Interactions of coal gangue and pine sawdust during combustion of their blends studied using differential thermogravimetric analysis

2016 ◽  
Vol 214 ◽  
pp. 396-403 ◽  
Author(s):  
Yuanyuan Zhang ◽  
Zhezi Zhang ◽  
Mingming Zhu ◽  
Fangqin Cheng ◽  
Dongke Zhang
Keyword(s):  
Thermogravimetric Analysis ◽  
Coal Gangue ◽  
Pine Sawdust ◽  
Differential Thermogravimetric Analysis

scholarly journals Synthesis and Electrochemical Properties of C/LiMnPO4 Cathode Materials by Complex Polymerized Method

2011 ◽  
Vol 485 ◽  
pp. 115-118
Author(s):  
Atsushi Fujita ◽  
Fuminari Isobe ◽  
Takayuki Kodera ◽  
Takashi Ogihara
Keyword(s):  
Thermogravimetric Analysis ◽  
Electrochemical Properties ◽  
Carbon Content ◽  
Discharge Capacity ◽  
Cathode Materials ◽  
Type Structure ◽  
Initial Discharge Capacity ◽  
Initial Discharge ◽  
Differential Thermogravimetric Analysis

C/LiMnPO4 materials were synthesized by the complex polymerized method. An orthorhombic olivine type structure was obtained by calcination at temperatures over 973 K under an argon/hydrogen (5%) atmosphere. Differential thermogravimetric analysis showed that the carbon content of C/LiMnPO4 was about 65 wt%. The initial discharge capacity of C/LiMnPO4 calcined at 973 K was 135 mAh/g at 0.1 C and 60 mAh/g at 1 C.

Effect of oxygen concentration on oxy-fuel combustion characteristic and interactions of coal gangue and pine sawdust

2019 ◽  
Vol 87 ◽  
pp. 288-294 ◽  
Author(s):  
Yuanyuan Zhang ◽  
Jiangting Zhao ◽  
Zhibin Ma ◽  
Fengling Yang ◽  
Fangqin Cheng
Keyword(s):  
Oxygen Concentration ◽  
Fuel Combustion ◽  
Coal Gangue ◽  
Combustion Characteristic ◽  
Pine Sawdust ◽  
Effect Of Oxygen

Polymerization studies: The application of differential thermogravimetric analysis

1993 ◽  
Vol 50 (8) ◽  
pp. 1475-1482 ◽  
Author(s):  
Ivanka G. Popović ◽  
Lynne Katsikas ◽  
Horst Weller ◽  
Susanne Schrötter ◽  
Jovan S. Veliĉkoví
Keyword(s):  
Thermogravimetric Analysis ◽  
Differential Thermogravimetric Analysis

Thermal Degradation of Aged Chloroprene Rubber Studied by Thermogravimetric Analysis

2001 ◽  
Vol 74 (4) ◽  
pp. 622-629 ◽  
Author(s):  
Elton L. G. Denardin ◽  
Dimitrios Samios ◽  
Paulo R. Janissek ◽  
Gabriel P. de Souza
Keyword(s):  
Thermogravimetric Analysis ◽  
Thermal Degradation ◽  
Mass Loss ◽  
Activation Energies ◽  
Half Width ◽  
Temperature Elevation ◽  
Kinetic Methods ◽  
Degradation Processes ◽  
Chloroprene Rubber ◽  
Differential Thermogravimetric Analysis

Abstract The thermal degradation of original and aged chloroprene rubber was studied using thermogravimetric analysis. Thermogravimetric analysis (TGA) and differential thermogravimetric analysis (DTG) techniques were used to detect the mass loss during the temperature elevation. By the analysis of the mass loss curves through usual kinetic methods, it was possible to evaluate the different degradation processes present in the overall degradation. The activation energies of the degradation processes were obtained using the dynamic, non-isothermal Kissinger and Osawa methods and the half-width at half-high technique (HWHH). The results obtained demonstrate clearly the differences between original and aged chloroprene rubber as well as the influence of the air and N2 in TGA.

scholarly journals Effect of ZnSO4 and MnSO4 on the Growth of Sulphamic Acid Single Crystals

2018 ◽  
Vol 15 (2) ◽  
pp. 151-158 ◽  
Author(s):  
K.G. Anupriya ◽  
P. Hemalatha
Keyword(s):  
Thermogravimetric Analysis ◽  
Single Crystals ◽  
Second Harmonic ◽  
Spectral Studies ◽  
X Ray Diffraction ◽  
X Ray ◽  
Evaporation Technique ◽  
Differential Thermogravimetric Analysis ◽  
Sulphamic Acid ◽  
Vicker’S Microhardness

Single crystals of Sulphamic Acid doped with Zinc Sulphate and Manganese Sulphate were grown at room temperature using slow evaporation technique. Structural analysis of the grown crystals was done using single crystal X Ray Diffraction and powder X Ray Diffraction studies. Various functional groups seen in the grown crystals are determined using FTIR spectroscopic analysis. The cut-off wavelength of ZnSO4 and MnSO4 doped Sulphamic acid were evaluated by UV-Vis-NIR spectral studies. Thermal behaviour of the grown crystals was identified from Thermogravimetric Analysis (TGA) and Differential Thermogravimetric Analysis (DTA). The mechanical strength and Second harmonic generation of the grown crystals was identified by Vicker’s Microhardness Test and Kurtz powder technique respectively.

scholarly journals Nature and adsorption capacity of banana leaf rim carbon

2017 ◽  
Vol 20 (1) ◽  
pp. 49-56
Keyword(s):  
Thermogravimetric Analysis ◽  
Adsorption Capacity ◽  
Adsorption Process ◽  
Experimental Result ◽  
Factors Affecting ◽  
Malachite Green Dye ◽  
Infrared Spectrometer ◽  
Ft Ir ◽  
Differential Thermogravimetric Analysis ◽  
Banana Leaf

The activated charcoal (AC) was synthesized from banana leaf rim (BLR) through three activation methods; physical (BLRC), chemical (Z BLRC, zinc chloride) and microwave activation (MW BLRC). The AC was characterized using fourier transform infrared spectrometer (FT-IR), Thermogravimetric analysis (TGA) & Differential thermogravimetric analysis (DTA) instrument and Field emission scanning electron microscope (FE-SEM). The Z BLRC has better thermal stability and adsorbent character compared with BLRC or MW BLRC. The present work is confined to an investigation on the adsorption process of Malachite green dye onto BLRC, Z BLRC & MW BLRC. Factors affecting adsorption process were studied and results that adsorption increases with concentration of dye, agitation time and temperature. This experimental data satisfied the Langmuir adsorption isotherm model. Second order kinetics holds good for the present adsorption process. Thermodynamic parameters were (∆H‡, ∆S‡ & ∆G‡) evaluated. Based on the characterization and adsorption experimental result it may be concluded that Z BLRC has better adsorption capacity than BLRC or MW BLRC.

scholarly journals Desorption characteristics and kinetic parameters determination of molecular sieve by thermogravimetric analysis/differential thermogravimetric analysis technique

2018 ◽  
Vol 36 (7-8) ◽  
pp. 1389-1404 ◽  
Author(s):  
Yalou Guo ◽  
Hui Zhang ◽  
Yingshu Liu
Keyword(s):  
Activation Energy ◽  
Thermogravimetric Analysis ◽  
Heating Rates ◽  
Carrier Gas ◽  
Zeolite 13X ◽  
Analysis Technique ◽  
Desorption Activation Energy ◽  
Differential Thermogravimetric Analysis ◽  
Kinetics Of

The kinetics of the thermal desorption of CO2 adsorbed on zeolite 13X were obtained using a differential thermogravimetric analyser under two different carrier gas conditions. The varying heating rates were set as 8, 12, 16, and 20 K min−1, respectively. The desorption activation energy of the physisorption sites for this experiment evaluated by an integral method without prediction of the reaction order ranged from 12.15 to 14.12 kJ mol−1 (CO2 as the carrier gas) and 43.32 to 50.42 kJ mol−1 (Ar as the carrier gas), respectively. The desorption activation energy of the chemisorption sites ranged from 57.95 to 58.53 kJ mol−1 (CO2 as the carrier gas) and 74.02 to 79.92 kJ mol−1 (Ar as the carrier gas), respectively.

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