scholarly journals Spray-drying of alumina powder for APS: effect of slurry properties and drying conditions upon particle size and morphology of feedstock

2011 ◽  
Vol 34 (7) ◽  
pp. 1653-1661 ◽  
Author(s):  
Bai Yu ◽  
Yang Jian Feng ◽  
Lee Soo Wohn ◽  
Chen Huang ◽  
Yu Fang Li ◽  
...  
Keyword(s):  
Particle Size ◽  
Spray Drying ◽  
Alumina Powder ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Drying Conditions

scholarly journals Dehumidified Air-Assisted Spray-Drying of Cloudy Beetroot Juice at Low Temperature

2021 ◽  
Vol 11 (14) ◽  
pp. 6578
Author(s):  
Aleksandra Jedlińska ◽  
Alicja Barańska ◽  
Dorota Witrowa-Rajchert ◽  
Ewa Ostrowska-Ligęza ◽  
Katarzyna Samborska
Keyword(s):  
Particle Size ◽  
Physicochemical Properties ◽  
Spray Drying ◽  
Low Temperatures ◽  
Beetroot Juice ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Tapped Density ◽  
Lower Loss ◽  
Better Than

This paper discusses the physicochemical properties of powders obtained by spray drying of cloudy beetroot juice, using dehumidified air in variants with or without carriers. The inlet air temperature was 130 °C or 90 °C, and the addition of the carriers was at a ratio of juice to carrier solids of 3:2. In the obtained powders, the following physicochemical properties were determined: water content and water activity, apparent density, loose and tapped density, porosity, flowability, particle size and morphology, and the content and retention of betalains. It was possible to dry cloudy beetroot juice without the use of carriers at low temperatures (90 or 130 °C). The 100% beetroot powders were characterized by satisfactory physicochemical properties, often better than those with carriers (including lower hygroscopicity and higher color saturation and yield). A lower loss of betalains was found for the powders with the addition of carriers. The best process yields were obtained for the powder without carriers at 130 °C and 90 °C.

Preparation of Flaky Alumina Powder by Molten Salt Synthesis Method

2014 ◽  
Vol 997 ◽  
pp. 428-432
Author(s):  
Qian Ying Zhang ◽  
Xun Geng
Keyword(s):  
Particle Size ◽  
Molten Salt ◽  
Synthesis Method ◽  
Morphology Control ◽  
Molten Salt Synthesis ◽  
Alumina Powder ◽  
High Quality ◽  
Uniform Size ◽  
Particle Size And Morphology ◽  
Size And Morphology

High-quality flaky α-Al2O3 powder with regular morphology, uniform size, larger diameter-thickness proportion and excellent dispersibility in water and free from agglomeration and staggered growth was obtained on the basis of molten salt synthesis method. The effects of experiment parameter on the particle size and morphology of flaky alumina powder were studied. The mechanism of morphology control was discussed.

scholarly journals Uniform Chitosan Microparticles Prepared by a Novel Spray-Drying Technique

2011 ◽  
Vol 2011 ◽  
pp. 1-7 ◽  
Author(s):  
Wenjie Liu ◽  
Winston Duo Wu ◽  
Cordelia Selomulya ◽  
Xiao Dong Chen
Keyword(s):  
Particle Size ◽  
Spray Drying ◽  
Storage Time ◽  
Particle Morphology ◽  
Surface Characteristics ◽  
Single Step ◽  
Drying Temperature ◽  
Chitosan Microparticles ◽  
Particle Size And Morphology ◽  
Size And Morphology

Particle size and morphology are important properties of pharmaceutical particles. Preparation of microparticles with uniform particle size and morphology is necessary in order to systematically relate these properties to the release behavior and other functionalities such as drug encapsulation and dissolution. In this study, we successfully prepared monodisperse, nonagglomerated chitosan microparticles in a single step by a novel spray-drying technique. The control of particle size and morphology of spray-dried microparticles was investigated experimentally. Microparticles with larger particle size can be produced when chitosan precursor of higher concentration was used. Storage time of chitosan precursor, drying temperature, and addition of lactose were shown to be crucial parameters that affect the particle morphology. Appropriate choice of the drying temperature and precursor storage time permitted control of the particle morphology, ranging from nearly spherical to cap-shaped. Surface characteristics of the particles can be finely tuned by the amount of lactose added into the chitosan precursor.

Influence of Spray Drying Conditions on Particle Size and Morphology of Al2O3/ZrO2(3Y) Composite Particles

2017 ◽  
Vol 728 ◽  
pp. 172-177 ◽  
Author(s):  
Saowaluk Chiangka ◽  
Sukasem Watcharamaisakul ◽  
Boris Golman
Keyword(s):  
Spray Drying ◽  
Solid Content ◽  
Composite Particles ◽  
Inlet Temperature ◽  
Sem Images ◽  
Median Diameter ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Drying Conditions ◽  
Monolithic Alumina

Zirconia toughened alumina materials are frequently used in biomedical applications due to their enhanced toughness, strength and wear resistance compared to monolithic alumina. In this work, the influence of spray drying conditions is studied on the characteristics of spray-dried Al2O3/ZrO2(3Y) composite particles. The SEM images of composite particles confirm the formation of dense composite particles of round shape without internal holes. The particles of the best morphology of the median diameter of 44 µm were produced by drying the slurry of 70 wt.% solid content with feed rate of 15 ml/min using the drying air with inlet temperature of 210 °C and spraying air with flow rate of 357 l/h.

Direct manipulation of particle size and morphology of ordered mesoporous silica by flow synthesis

RSC Advances ◽  
2015 ◽  
Vol 5 (18) ◽  
pp. 13331-13340 ◽  
Author(s):  
T. N. Ng ◽  
X. Q. Chen ◽  
K. L. Yeung
Keyword(s):  
Particle Size ◽  
Mesoporous Silica ◽  
Hollow Spheres ◽  
Ordered Mesoporous Silica ◽  
Direct Manipulation ◽  
Flow Synthesis ◽  
Precise Control ◽  
Ordered Mesoporous ◽  
Particle Size And Morphology ◽  
Size And Morphology

Flow-synthesis of mesoporous silica allows deliberate and precise control over the size and shapes and enables the preparation of complex microstructures (i.e., hollow spheres).

Synthesis and Properties of (Bi0.5Na0.5)TiO3 Powders by Hydrothermal Method

2007 ◽  
Vol 336-338 ◽  
pp. 140-142
Author(s):  
Jun Jie Hao ◽  
Xiao Hui Wang ◽  
Shi Yun Lin ◽  
Long Tu Li
Keyword(s):  
Particle Size ◽  
Hydrothermal Method ◽  
Single Phase ◽  
Piezoelectric Ceramics ◽  
Treatment Temperature ◽  
Lead Free ◽  
Excellent Candidate ◽  
Traditionally Prepared ◽  
Particle Size And Morphology ◽  
Size And Morphology

Na0.5Bi0.5TiO3 (NBT) is considered to be an excellent candidate for lead-free piezoelectric ceramics. In this study, we propose a hydrothermal method for the preparation of single phase NBT powder at relatively low treatment-temperature. The particle size and morphology of the synthesized powders were examined by SEM. The powders were further pressed into disk and sintered at 1120°C/2h in air, and its properties and microstructure were compared with traditionally prepared samples.

Particle-size and morphology dependence of the preferred interface orientation in LiFePO4 nano-particles

2014 ◽  
Vol 2 (37) ◽  
pp. 15437-15447 ◽  
Author(s):  
Aziz Abdellahi ◽  
Oncu Akyildiz ◽  
Rahul Malik ◽  
Katsuyo Thornton ◽  
Gerbrand Ceder
Keyword(s):  
Particle Size ◽  
First Principles ◽  
Nano Particles ◽  
Particle Size And Morphology ◽  
Interface Orientation ◽  
Size And Morphology

Using calculations based on first principles, we demonstrate that the preferred interface in singles LiFePO4 particles depends both on the particle size and morphology.

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