispersion strengthening structure. The grain size of the workpiece was about 1 μm, and that of the Ti3Al particle was about 200 nm. Granular Ti3Al was precipitated after the aluminum-containing workpiece formed, with a relatively uniform distribution. Regarding the mechanical properties, the hardness (539 HV) and the wear resistance were significantly improved when compared with the Cp-Ti workpiece. The compressive strength of the workpiece increased from 886.32 MPa to 1568 MPa, and the tensile strength of the workpiece increased from 531 MPa to 567 MPa after adding aluminum. In the future, the combination of in-situ synthesis technology and SLM technology can be used to flexibly adjust the properties of Ti-based materials.

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